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Nitroethane synthesis trouble
[rquote=705895&tid=159797&author=zed]An Alanine oxidation process producing 3-Nitropropionic ...
10-3-2026 at 07:42
by: Sir_Gawain
Nitroethane synthesis trouble
I thought of trying the alanine oxidation process, but quickly realized that was not a good idea. Th ...
6-3-2026 at 19:52
by: Sir_Gawain
Nickel aminoguanidine diperchlorate
Very interesting! I had also noticed that there seemed to be some nickel left in solution, it’s ve ...
27-12-2025 at 13:25
by: Sir_Gawain
Preparation of perchloric acid
A mixture of hydrochloric and nitric acid can completely oxidize the ammonium ion. You simply dissol ...
26-12-2025 at 08:22
by: Sir_Gawain
how effective is a Vigreaux column ?
How do you calculate “theoretical plates” and what exactly does it represent? I’ve never gotte ...
14-12-2025 at 07:52
by: Sir_Gawain
Nickel aminoguanidine diperchlorate
Axt, I tried that method you posted with some changes and it works phenomenally. Procedure was as fo ...
13-12-2025 at 14:57
by: Sir_Gawain
Large List of Chemicals for Sale (Shipping Available)
Sent you an email
11-12-2025 at 18:13
by: Sir_Gawain
Slayer exciter circuit help
Check your secondary feedback connection

[Edited on 12-2-2025 by Sir_Gawain]
2-12-2025 at 14:08
by: Sir_Gawain
Secret Santa 2025
I just received a box of random bottles and stuff, thanks Dr. Bob!
25-11-2025 at 18:06
by: Sir_Gawain
Secret Santa 2025
Just signed up yesterday. Second year doing it, had a lot of fun the first time

Thanks for settin ...
31-10-2025 at 19:55
by: Sir_Gawain
Sodium percarbonate
Diethyl ether should work, but a solution of pure peroxide in diethyl ether sounds a little suicidal ...
28-10-2025 at 04:59
by: Sir_Gawain
Glacial Acetic Acid via Distillation
I’ve found that drying acetic acid in general is quite difficult, even at high concentrations. Rep ...
11-10-2025 at 12:21
by: Sir_Gawain
New Member
For the phosphor, some people have had success with the phosphor found inside fluorescent light bulb ...
25-9-2025 at 14:18
by: Sir_Gawain
benzyl alcohol + sulphuric acid = ?
I've ran into this exact phenomenon recently while trying to make benzyl acetate. Upon the addition ...
13-9-2025 at 14:29
by: Sir_Gawain
Pretty Pictures (2)
Hydrazine perchlorate

[file]106817[/file]
[file]106819[/file]
21-7-2025 at 23:13
by: Sir_Gawain
Recent ridiculously cheap Chinese glass acquisition
You can get synthware stuff for a very good price from [url=https://chengduglassware.com/product-cat ...
21-7-2025 at 23:11
by: Sir_Gawain
Recent ridiculously cheap Chinese glass acquisition
[rquote=701996&tid=161195&author=Radiums Lab]Any way it looks good but quality is "?".[/rquo ...
19-7-2025 at 21:15
by: Sir_Gawain
Synthesis of White fuming nitric acid via vacuum distillation
Make sure to use a very good trap or your pump will get absolutely destroyed
9-7-2025 at 21:14
by: Sir_Gawain
Why do most hobby chemists rely on YouTube ?
Because no other site has remotely as big of a user base.
24-6-2025 at 12:33
by: Sir_Gawain
DIY Spinthariscope
A thoriated welding electrode produces barely detectable amounts of radiation due to most of it bein ...
30-5-2025 at 20:01
by: Sir_Gawain
How to make white fuming nitric acid from red fuming for rdx synthesis
Did you rinse the HDN with a little ice cold acetone and dry thoroughly on the pump?
28-5-2025 at 15:32
by: Sir_Gawain
How to make white fuming nitric acid from red fuming for rdx synthesis
The hydrogen peroxide method works great for me, perhaps you added too much. For the RDX synthesis, ...
27-5-2025 at 13:38
by: Sir_Gawain
ETN-erythirthol tetranitrate good and bag yields
Since nitric acid is nearly always the most expensive and difficult to obtain, shouldn’t the yield ...
26-5-2025 at 21:00
by: Sir_Gawain
ETN-erythirthol tetranitrate good and bag yields
That’s interesting, I tried the dissolve-in-sulfuric-acid-first method and got an abysmal yield. P ...
26-5-2025 at 14:01
by: Sir_Gawain
Looking for Dichloromethane
It’s not just proportions, you also have to keep the temp really low or it will all boil away. You ...
23-5-2025 at 20:52
by: Sir_Gawain
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