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Could someone make conclusions of what has been done yet? ie some proven methods for preparation?
30-5-2005 at 09:55
by: Tweenk
Phosphorus Chlorides
The standard procedure to make PCl3 is reacting chlorine gas with P, at first leting in the chlorine ...
30-5-2005 at 09:23
by: Tweenk
To everyone using peroxides (important!)
After seeing dozens of reports of organic peroxides accidentally exploding while being loaded into m ...
4-1-2005 at 12:53
by: Tweenk
Not emulsion...
Have anybody read about two-phase systems? Those are systems of two partially miscible liquids. For ...
1-1-2005 at 06:01
by: Tweenk
Diphoronepentaperoxide (DPPP)
To make something clear: I do not doubt if it has formed, but how has it formed :) It's very st ...
30-12-2004 at 11:56
by: Tweenk
Diphoronepentaperoxide (DPPP)
Chloroacetone is made by bubbling Cl2 gas through a solution of acetone in HCl, the process is not s ...
30-12-2004 at 11:10
by: Tweenk
The most efficient method to prepare Hydrazine Nitrate
[quote][i]Originally posted by neutrino[/i]
Molten AN would be suicide[/quote]

Molten AN doesn&# ...
30-12-2004 at 09:42
by: Tweenk
Diphoronpentaperoxyd & Chloroacetone
How do you heat acetone to 110*C when it boils at 56*C? Is it a gas phase reaction? :D
Still wonder ...
30-12-2004 at 09:27
by: Tweenk
The nichrome wire reacts with MEKP as metals reacts with all organic peroxides (decomposition over t ...
30-12-2004 at 09:23
by: Tweenk
Diphoronepentaperoxide (DPPP)
Well I'm wondering why this procedure works (or seems to work) when the reaction conditions are ...
30-12-2004 at 09:18
by: Tweenk
Diphoronepentaperoxide (DPPP)
The rxn proceeds not quite as stated on this site... IMO this sholud happen only in alkaline conditi ...
30-12-2004 at 08:28
by: Tweenk
AlCl3 experiments...
I think this is aluminium hydroxide. By dissolving a protective layer of Al2O3 (which always exists ...
7-12-2004 at 14:56
by: Tweenk
I think a better way would be to
1. chlorinate the toluene with uv irradiation (sunlight exposure), ...
7-12-2004 at 14:46
by: Tweenk
Friedel-Crafts Alkylation
Also, benzene acts as a solvent. The high excess needed can be rather easily separated after the rxn ...
7-12-2004 at 14:35
by: Tweenk
Tetrameric AP is better
[quote][i]Originally posted by trichomegrower[/i]
(..) I used 1 inch copper tubes. I seperated prob ...
7-12-2004 at 13:57
by: Tweenk

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