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Azides
For the chemistry I am lover and fucker and from this position I feel me not competent,despite of 13 ...
19-1-2017 at 22:25
by: Thraxx
Azides
Well,but what could be the strange liquid?Hydrazine is reducing. agent.Alcohol is not possible to be ...
18-1-2017 at 13:00
by: Thraxx
Azides
About the IP extract + IP nitrit method.
Schema of reaction:
HS Extract (3 times) + NaOH + IP nitr ...
17-1-2017 at 02:37
by: Thraxx
Semicarbazide ?
I decided me to do semikarbazide and from it make the sodium azide.This method I found elsewhere her ...
14-1-2017 at 07:45
by: Thraxx
Azides


@Thraxx,
"You didn't gave an answer about the purity of your reactants.
Commercial aceton, NaO ...
13-1-2017 at 07:06
by: Thraxx
Azides
[rquote=471760&tid=1987&author=Theoretic]Philou: could this be oxidation of isopropyl nitrit ...
12-1-2017 at 22:08
by: Thraxx
Azides

"Are you sure you are not trying to fool us with a picture of TNT trial from toluen and medium con ...
12-1-2017 at 14:05
by: Thraxx
Azides
I would like to ask you,what could be the substance on the picture below.
This is product of my twe ...
12-1-2017 at 08:09
by: Thraxx
Azides

To the NCl 3 method-
Hentschel (,Ber.1897,30,1434,1792) wrote,that NH4Cl react with sodium hypoch ...
12-1-2017 at 00:32
by: Thraxx
Azides
I would like to tell you,that after 12 experiments with IP extract + IPnitrite + hydroxide was my yi ...
10-1-2017 at 05:17
by: Thraxx
Azides
Thank you for advice about the Na2SO4 and NaHSO4.If there is only Na2SO4,then it could be separate f ...
6-1-2017 at 02:56
by: Thraxx
Azides
What you think about this method ? :

1.-Hydrazine Sulphate + Ba/NO3/2 == Filtration==
2. Hydrazi ...
5-1-2017 at 12:49
by: Thraxx
Azides
Important is,that with the technical ethanol I had yield zero-nothing.the layer on the bottom was br ...
18-12-2016 at 11:27
by: Thraxx
Azides
I am careful and timid.These experiments I did on balkony in military gasmask and many pairs of glov ...
15-12-2016 at 23:08
by: Thraxx
Azides
My azide synthesis experiments:
Exp.Nr.1Azide Na synt.
- Bottle One :
Hydraz ...
15-12-2016 at 09:03
by: Thraxx
RDX synthesis
[rquote=468853&tid=250&author=Microtek]
[quote]
Therefore if we use the HDN instead of Hex ...
14-12-2016 at 09:41
by: Thraxx
Ancient metallurgy
The Wootz is iron with Vanad carbid,in 19 century in London expo was one Russian with wootz,after wa ...
11-12-2016 at 11:32
by: Thraxx
Silver azide synthesis question?
[rquote=468648&tid=28997&author=Etanol][rquote=468497&tid=28997&author=Thraxx]To Sil ...
10-12-2016 at 08:40
by: Thraxx
Silver azide synthesis question?
To Silver Azide:

[i]I worked in acording to Hodgkinson patent from y. 1918(which was outgoing fro ...
8-12-2016 at 11:35
by: Thraxx
Short question / quick answer - Thread
Thank you,I was frightened,that in my bottle is born some dangerous something like Potassium or Mang ...
8-12-2016 at 08:49
by: Thraxx
Short question / quick answer - Thread
Please,I have a problem and I would like to please you for advice.
I did the hydrazinsulfate like h ...
8-12-2016 at 06:35
by: Thraxx
Silver azide synthesis question?
[rquote=468463&tid=28997&author=Bert]Mix Mercury fulminate with Lead azide, then you can't u ...
8-12-2016 at 02:03
by: Thraxx
Silver azide synthesis question?
Blechtas idea was to mix into the reaction beaker with silver azid synthesis crystals of aromatic ...
7-12-2016 at 22:28
by: Thraxx
Silver azide synthesis question?
Today I did this reaction:
Into 1000 ml bottle I did 500 ml of 4,7% NaClO and in to ice bath I adde ...
7-12-2016 at 11:31
by: Thraxx
help make white fuming nitric acid.
[rquote=468007&tid=13749&author=Microtek]
I have experimentet with boiling down dilute sulf ...
2-12-2016 at 04:45
by: Thraxx
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