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Summary?
Could someone make conclusions of what has been done yet? ie some proven methods for preparation? |
30-5-2005 at 09:55
by: Tweenk |
Phosphorus Chlorides
The standard procedure to make PCl3 is reacting chlorine gas with P, at first leting in the chlorine ... |
30-5-2005 at 09:23
by: Tweenk |
To everyone using peroxides (important!)
After seeing dozens of reports of organic peroxides accidentally exploding while being loaded into m ... |
4-1-2005 at 12:53
by: Tweenk |
Not emulsion...
Have anybody read about two-phase systems? Those are systems of two partially miscible liquids. For ... |
1-1-2005 at 06:01
by: Tweenk |
Diphoronepentaperoxide (DPPP)
To make something clear: I do not doubt if it has formed, but how has it formed 
It's very st ... |
30-12-2004 at 11:56
by: Tweenk |
Diphoronepentaperoxide (DPPP)
Chloroacetone is made by bubbling Cl2 gas through a solution of acetone in HCl, the process is not s ... |
30-12-2004 at 11:10
by: Tweenk |
The most efficient method to prepare Hydrazine Nitrate
[quote][i]Originally posted by neutrino[/i]
Molten AN would be suicide[/quote]
Molten AN doesn&# ... |
30-12-2004 at 09:42
by: Tweenk |
Diphoronpentaperoxyd & Chloroacetone
How do you heat acetone to 110*C when it boils at 56*C? Is it a gas phase reaction? 
Still wonder ... |
30-12-2004 at 09:27
by: Tweenk |
Wires
The nichrome wire reacts with MEKP as metals reacts with all organic peroxides (decomposition over t ... |
30-12-2004 at 09:23
by: Tweenk |
Diphoronepentaperoxide (DPPP)
Well I'm wondering why this procedure works (or seems to work) when the reaction conditions are ... |
30-12-2004 at 09:18
by: Tweenk |
Diphoronepentaperoxide (DPPP)
The rxn proceeds not quite as stated on this site... IMO this sholud happen only in alkaline conditi ... |
30-12-2004 at 08:28
by: Tweenk |
AlCl3 experiments...
I think this is aluminium hydroxide. By dissolving a protective layer of Al2O3 (which always exists ... |
7-12-2004 at 14:56
by: Tweenk |
Workaround
I think a better way would be to
1. chlorinate the toluene with uv irradiation (sunlight exposure), ... |
7-12-2004 at 14:46
by: Tweenk |
Friedel-Crafts Alkylation
Also, benzene acts as a solvent. The high excess needed can be rather easily separated after the rxn ... |
7-12-2004 at 14:35
by: Tweenk |
Tetrameric AP is better
[quote][i]Originally posted by trichomegrower[/i]
(..) I used 1 inch copper tubes. I seperated prob ... |
7-12-2004 at 13:57
by: Tweenk |
