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Non reactive Solvent for potassium permanganate
If you can buy ethyl acetate, it should be pretty easy to make acetonitrile, if slow -- just stir wi ...
3-12-2020 at 13:40
by: clearly_not_atara
Non reactive Solvent for potassium permanganate
The one paper I have read using this technique uses methylene chloride. This seems like an excellent ...
3-12-2020 at 12:40
by: clearly_not_atara
Mn2O7 to manganyl cation
https://www.sciencedirect.com/science/article/abs/pii/0022190261802029
3-12-2020 at 08:31
by: clearly_not_atara
Cheap radioisotope sources
If you want to order some thorium or depleted uranium so that you can observe their unusual and inte ...
3-12-2020 at 08:23
by: clearly_not_atara
CuS isn't actually copper(II) sulfide
Attempting to describe CuS as an ionic compound when Cu has electronegativity 1.9 and sulfur 2.6 doe ...
1-12-2020 at 08:14
by: clearly_not_atara
Nitration with NO2 instead of H2SO4?
NO2 is a nitrosating agent, not a nitrating agent. It generally reacts as NO+*NO3-. But because it's ...
30-11-2020 at 19:49
by: clearly_not_atara
Do not keep illegal drugs for personal use in your house, if you do chemistry as a hobby
Cannabis hasn't been illegal for me to possess since 2014. I actually forget to think about it as il ...
27-11-2020 at 14:39
by: clearly_not_atara
Seperation of potassium chlorate and perchlorate from perchlorate cell
If ammonium bitartrate is available, this will take KClO4 directly to NH4ClO4 by salt metathesis. Th ...
27-11-2020 at 12:08
by: clearly_not_atara
Malic acid to malonic acid?
In principle, periodate/periodic acid will convert malic acid to formylacetic acid by cleavage of th ...
25-11-2020 at 06:45
by: clearly_not_atara
Preparation of Di-(4-chloro-2-nitrophenyl)-disulphide
Looks a bit like nutritional yeast. Nice work!
24-11-2020 at 07:57
by: clearly_not_atara
Otc oxalyl chloride success?
DMSO reacts with oxalyl chloride at ambient temperature, as karlos alluded. Not recommended.
20-11-2020 at 13:50
by: clearly_not_atara
Isocyanate synthesis via halide displacement
[rquote=649418&tid=156558&author=ArbuzToWoda]
Maybe, but why do we need to come up with alt ...
19-11-2020 at 12:19
by: clearly_not_atara
Ammonia by the haber process--tabletop chemistry
[rquote=649335&tid=13838&author=Fluorite]
https://m.youtube.com/watch?v=8LriocEzpC0 They tr ...
18-11-2020 at 10:21
by: clearly_not_atara
perchlorate without electricity
PbO2 <> Pb2+ SEP = +1.5 V, ClO4- <> ClO3- SEP = +1.2 V, so this reaction is at least not ...
16-11-2020 at 07:48
by: clearly_not_atara
Acid Chlorides
The best way I know to make alpha-halo ethers is to use the reaction of acetals with ZnCl2 and acety ...
16-11-2020 at 07:40
by: clearly_not_atara
Free radical bromination on only the terminal ends of hexane
[rquote=649166&tid=156532&author=Triflic Acid]@clearly_not_atara Is there any way to create ...
15-11-2020 at 19:30
by: clearly_not_atara
Acid Chlorides
You're confusing electrophilic chlorination with nucleophilic chlorination. C3N3Cl3 transfers Cl-. C ...
15-11-2020 at 19:12
by: clearly_not_atara
Free radical bromination on only the terminal ends of hexane
TA: if you brominate at random the chance of getting 1,6 is one in 15, a 6.7% yield before you even ...
15-11-2020 at 08:55
by: clearly_not_atara
Free radical bromination on only the terminal ends of hexane
Hm... Wurtz coupling of allyl bromide and anti-Markovnikov dihydrobromination of the 1,5-hexadiene w ...
14-11-2020 at 18:38
by: clearly_not_atara
Iodine did not precipitate from Potassium Iodide? (HCL+ H2O2)
Use H2SO4/H3PO4, since these do not form complexes with I+ or I3+ ions. It may be possible to recove ...
14-11-2020 at 13:35
by: clearly_not_atara
diethyl carbonate (NO PHOSGENE)
So I'm not sure if you're aware, but ethylene glycol and urea makes ethylene carbonate, not diethyl ...
11-11-2020 at 18:24
by: clearly_not_atara
Sodium benzoate -> Ferric benzoate (and similar rxns)
I thought it was the ferrous salts?

Anyway you could start from ferrous sulfate and calcium benzo ...
10-11-2020 at 15:14
by: clearly_not_atara
Straight-chain acyl chlorides from TCCA and aldehyde
It's highly unlikely. The same reaction is well-known for benzoyl and alpha-quaternary chlorides (th ...
9-11-2020 at 12:04
by: clearly_not_atara
Acetic anhydride preparation
[rquote=648344&tid=156476&author=Triflic Acid]So how do I convert benzyl-acetic anhydride to ...
6-11-2020 at 05:24
by: clearly_not_atara
Acetic anhydride preparation
You actually need to do the double dehydrohalogenation in two steps because otherwise you'll probabl ...
5-11-2020 at 14:35
by: clearly_not_atara
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