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Setting up a burner
Sorry for bringing up an old thread.

I have a teclu burner, which I belive is designed to work on ...
22-4-2011 at 07:01
by: Zinc
Hydrazine
[rquote=204312&tid=1128&author=NurdRage]thats actually really good considering low concentra ...
15-3-2011 at 08:05
by: Zinc
Hydrazine
Actualy I failed in my calculations, I calculated how much pure hydrazine should I get, not how much ...
15-3-2011 at 06:23
by: Zinc
Hydrazine
Fail, if I calculated it correctly that would be cca. 160% yield (based on NaOCl), impossible.
I am ...
14-3-2011 at 15:55
by: Zinc
Hydrazine
Yesterday I weighed the hydrazine sulphate, and there is 18 g, much more than expected :D It seems t ...
14-3-2011 at 06:15
by: Zinc
Hydrazine
I tested the mixture of batches, and indeed there was ketazine in it. I devided it into three portio ...
11-3-2011 at 07:55
by: Zinc
Hydrazine
Yesterday I made a batch with 17 ml of NH3, 7 ml of MEK and 26 g of NaOCl soln. and let it stay over ...
11-3-2011 at 03:43
by: Zinc
Hydrazine
The last time I waited around 1-1.5 h, the mix was clear, no turbidity like it would be expected fro ...
10-3-2011 at 10:40
by: Zinc
Hydrazine
I did antoher try, this time with 15 ml 25% NH3, 6 ml MEK and 24 ml NaOCl, and let the NH3 and MEK r ...
10-3-2011 at 09:12
by: Zinc
Hydrazine
Today I tried the procedure again but with much smaller quantities.

I used 30 ml of 25% NH3, 12 m ...
10-3-2011 at 03:00
by: Zinc
Hydrazine
Indeed I added the hypochlorite cca. 1-2 min after the MEK.

I have a question about stirring. Is ...
8-3-2011 at 15:13
by: Zinc
Hydrazine
Today I tried to make hydrazine sulfate following Nurdrages ketazine process.

The differences wer ...
8-3-2011 at 11:29
by: Zinc
KNO3,P, charcoal mixture
Be careful when using any mixture containing P, they tend do be very sensitive.
28-2-2011 at 05:04
by: Zinc
NO2 ventilation in HNO3 distillation
Today I tried to distill HNO3 from a distillation flask closed by a plastic cork (I don't know what ...
26-2-2011 at 10:45
by: Zinc
NO2 ventilation in HNO3 distillation
I will soon get a 250ml distillation flask, but it doesn't have a ground glass neck so I can't close ...
19-2-2011 at 06:21
by: Zinc
Pressed Cast Explosivies?
I belive that the ANNM is more "powerfull" than KNO3/NM as AN is itself an explosive, and all the de ...
2-2-2011 at 14:15
by: Zinc
Diving Into the World of Fulminates
Yesterday I made some Hg(ONC)2.

To cca. 6g of Hg i added 45ml of 60-70% nitric acid (which was ma ...
2-2-2011 at 06:10
by: Zinc
Diving Into the World of Fulminates
Sorry to bring up an old thread, but this one seemed the most suitable for the question that I have. ...
27-1-2011 at 11:17
by: Zinc
nitroglycerin
Yesterday I tried to set off a mix of 40g DNT, 30g NG and 5g paint-grade Al powder and cca. 1g of Na ...
24-1-2011 at 03:24
by: Zinc
nitroglycerin
Sorry for the double post, and if the question is too "practical".

I was thinking about trying NG ...
21-1-2011 at 11:04
by: Zinc
nitroglycerin
I washed the NG with an another portion of conc. NaCl soln. and transported it with a syringe into a ...
16-1-2011 at 12:05
by: Zinc
nitroglycerin
My NG has now been 4 days under the NaCl solution. Already after the first day it almost completely ...
16-1-2011 at 05:37
by: Zinc
nitroglycerin
[rquote=198254&tid=949&author=hissingnoise]
What lack of equipment could possibly prevent y ...
12-1-2011 at 08:36
by: Zinc
NG neutralization
I have noticed NG can be difficult to properly neutralize.

Two times have I put NG under a NaHCO ...
12-1-2011 at 05:47
by: Zinc
Trinitrotoluene preparation
Sorry to bring up an old thread, but I didn't want to start a new one.

I tried to make nitrotolue ...
28-12-2010 at 04:02
by: Zinc
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