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TheVespiary.org .... Sedit or jon or java
[rquote=488850&tid=31027&author=scronaldo-totse][
I just want to have Max Gurgle-esque adve ...
26-7-2017 at 16:01
by: clearly_not_atara
TheVespiary.org .... Sedit or jon or java
SSL cert at thevespiary expired almost a week ago and now this... forum may have been taken over by ...
26-7-2017 at 15:18
by: clearly_not_atara
What is a good first project for someone with college-level chemistry knowledge, but no lab equipment?
Acetonitrile (if you can distill), because it opens doors to so much else, and starts just from ammo ...
26-7-2017 at 10:26
by: clearly_not_atara
Have any of the sciencemadness members discovered anything?
Tsath, I understand from previous conversations elsewhere that you've been having some "issues". Fir ...
25-7-2017 at 15:26
by: clearly_not_atara
Acetic anhydride preparation
That's a problem for sure.

Interesting. I think vacuum distillation is probably necessary as you ...
25-7-2017 at 10:46
by: clearly_not_atara
Have any of the sciencemadness members discovered anything?
Ullmann's methyl ethanesulfonate synthesis used two known reactions but put them together in a way t ...
23-7-2017 at 18:12
by: clearly_not_atara
Acetic anhydride preparation
Previous attempts at making acetic anhydride from copper acetate failed due to the difficulty of pre ...
23-7-2017 at 18:06
by: clearly_not_atara
Nitric Acid and Silver Nitrate
It turns out that silver [b]methanesulfonate[/b] is many times more soluble than the tosylate. This ...
23-7-2017 at 14:59
by: clearly_not_atara
Benzene synthesis
Benzophenone or triphenylmethanol are my first guesses.
22-7-2017 at 20:48
by: clearly_not_atara
Need an easy synthesis of Perchloric acid
[rquote=488255&tid=75570&author=Metacelsus]Distillation is the best way, especially because ...
21-7-2017 at 16:09
by: clearly_not_atara
Piperine extraction question
Aye, and if it crashed out it could form a cloudy suspension like you're seeing. It should be possib ...
20-7-2017 at 11:50
by: clearly_not_atara
Ultrahigh-purity CHBr3 preparation (interesting use, 1atm synthetic ultrananocrystalline hexagonal diamond
This actually sounds too good to be true. An ambient-pressure condensed-phase synthesis of DIAMOND?! ...
19-7-2017 at 22:15
by: clearly_not_atara
Acetaldehyde synthesis
This paper outlines the use of N-chlorosuccinimide for the selective oxidation of alkoxides:

htt ...
19-7-2017 at 13:49
by: clearly_not_atara
OTC Oxalyl Chloride Challenge
I suggest using iron phosphate with titanium metal since the corresponding phosphides are much less ...
13-7-2017 at 11:46
by: clearly_not_atara
OTC Oxalyl Chloride Challenge
I think sulfur tetrachloride with liquid chlorine is already easier than using hella-nasty and explo ...
12-7-2017 at 11:13
by: clearly_not_atara
Easy pyridine synth. found in a paper, does it work?
[quote]I ran across this article during my pyridine research:
https://en.wikipedia.org/wiki/M5_fibe ...
11-7-2017 at 19:02
by: clearly_not_atara
Easy pyridine synth. found in a paper, does it work?
The paper I linked has a free fulltext. The link is at the bottom of the page but it's kinda small:
...
11-7-2017 at 09:01
by: clearly_not_atara
OTC Oxalyl Chloride Challenge
I was thinking about other esters that could be converted to the chloride -- maybe try radical chlor ...
10-7-2017 at 18:49
by: clearly_not_atara
Easy pyridine synth. found in a paper, does it work?
https://www.jstage.jst.go.jp/article/bpb/26/8/26_8_1211/_article

Hiprex is hexamine hippurate
10-7-2017 at 18:42
by: clearly_not_atara
Easy pyridine synth. found in a paper, does it work?
A friend tells me you can make the Hanzsch ester from acetoacetate esters and hexamine. So that just ...
10-7-2017 at 13:48
by: clearly_not_atara
Where is Blogfast25 ?
[rquote=487401&tid=71575&author=JJay]That doesn't necessarily make it magically legal... in ...
10-7-2017 at 11:31
by: clearly_not_atara
Where is Blogfast25 ?
[quote] if you had something illegal in your lab (hypothetically, of course), wouldn't you know abou ...
9-7-2017 at 19:15
by: clearly_not_atara
Ammonium nitrate and zinc: Why so sensitive?
Zn2+ is a Lewis acid so maybe it pisses off the nitrate anion once even a tiny bit forms
9-7-2017 at 17:58
by: clearly_not_atara
Propylene carbonate Synthesis
You tossed the flask? Like across the room? Or it slipped out of your hands?

Anyway, sounds like ...
9-7-2017 at 11:29
by: clearly_not_atara
Detritus from Where is Blogfast25 ?
[rquote=487290&tid=71575&author=Rosco Bodine] It would be politically incorrect to simply st ...
8-7-2017 at 17:11
by: clearly_not_atara
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