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ethylate
There is a patent somewhere which suggests refluxing the mix under a column packed with CaO to remov ...
31-3-2009 at 22:24
by: ballzofsteel
BA + AA
For those benzal chloride buffs out thar.
Dont know if this is within the scope of this thread,but ...
28-7-2005 at 05:55
by: ballzofsteel
N2o
Is there any chance of producing sodium nitrite by venting nitrous oxide(N2O) into a concentrated so ...
27-4-2005 at 04:25
by: ballzofsteel
cleaning sulfuric acid
CAn anybody tell me what might be put in
Hardware store Sulfuric acid to act as a corrosion inhibi ...
6-4-2005 at 01:18
by: ballzofsteel
beanbags for fun
Cheers Guys.

Say I want a few kgs of styrene,can you imagine how tedious it would be to ,aquire,s ...
11-2-2005 at 20:35
by: ballzofsteel
Wrong again?
Hold your horses thar big fella!

Now,Im quite accustomed to being not 100% right all the time(wel ...
11-2-2005 at 19:25
by: ballzofsteel
Styrene from resin
I know this is a realy slack-ass question.

Can anyone suggest a way to isolate the styrene in a f ...
11-2-2005 at 19:08
by: ballzofsteel
Realy?
No,I dont think so.

But that sound a hell of a lot better if it can be done!
Do you have a link ...
11-2-2005 at 16:39
by: ballzofsteel
sorry
No, no personal experience with producing acetic acid this way.
I think I remember reading it somew ...
11-2-2005 at 15:10
by: ballzofsteel
aa
Hows about dry distillation of an acetate salt with sodium bisulfate.
Has this been mentioned?
11-2-2005 at 03:07
by: ballzofsteel
Improvised Hotplate
Halogen light bulbs and dimmer switch make good heat sources.
21-1-2005 at 18:04
by: ballzofsteel
persulfate
Just breezing through so excuse me if this has been posted already.(likely)

Patent GB190317982

...
20-1-2005 at 22:52
by: ballzofsteel
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
Yes you are right.

So sorry,Wasnt thinking right.

I made a mistake when writting that post,thi ...
23-12-2004 at 14:00
by: ballzofsteel
Yellow
Tried today with Tcca.

Added a couple of kilo ice to 1l toluene
and roughly 500gm TCCA.
Stirred ...
23-12-2004 at 05:13
by: ballzofsteel
aromatic sidechainchlorinations - Toluene - Benzylchloride, Benzalchloride, Benzotrichloride and followup reactions yielding Ben
Great work:D

Use Ice instead of water,in an insulated container
This seemed to help yeilds a lit ...
21-12-2004 at 15:12
by: ballzofsteel
Cold , Wet Sidechain chlorination
This is the simplest route to benzyl chloride Ive found so-far.


PATENT NO.GB134250

Abstract: ...
7-12-2004 at 06:09
by: ballzofsteel
Reductive amination and water
Thanks Mendeleev .The Leukart-Wallach then:D
4-12-2004 at 17:26
by: ballzofsteel
formic %
I know I should know...but my memory fails me.

Is 70+-% formic acid, like the homemade stuff, use ...
4-12-2004 at 07:49
by: ballzofsteel
Reductive amination and water
Hi Org,

Cherry baby mentions a monomode microwave reactor in the post on Rhodiums.Did you modify ...
3-12-2004 at 02:47
by: ballzofsteel
Castner
This is a patent from Castner.
He uses tar as the carbon source,mixed with iron oxide,which is then ...
29-6-2004 at 21:23
by: ballzofsteel
sulfuric
Alternatively,you could mix salt with your TCCA and drip sulfuric onto it.
Wouldnt this eliminate t ...
29-6-2004 at 18:08
by: ballzofsteel
sulfuric
Alternatively,you could mix salt with your TCCA and drip sulfuric onto it.
Wouldnt this eliminate t ...
29-6-2004 at 18:05
by: ballzofsteel
Chlorine
Why not just drip conc Hcl onto your TCCA?
28-6-2004 at 21:38
by: ballzofsteel
hydroxyphenylacetone - a biosynthesis
Edited out of respect

[Edited on 1-5-2004 by ballzofsteel]
29-4-2004 at 23:11
by: ballzofsteel
Nitrate patent
Hey Bromic,

Did you take a look at the patent I posted
further on up the thread regarding reduc ...
28-4-2004 at 20:47
by: ballzofsteel
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