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POCl3 via P2O5 + NaCl in borosilicate glass?
Has anybody prepared phosphoryl chloride via the following method? I found it within a small-scale r ... |
16-7-2021 at 12:06
by: Opylation |
Copper hydride as a reducing agent?
That’s interesting. If copper hydride is easily made then maybe the borohydride could be prepared ... |
20-6-2021 at 04:35
by: Opylation |
Interesting hydrodechlorination of PCE to (edit) dichloroethylene
Hello all, on my search for a neat chloral procedure for its use in preparing trichloroacetic acid I ... |
20-6-2021 at 04:30
by: Opylation |
Forming oxalte salts of amines
I know this is an old thread, but I found the conversation intriguing and wanted to add a little bit ... |
16-6-2021 at 17:11
by: Opylation |
Sythesis proposal for preparing 1,3-benzodioxole oxidation products using simple precursors
If you’re looking for a phenolic dealkylation procedure then take a look at this paper. The most O ... |
14-6-2021 at 21:13
by: Opylation |
Oxalyl Chloride Challenge
Off topic… removed for irrelevance
[Edited on 10-6-2021 by Opylation] |
9-6-2021 at 17:44
by: Opylation |
Oxalyl Chloride Challenge
I would like to post one more paper, a parent actually, that describes the preparation on oxalyl chl ... |
8-6-2021 at 16:29
by: Opylation |
Oxalyl Chloride Challenge
Liquid bromine and Oxalic acid react to form hypobromic acid, carbon monoxide and carbon dioxide. Hy ... |
8-6-2021 at 01:58
by: Opylation |
Oxalyl Chloride Challenge
Just would like to provide an update that I have found a patent on the preparation of tetrachloroeth ... |
8-6-2021 at 01:12
by: Opylation |
Carbon disulfide synthesis (alternative routes)
I’m not quite sure. I haven’t performed this reaction but have logged it for when I have time to ... |
6-6-2021 at 03:15
by: Opylation |
Acetaldehyde synthesis
[rquote=659047&tid=55&author=EverythingAl2O3]Have we also considered the Corey-Kim oxidation ... |
5-6-2021 at 19:32
by: Opylation |
Preparation of dimethyl carbonate without autoclave or phosgene
If your goal is to truly prepare dimethyl carbonate I have no tips or tricks to give. But I do want ... |
5-6-2021 at 13:43
by: Opylation |
Carbon disulfide synthesis (alternative routes)
Ammonia and Carbon Disulfide react to form ammonium thiocyanate and hydrogen sulfide. However, what ... |
5-6-2021 at 00:30
by: Opylation |
toluene --> benzaldehyde
I don't have any experience going through the procedure, but the salicylaldehyde synthesis via pheno ... |
4-6-2021 at 14:55
by: Opylation |
Carbon disulfide synthesis (alternative routes)
[rquote=661017&tid=147199&author=garphield]Cyanamide will react with hydrogen sulfide to gen ... |
4-6-2021 at 10:49
by: Opylation |
toluene --> benzaldehyde
This isn’t toluene, but phenol (made easily from salicylic acid) can be reacted with chloroform an ... |
4-6-2021 at 10:15
by: Opylation |
Oxalyl Chloride Challenge
I found a paper on cyclic oxalate ester formation and properties. It looks like ethylene oxalate has ... |
4-6-2021 at 09:49
by: Opylation |
Preparation of dimethylamine
I would just like to mention, “2,4-D” is an herbicide readily sold in hardware stores in the US ... |
4-6-2021 at 08:53
by: Opylation |
Oxalyl Chloride Challenge
I was just thinking back to the ethylene carbonate -> chlorination -> oxalyl chloride + phosge ... |
3-6-2021 at 18:48
by: Opylation |
Cicada fungi
I believe psilocin when shielded from light and oxygen can last a relatively long time compared to w ... |
3-6-2021 at 18:11
by: Opylation |
Cicada fungi
“What’s wrong? Fungus got your nethers?”
That’s super interesting though. I wonder if it ... |
3-6-2021 at 12:45
by: Opylation |
Retrofinkelstein reaction (baseless inquiry)
I was referring to 1.2-dichloroethane. I was under the impression that ethylene glycol + HCl makes e ... |
3-6-2021 at 01:33
by: Opylation |
Retrofinkelstein reaction (baseless inquiry)
So, let me start this by saying my mind wonders when thinking of solutions to unasked questions. I w ... |
2-6-2021 at 23:59
by: Opylation |
Pyridine hydrogenation - methods?
Here's a couple different sources I had logged away for the reduction of pyridine and substituted py ... |
23-5-2021 at 13:29
by: Opylation |
Oxalyl Chloride Challenge
[rquote=660556&tid=82462&author=clearly_not_atara]BzCl + H2C2O4 >> BzOH + CO2 + CO + H ... |
22-5-2021 at 19:57
by: Opylation |
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