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What to do with 100 grams of lithium chloride
LiCl/dimethylacetamide is a popular system for dissolving cellulose. 		13-9-2024 at 07:03
by: clearly_not_atara
furfural
[rquote=653261&tid=15774&author=Boffis]
At present it still looks like d-ribose, available ...		 12-9-2024 at 18:59
by: clearly_not_atara
Facile synthesis of a sponge
(Do not rub on skin.)

Schwarz and Epple report that the simple heating of sodium chloroacetate re ...		 12-9-2024 at 11:37
by: clearly_not_atara
Increasing steam bath temperature with solutes
So it appears that you can get to around 150 C, although you may need to keep replenishing the water ...		 11-9-2024 at 10:46
by: clearly_not_atara
Increasing steam bath temperature with solutes
I'm not sure about this but I think that MgCl2/H2O will produce "relatively" stable liquids up to 20 ...		 10-9-2024 at 15:12
by: clearly_not_atara
Oxalic acid
[rquote=695136&tid=160539&author=Alkoholvergiftung]Alternative the Sodium salt was made when ...		 10-9-2024 at 13:15
by: clearly_not_atara
Tl properties
Most likely because it's univalent. Thallium (I) hydroxide is significantly more soluble in pure wat ...		 10-9-2024 at 11:56
by: clearly_not_atara
Tl properties
IIRC it has some similarities to silver: it forms insoluble +1 compounds with halides which are ligh ...		 10-9-2024 at 07:47
by: clearly_not_atara
Trimethylsulfonium bromide and its use for the methylation of phenols
https://onlinelibrary.wiley.com/doi/abs/10.1111/j.1748-1716.1943.tb02053.x

It will kill a rat, ap ...		 9-9-2024 at 11:34
by: clearly_not_atara
Potassium from K2CO3 + Mg lathings
Awesome find! 		6-9-2024 at 11:22
by: clearly_not_atara
Glyoxylic acid
Many threads on this forum over the years have discussed the preparation of glyoxylic acid. A sample ...		 6-9-2024 at 08:55
by: clearly_not_atara
Bromination of anilines
Using more solvent can be a way to avoid exothermic issues or side-reactions. In this case, the prop ...		 4-9-2024 at 11:16
by: clearly_not_atara
Bromination of anilines
Cu2+ is more strongly oxidizing in nitrile solvents versus other solvents due to complex formation. ...		 3-9-2024 at 09:50
by: clearly_not_atara
Reversing sulfate salts reaction
Sulfuric acid decomposes before it boils at atmospheric pressure. So this route is not possible. 		30-8-2024 at 19:39
by: clearly_not_atara
Demethylation of Eugenol
^well that's certainly something.

So many failures doing this rxn without nitrogen I have to won ...		 29-8-2024 at 16:52
by: clearly_not_atara
The First Room-Temperature Ambient-Pressure Superconductor
^My reaction was "whaaaaat?!" and then I looked it up:

[quote]We present here a reassessment of o ...		 29-8-2024 at 11:10
by: clearly_not_atara
What's the densest gas (or mix) you can create?
I trust you are reasonably prepared for the hazards associated with practically all heavy gases!

...		 28-8-2024 at 09:59
by: clearly_not_atara
Demethylation of Eugenol
You basically need an inert atmosphere to do this rxn. 		19-8-2024 at 09:18
by: clearly_not_atara
paradiclorobenzene - possible degradation of
If we are innovating the method, then there is always the possibility of something like sodium diiso ...		 13-8-2024 at 12:00
by: clearly_not_atara
paradiclorobenzene - possible degradation of
I guess I think it's moderately surprising that you're objecting to sodamide (which is pretty nasty) ...		 12-8-2024 at 18:11
by: clearly_not_atara
paradiclorobenzene - possible degradation of
According to Rao et al, rxn of paradichlorobenzene with NaNH2 in ammonia gives a 2:1 ratio of 4-chlo ...		 6-8-2024 at 12:57
by: clearly_not_atara
Preparation of pyroglutamic acid
Looks awesome!

I've read some papers that say silver pyroglutamate is soluble in hot water, so I' ...		 13-7-2024 at 09:49
by: clearly_not_atara
Silver anode for making sulfuric acid?
There seems to be some work about SnO2-coated titanium as an oxygen-evolution anode in sulfuric acid ...		 13-7-2024 at 09:41
by: clearly_not_atara
Notes on the new NurdRage video: making sulphuric acid from sulphates and oxalic acid
What was wrong with magnesium sulfate? Shouldn't that be massively cheaper than copper, and with no ...		 28-6-2024 at 06:29
by: clearly_not_atara
Isoamyl Acetate to Isoamyl alcohol
As with most alkyl acetates, fusion with NaOH ought to do it. 		19-6-2024 at 08:57
by: clearly_not_atara
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