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nitrate from cyanide?
Oxidation of urine has been practiced for centuries:

https://en.wikipedia.org/wiki/Potassium_nitr ...
28-3-2020 at 14:30
by: clearly_not_atara
N-nitroso-N-methyl-p-toluenesulphonamide
[i]"CH2N2 may explode in contact with sharp edges, such as ground-glass joints, even scratches in gl ...
28-3-2020 at 14:27
by: clearly_not_atara
Formamide from urea
The point is, in a system like Zn/HCl, there are two things that can be reduced:

2 H3O+ + Zn > ...
28-3-2020 at 08:16
by: clearly_not_atara
Al(O-i-Pr) decomposition problem
The limiting factor in the MPV reduction is usually aldol condensation. Ketones are usually resistan ...
28-3-2020 at 03:57
by: clearly_not_atara
Formamide from urea
The problem with basic reductions is that urea gets deprotonated and then it's hard to transfer elec ...
27-3-2020 at 15:50
by: clearly_not_atara
Problem in synthesising Nickel Sulfate
Wiki says the anhydrous salt is "yellow", but this may be a faint color in pure crystals that only b ...
26-3-2020 at 13:22
by: clearly_not_atara
Alternative to MeCN
Not using MeCN is [i]already[/i] a different route. Just use Klute's route, it makes more sense.

...
26-3-2020 at 11:30
by: clearly_not_atara
Sodium permanganate
UTFSE

https://www.sciencemadness.org/whisper/viewthread.php?tid=8480&page=16#pid459691

Sod ...
26-3-2020 at 10:41
by: clearly_not_atara
azelaic + pelargonic acids from oleic acid, C=C double bound cleavage using H2O2 as oxidizer, H2WO4 catalyst
[applause]

I think your prep of the peroxotungstic acid catalyst is very clever. When I posted ab ...
26-3-2020 at 10:27
by: clearly_not_atara
Alternative to MeCN
http://www.sciencemadness.org/talk/viewthread.php?tid=10124
26-3-2020 at 09:59
by: clearly_not_atara
Sodium permanganate
You are trying to make permanganate. The correct way is to use potassium manganate. You are resistin ...
25-3-2020 at 11:50
by: clearly_not_atara
Q: Making sodium cyanide from sodium cyanate and sodium metal
[quote] reacting the mix with ammonium carbonate will give mix of NaCN and NaHCO3 (Na2CO3+(NH4)2CO3 ...
25-3-2020 at 08:56
by: clearly_not_atara
Sodium permanganate
Oh no, is this another "I'd rather fuck around in the lab for three years rather than spend an hour ...
25-3-2020 at 08:38
by: clearly_not_atara
Better synthesis route to Favipiravir anyone?
So I thought a bit more about the route I posted.

Unfortunately, glyoxylamide is not commercially ...
24-3-2020 at 17:32
by: clearly_not_atara
Trouble with synthesizing HClO4
I would say yes, just make sure to be careful of possible carbon monoxide evolution during the disti ...
23-3-2020 at 17:38
by: clearly_not_atara
DIY C-virus masks. No politics, science only so we don't lose the thread again
tl;dr: soak polypropylene microfiber cloth in salt water and let dry. Should work with polyester. Wi ...
23-3-2020 at 06:31
by: clearly_not_atara
does fresh milk enzyme able to break down capsaicinoids from chili peppers?
The phrase "detergent effect" should give you all the information you need. Would be interesting to ...
23-3-2020 at 05:31
by: clearly_not_atara
Trouble with synthesizing HClO4
In distilling an aqueous mixture of oxalic acid and perchloric acid, one should take care to avoid i ...
22-3-2020 at 14:04
by: clearly_not_atara
Trouble with synthesizing HClO4
[b]unionised:[/b] Solubility product of MgC2O4 is 1.14 * 10^(-5). From Wiki, we have a solubility of ...
22-3-2020 at 12:07
by: clearly_not_atara
Trouble with synthesizing HClO4
Assuming you still have magnesium perchlorate, you could try adding oxalic acid and filtering.

B ...
21-3-2020 at 14:24
by: clearly_not_atara
Vanillin demethylation via aluminum tribromide -- still confused.
The literature is not wrong, but nobody bothers making acetonitrile and pyridine for this rxn. I'd i ...
21-3-2020 at 09:39
by: clearly_not_atara
A theoretical total synthesis of chloroquine I thought up this afternoon
The problem with chloroquine as an antiviral therapy is that it tends to inhibit the host immune sys ...
20-3-2020 at 18:35
by: clearly_not_atara
Better synthesis route to Favipiravir anyone?
CuReUS: elemental fluorine seems a bit bold for a substrate bearing an aldehyde. Likewise for a subs ...
20-3-2020 at 16:58
by: clearly_not_atara
Low denisty organic fluids for making immiscible bi-layers.
[quote] Cymenes are very similar to D-limonine, correct?[/quote]

Both cymene and limonene are mon ...
20-3-2020 at 08:19
by: clearly_not_atara
Stevens rearrangement
Yes, it must be fully substituted. Also, generally only benzyl or allyl groups migrate for some uncl ...
19-3-2020 at 12:22
by: clearly_not_atara
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