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Steven's Rearrangement - Alternative strong bases to NaNH2
Thanks for the replies!
I bring news of success...
@karlos
I think potassium tert butoxide wa ... |
2-9-2020 at 16:14
by: SplendidAcylation |
Can you make methanol from formic acid?
[rquote=640426&tid=155776&author=Junk_Enginerd][rquote=640415&tid=155776&author=Alko ... |
11-7-2020 at 15:22
by: SplendidAcylation |
Thiamine catalyzed benzoin condensation failure
[rquote=640418&tid=155748&author=Tsjerk]Benzoic acid is not soluble in benzaldehyde, so it w ... |
11-7-2020 at 12:50
by: SplendidAcylation |
Thiamine catalyzed benzoin condensation failure
Thanks for the replies!
I have got it to work.
I left it overnight after the initial (failed) at ... |
11-7-2020 at 11:35
by: SplendidAcylation |
Thiamine catalyzed benzoin condensation failure
Hi,
Today I attempted the much awaited synthesis of benzoin... Well, it is much awaited by me, as ... |
7-7-2020 at 17:50
by: SplendidAcylation |
Benzoin condensation using hydrogen cyanide?
I'm sorry, I thought I had responded to all of the posts here 
@woelen, thanks for the advice, ... |
5-7-2020 at 17:24
by: SplendidAcylation |
Making sodium isopropoxide - Sodium is not dissolving
[rquote=639625&tid=155696&author=DraconicAcid][rquote=639624&tid=155696&author=Splen ... |
1-7-2020 at 17:47
by: SplendidAcylation |
Making sodium isopropoxide - Sodium is not dissolving
Thanks for the replies everyone!
[rquote=639583&tid=155696&author=woelen]With increasin ... |
1-7-2020 at 13:37
by: SplendidAcylation |
Making sodium isopropoxide - Sodium is not dissolving
Hi
I have recently acquired some sodium metal, with which I intend to make an anhydrous superbase ... |
30-6-2020 at 17:36
by: SplendidAcylation |
Why is tin and HCl rxn so slow?
[rquote=639352&tid=155674&author=DraconicAcid][rquote=639350&tid=155674&author=Splen ... |
29-6-2020 at 17:06
by: SplendidAcylation |
Why is tin and HCl rxn so slow?
I did this reaction recently
It is indeed very slow, I reasoned that it is because of tin's posit ... |
27-6-2020 at 17:30
by: SplendidAcylation |
Steven's Rearrangement - Alternative strong bases to NaNH2
Hi
Having been scheming about the synthesis of N,N-dimethyl-1,2-diphenylethylamine for many month ... |
27-6-2020 at 10:28
by: SplendidAcylation |
Disappointing results with 3A molecular sieves
I tried the same thing with sieves bought from China
Something like:
Sieves were first weighe ... |
22-6-2020 at 09:47
by: SplendidAcylation |
Benzoin condensation using hydrogen cyanide?
[rquote=637385&tid=155502&author=DavidJR]Found online:
(From http://www.chem.latech.edu/ ... |
4-6-2020 at 18:02
by: SplendidAcylation |
Synthesis of benzonitrile by P2O5 dehydration of benzamide - another perplexing failure
[rquote=637368&tid=155509&author=clearly_not_atara]As P2O5 is hydrated, it converts to metap ... |
4-6-2020 at 17:57
by: SplendidAcylation |
ethyl formate - esterification by reactive distillation
Fantastic.
Thanks for taking the time to write this up.
I think I might give it a try, but I onl ... |
1-6-2020 at 18:01
by: SplendidAcylation |
Synthesis of benzonitrile by P2O5 dehydration of benzamide - another perplexing failure
Another addition to the fail collection!
A few months ago, I got quite excited when I found out t ... |
1-6-2020 at 17:47
by: SplendidAcylation |
Benzoin condensation using hydrogen cyanide?
Thanks for all the replies.
Looks like thiamine is the way to go, although I'll probably end up t ... |
1-6-2020 at 17:10
by: SplendidAcylation |
Benzoin condensation using hydrogen cyanide?
Hi,
Sorry about the title, I tried 10 others but none were any better.
I am planning to make b ... |
31-5-2020 at 17:39
by: SplendidAcylation |
Problems with the synthesis of formaldehyde by pyrolysis of metal formates
[rquote=636639&tid=155405&author=Alkoholvergiftung]The patent says if you mix formiate with ... |
23-5-2020 at 09:04
by: SplendidAcylation |
Problems with the synthesis of formaldehyde by pyrolysis of metal formates
[rquote=636452&tid=155405&author=kmno4]Another paper about thermal decomposition of formates ... |
21-5-2020 at 16:38
by: SplendidAcylation |
Problems with the synthesis of formaldehyde by pyrolysis of metal formates
[rquote=636288&tid=155405&author=WGTR]"The result was a volume that corresponded almost exac ... |
19-5-2020 at 04:54
by: SplendidAcylation |
Problems with the synthesis of formaldehyde by pyrolysis of metal formates
[rquote=636223&tid=155405&author=WGTR]I don’t know German to translate, sorry.
Have fun ... |
17-5-2020 at 05:08
by: SplendidAcylation |
Problems with the synthesis of formaldehyde by pyrolysis of metal formates
Hi,
I have been attempting to make a solution of formaldehyde, by passing the gases produced by ... |
16-5-2020 at 11:45
by: SplendidAcylation |
How do you draw benzene rings?
I draw it so that it is sitting on a flat side rather than on a single CH group.
I usually draw a ... |
28-10-2018 at 08:58
by: SplendidAcylation |
