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Vacuum desiccator implosion risk (and how much vacuum is a Buchner funnel designed for?)
[rquote=675455&tid=158779&author=Deathunter88]You're fine and overthinking it, its not going ...
31-7-2022 at 02:04
by: SplendidAcylation
Vacuum desiccator implosion risk (and how much vacuum is a Buchner funnel designed for?)
Hi,

I have a rather large, glass vacuum desiccator;
I'm not sure the exact size as it is stored ...
29-7-2022 at 02:12
by: SplendidAcylation
Isopropyl nitrite to sodium nitrite
[rquote=675295&tid=158648&author=Lion850]@Myc I am in QLD. “stump remover” which is KNO3 ...
24-7-2022 at 03:19
by: SplendidAcylation
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
[rquote=675264&tid=158709&author=Fulmen]Funny coincidence: I'm working with magnesium nitrat ...
23-7-2022 at 03:21
by: SplendidAcylation
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
Update:

I finally managed to dry the salt, I think, fully, however it refuses to crystallize.
A ...
22-7-2022 at 02:28
by: SplendidAcylation
Conversion of Manganese Sulphate to Acetate
[rquote=675216&tid=158759&author=j_sum1][rquote=675214&tid=158759&author=SplendidAcy ...
20-7-2022 at 02:05
by: SplendidAcylation
Conversion of Manganese Sulphate to Acetate
I feel like a bit of an idiot here, but can someone explain how this reaction is even possible?

T ...
19-7-2022 at 14:07
by: SplendidAcylation
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
Update:

I tried distilling off isopropanol, but that didn't seem to work, I would have tried etha ...
16-7-2022 at 02:29
by: SplendidAcylation
Why is the wiki not properly displayed ?
[rquote=674896&tid=158017&author=Texium]Seems to be a problem with https. Both on my laptop ...
13-7-2022 at 02:13
by: SplendidAcylation
Confusion regarding the phosphoric acid reaction
As far as I know, the first reaction is a displacement reaction, more precisely it is an acid-base r ...
11-7-2022 at 03:41
by: SplendidAcylation
Why is the wiki not properly displayed ?
I'm not using Tor, and it looks like this to me too, sometimes it looks right, but it seems to be ra ...
6-7-2022 at 01:56
by: SplendidAcylation
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
Alrighty, I will try this!

There appears to be some oily organic compound in the salt as well, so ...
3-7-2022 at 01:57
by: SplendidAcylation
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
Thanks, everyone!

I eventually managed to get the flasks vacuum-tight but even at 76mmHg and heat ...
2-7-2022 at 02:05
by: SplendidAcylation
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
[rquote=674708&tid=158709&author=clearly_not_atara][quote]such as isopropanol[/quote]
I don ...
1-7-2022 at 02:14
by: SplendidAcylation
Drying an impossibly deliquescent iminium salt (how stable are iminium salts?)
Hi,

I have recently attempted to prepare Böhme's salt, which is N,N-dimethylaminomethyleneiminiu ...
29-6-2022 at 02:19
by: SplendidAcylation
Drying acyl halides with molecular sieves?
Thanks for the responses.

[rquote=674600&tid=158699&author=UC235]There is no way there wo ...
26-6-2022 at 02:08
by: SplendidAcylation
Drying acyl halides with molecular sieves?
[rquote=674594&tid=158699&author=PirateDocBrown]Sieves do not like acids. If you have some h ...
25-6-2022 at 02:16
by: SplendidAcylation
Drying acyl halides with molecular sieves?
Hi,

Having recently prepared benzoyl chloride by the chlorination of benzaldehyde, I was about to ...
24-6-2022 at 14:20
by: SplendidAcylation
Antimony Sulfide
[rquote=673934&tid=15349&author=clearly_not_atara]I honestly cannot think of a single reacti ...
2-6-2022 at 03:07
by: SplendidAcylation
Replacement for Chloroform?
@DocX I doubt OP would be interested in DCM since it too is a halogenated solvent, although it is a ...
25-5-2022 at 02:33
by: SplendidAcylation
Replacement for Chloroform?
[rquote=673676&tid=158603&author=clearly_not_atara][quote]I can't imagine chlorobenzene bein ...
21-5-2022 at 02:14
by: SplendidAcylation
Replacement for Chloroform?
Any particular reason for avoiding chloroform?
My daily glass of chloroform doesn't seem to have do ...
20-5-2022 at 03:17
by: SplendidAcylation
What to do with styrene?
[rquote=673388&tid=158580&author=Antiswat]iirc you can turn styrene oxide - or just styrene ...
11-5-2022 at 06:36
by: SplendidAcylation
Some practical questions about Grignard reactions
[rquote=673316&tid=158575&author=zed]To my recollection, this type synthesis calls for an ad ...
8-5-2022 at 02:28
by: SplendidAcylation
What to do with styrene?
I too have been interested in the potential fun projects involving styrene.

You could convert it ...
7-5-2022 at 05:23
by: SplendidAcylation
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