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Toluene > benzyl chloride
I found one method which uses toluene and hypochlorite, but I found no user references whatsoever.
...
25-1-2013 at 22:10
by: chucknorris
Vinegar purification
I vaporized some vinegar and found out it contains 0.5-2% of impurities that will leave brown-blacki ...
25-1-2013 at 22:08
by: chucknorris
Aluminum BBs Vs. Lab Armor
How about steel grains? I found a bag of 0.2-0.4mm sized stuff. I also found 0.5-1mm sized, which on ...
21-12-2012 at 20:30
by: chucknorris
Liquid choice for 200C in closed system?
Well, the mantle volume is over 200 liters and it should run for thousands of hours non-stop, so sil ...
21-12-2012 at 20:25
by: chucknorris
Liquid choice for 200C in closed system?
A liquid that stays liquid at 200C and is not inherently expensive or toxic would be needed for heat ...
20-12-2012 at 19:36
by: chucknorris
Unknown powder, lets find out what it is
Thanks for the tips! I'll take a look about those and see what I can find out. Not gonna be posting ...
19-12-2012 at 13:26
by: chucknorris
Unknown powder, lets find out what it is
I discovered this substance a year ago from my warehouse box, and there it was: about 200 grams of o ...
19-12-2012 at 11:55
by: chucknorris
Using table salt in heat bath?
I used DOT5.1 fluid, but it started smoking heavily at just only 120C. IDK if its shitty or somethin ...
18-12-2012 at 17:18
by: chucknorris
Using table salt in heat bath?
How about steel grains? I found a bag of 0.2-0.4mm sized stuff. I also found 0.5-1mm sized, which on ...
18-12-2012 at 15:26
by: chucknorris
Using table salt in heat bath?
The veg oil autoignition went actually pretty fast, I had the plate on for maybe 15-20 minutes, it s ...
18-12-2012 at 10:35
by: chucknorris
Using table salt in heat bath?
Ok thanks for giving me chance to pass that salt test. :P

Silicone oil is ok but the high price s ...
17-12-2012 at 21:09
by: chucknorris
Using table salt in heat bath?
I have tried couple of different options:

water - only good up to 100c
sand - damn good heat ins ...
17-12-2012 at 14:53
by: chucknorris
Chloroalkali process
Oh great thanks :)
16-12-2012 at 13:43
by: chucknorris
Propane + HNO3 400C + 10bar vapor phase?
Giving a thought for nitrating short chain paraffins, I was interested in the idea of making titaniu ...
16-12-2012 at 10:31
by: chucknorris
Generating HNO3 from NH4 in lab scale?
[quote]
In this process, anhydrous ammonia is oxidized to nitric oxide, in the presence of platinum ...
14-12-2012 at 00:47
by: chucknorris
Chloroalkali process
I suppose it looks like this:

http://upload.wikimedia.org/wikipedia/commons/thumb/1/1c/Hydrochlor ...
14-12-2012 at 00:35
by: chucknorris
Gas separation membrane (how-to-get-pure-N2)
By means of making ammonia from it and H2, I'll give it a thought, but just to say, anything in my c ...
13-12-2012 at 15:53
by: chucknorris
Gas separation membrane (how-to-get-pure-N2)
Are these gas separating membranes available for commercial sale or are they still at the prototype ...
13-12-2012 at 15:23
by: chucknorris
Chloroalkali process
Yep its quite exothermic, but I wouldn't say *explosive*. Steady flow of both gases into the reactor ...
13-12-2012 at 13:03
by: chucknorris
Ethyl/Isopropyl Bromide preparation
What happens to the sulfuric acid in this reaction? When my friend did this and he poured the leftov ...
13-12-2012 at 12:59
by: chucknorris
Chloroalkali process
Nope, my intention is to flow the Cl2 and H2 gases in common pipe and chamber to react them with UV ...
13-12-2012 at 12:30
by: chucknorris
Chloroalkali process
Could platinum coated materials be used as anode&cathode materials? Im looking for process that ...
13-12-2012 at 11:40
by: chucknorris
ClO2 uses?
Could ClO2 be used for anything useful in chemistry? For ex. creating chlorides, aldehydes, etc? One ...
13-12-2012 at 10:33
by: chucknorris
Chloroalkali process
What have I read about the chloroalkali process, one needs two electrodes and some sort of membrane ...
13-12-2012 at 08:17
by: chucknorris
cleaning sulfuric acid
Oh well.. Sulfuric acid boiling temp at 5 pascals(which is the max vac my pump will make) seems to b ...
10-12-2012 at 07:34
by: chucknorris
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