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Benzoic Acid, Carbamid>Benzamid>Anilin?
[quote][i]Originally posted by garage chemist[/i]
Would you give us a report of the synthesis, e.g. ... |
21-12-2006 at 00:41
by: Pabpa |
Benzoic Acid, Carbamid>Benzamid>Anilin?
I just tried the Organikum synthesis of aniline with success. Took bleach (2.8% NaOCl solution -> ... |
17-12-2006 at 04:04
by: Pabpa |
Benzoic Acid, Carbamid>Benzamid>Anilin?
[quote] I have looked in Organikum and they give a procedure which uses NaOCl, made directly before ... |
9-12-2006 at 05:00
by: Pabpa |
Benzoic Acid, Carbamid>Benzamid>Anilin?
[quote]Are the proportons of 1 part benzoic acid and 2 parts urea correct? If yes, then it's a large ... |
8-12-2006 at 14:14
by: Pabpa |
Benzoic Acid, Carbamid>Benzamid>Anilin?
[quote]
But the walls where almost full of crystals after some minutes [/quote]
Are these crysta ... |
8-12-2006 at 02:46
by: Pabpa |
Benzoic Acid, Carbamid>Benzamid>Anilin?
[quote]Btw.: the Phosphoric acid might maybe help to prevent the sublimation (or what ever) by washi ... |
8-12-2006 at 01:22
by: Pabpa |
Benzoic Acid, Carbamid>Benzamid>Anilin?
[quote] The sublimation of the benzoic acid every time spoiled any success ... [/quote]
Are you s ... |
7-12-2006 at 23:26
by: Pabpa |
Benzoic Acid, Carbamid>Benzamid>Anilin?
Hi,
I've done this reaction several times. It's very easy: 1kg benzoic acid, 2kg urea and 10ml ph ... |
7-12-2006 at 11:47
by: Pabpa |
o-Toluidine from xylene
[quote]IT sounds interesting, im looking for more data on it. [/quote]
http://en.wikipedia.org/wi ... |
29-11-2006 at 15:14
by: Pabpa |
o-Toluidine from xylene
[quote]I still think that the xylene to toluic acid to amide to amine route is the best. [/quote]
... |
28-11-2006 at 12:45
by: Pabpa |
o-Toluidine from xylene
o-xylene -> o-toluic acid:
http://www.orgsyn.org/orgsyn/orgsyn/prepcontent.asp?print=1&pre ... |
27-11-2006 at 08:58
by: Pabpa |
