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Decentralized Computing Power for Accessible Computational Resources
I managed to get mine to work after that, but it was still pretty long calculation. I'll pretty much ...
21-12-2022 at 23:06
by: Triflic Acid
Can DCM act as a Lewis Acid?
Try a bicarb wash of the DCM layer after the water quench, it would get rid of any of the HCl that D ...
21-12-2022 at 18:35
by: Triflic Acid
Decentralized Computing Power for Accessible Computational Resources
Hello again,

It's been a while since my last post, still alive; just busy. I now work in a univer ...
21-12-2022 at 18:31
by: Triflic Acid
Benzene to benzaldehyde conversion
If it were really that bad it would be banned. I'm not saying it's safe, but it's not the liquid cya ...
12-7-2022 at 20:30
by: Triflic Acid
[Cr(en)3]Cl3 3H2O IR spectra
First, why is this in pre-pub? Second, don't come here looking for people to just hand you some spec ...
5-7-2022 at 08:40
by: Triflic Acid
making H2SO4?
Distill battery acid, is much better than killing everyone around you with a fume of H2SO4 from an S ...
4-7-2022 at 10:19
by: Triflic Acid
Orthosilicate esters from silica gel
I'm going to try this. Funny how some of my old threads are getting bumped up lol. I never really co ...
23-6-2022 at 20:33
by: Triflic Acid
Electrolytic reduction of pyridine to piperidine
Super interesting. I've always wanted to try electrochemical reductions for organics, rather than ha ...
21-6-2022 at 10:42
by: Triflic Acid
Kid wants to do an experiment
Actually, now that everyone mentions it, someone under 12 could probably do it too. I too was 10 whe ...
15-6-2022 at 20:39
by: Triflic Acid
Safely conducting an Alkali Fusion
I'll do the neutralization, that's a stupidly simple idea that I'm disappointed I didn't think of do ...
10-6-2022 at 19:56
by: Triflic Acid
Anyone got an Buchi R-200 rotovap steam adapter?
Bump
10-6-2022 at 10:53
by: Triflic Acid
OTC Vanilin
I would doubt it works for normal toluene, but it probably would work for nitrotoluenes, since those ...
10-6-2022 at 09:40
by: Triflic Acid
Safely conducting an Alkali Fusion
I do, that's how I made the TsOH. I also have a dean stark trap, so that shouldn't be too hard. But ...
10-6-2022 at 09:35
by: Triflic Acid
Safely conducting an Alkali Fusion
As part of my vanillin synthesis, I plan to do alkali fusion of my p-TsOH to get p-cresol. Was wonde ...
9-6-2022 at 23:18
by: Triflic Acid
Kid wants to do an experiment
This could end very badly or be absolutely fine. It depends on the scale you chose to do this one. I ...
9-6-2022 at 23:13
by: Triflic Acid
Anyone got an Buchi R-200 rotovap steam adapter?
The title says it all. Mines broke, and I’ve been unable to find a part that works. Only parts wit ...
6-6-2022 at 23:11
by: Triflic Acid
OTC Vanilin
Interesting. I'm gonna try out the whole alkali fusion step soon. I will report on how that goes. Ma ...
3-6-2022 at 21:36
by: Triflic Acid
Cyclopentadiene
Interesting. Just came across this randomly. I gave up on the project and moved on, but I might just ...
3-6-2022 at 21:25
by: Triflic Acid
OTC Vanilin
I've been pretty bored lately, so I decided to take on a larger project. I'm gonna try to produce va ...
2-6-2022 at 11:02
by: Triflic Acid
mechanism of sodium dithionite aromatic nitro reduction?
https://www.google.com/url?sa=i&url=https%3A%2F%2Fchemistry-europe.onlinelibrary.wiley.com%2Fdoi ...
2-6-2022 at 08:34
by: Triflic Acid
Preparation of Succinic Acid
Just read over this, and would like to issue a warning to all SM members. DO NOT BUY Pd/C FROM CHEMC ...
1-6-2022 at 20:32
by: Triflic Acid
Looking for Heidolph rotovap G6 glass set adapter
Hi Dr. Bob,

I had a similar thing I sent in a U2U to you. Please let me know if you received it.
12-5-2022 at 19:03
by: Triflic Acid
Cleaning Nitric Acid Stains from Skin
Honestly, it doesn't hurt and doesn't have any negative health effects, so I don't see why you would ...
5-5-2022 at 10:55
by: Triflic Acid
Reduction of 4-Chloro-3-nitrotoluene failure
Using Mg metal in methanol has worked well for me in the past, when I was making dizaotoluene, from ...
3-5-2022 at 06:28
by: Triflic Acid
Catalyst for Amide hydrolysis
I’m actually trying to produce vanillin from capsaicin. So that doesn’t work for me sadly.
1-5-2022 at 12:06
by: Triflic Acid
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