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Dissolving titanium metal/dioxide
Practically all Ti3+ salts are soluble. Even TiPO4 is soluble IIRC. So any salt can be used, but it ...
21-2-2018 at 13:25
by: clearly_not_atara
Acid Chlorides
On the subject of benzotrichloride, benzoyl chlorides can be formed by chlorination of benzaldehydes ...
21-2-2018 at 13:11
by: clearly_not_atara
Acid Chlorides
The acetonitrile method deserves further consideration. A paper I dug up earlier shows that acetonit ...
21-2-2018 at 08:52
by: clearly_not_atara
Dissolving titanium metal/dioxide
No titanium (IV) binary salts can be obtained from aqueous solution. The lattice enthalpy of TiO2 is ...
21-2-2018 at 08:31
by: clearly_not_atara
Nitrogen Generator
Nitrogen is an active area of modern chemical research because it's incredibly difficult. You could ...
20-2-2018 at 20:39
by: clearly_not_atara
Catechol preparation
[quote]I would advise strongly against the Dakin reaction, the yields tend to suck balls[/quote] Whi ...
20-2-2018 at 08:51
by: clearly_not_atara
Al acetate from Al metal and acetic acid
Sometimes a salt loses the equivalent of acetic anhydride as a mixture of carbon dioxide and acetone ...
17-2-2018 at 19:15
by: clearly_not_atara
Al acetate from Al metal and acetic acid
Can you confirm the anhydride production? IIRC this was in an old reference but attempts to recreate ...
17-2-2018 at 17:53
by: clearly_not_atara
Reaction evolving H2 or CO gas, need help identifying
"The Removal of Carbon Monoxide from Air", Lamb, Bray & Frazer 1920.

https://pubs.acs.org/do ...
16-2-2018 at 12:20
by: clearly_not_atara
Processing BaSO4 to either carbonate or sulfide
To be clear: Wikipedia gives Ksp for [Ba2+][SO4(2-)] as 1.08 * 10^-10, and Ksp for [Ba2+][CO3(2-)] a ...
16-2-2018 at 11:37
by: clearly_not_atara
Processing BaSO4 to either carbonate or sulfide
It sounds like you're not familiar with the method, because your objections still don't make sense. ...
15-2-2018 at 12:49
by: clearly_not_atara
Processing BaSO4 to either carbonate or sulfide
RawWork: Barium carbonate is not soluble; the solution is simply filtered post-rxn. Not that it work ...
15-2-2018 at 08:14
by: clearly_not_atara
Aromatic aldehydes using Gattermann Koch Reaction
Is acetic formic anhydride applicable to aromatic substrates? This off-the-shelf reagent can perform ...
11-2-2018 at 13:02
by: clearly_not_atara
Removing alcohols from nonpolar solvents
Sulfuric acid may remove some non-alkane contaminants from gasoline but afaik it will not easily rea ...
8-2-2018 at 22:38
by: clearly_not_atara
Doable synthesis of F2 in amateur setting?
Found a ball-milling method. This one is also dependent on intercalation:

https://www.osapublishi ...
7-2-2018 at 14:14
by: clearly_not_atara
most appropriate material to topple tree
Put ropes on the tree, securely anchored, then cut the base. It can't fall down until you release th ...
5-2-2018 at 23:24
by: clearly_not_atara
Doable synthesis of F2 in amateur setting?
Sounds like the wrong salt though. We want K2MnF6 not K3MnF6.
5-2-2018 at 23:10
by: clearly_not_atara
Doable synthesis of F2 in amateur setting?
I found a paper in which a solution containing HF, KHF2 and KMnO4 forms K2MnF6 in the presence of Si ...
4-2-2018 at 11:35
by: clearly_not_atara
Doable synthesis of F2 in amateur setting?
I suggest performing the reaction in a xenon atmosphere with UV light. XeF2 is a solid which is much ...
3-2-2018 at 15:59
by: clearly_not_atara
Doable synthesis of F2 in amateur setting?
Doesn't the synthesis of F2 from fluoromanganates also depend on SbF5?

2 K2MnF6 + 4 SbF5 >> ...
3-2-2018 at 13:33
by: clearly_not_atara
Preparation of Succinic Acid
I was looking for old posts about something else, and I rediscovered the reaction of hydrochloric ac ...
2-2-2018 at 17:53
by: clearly_not_atara
1-Propanol from 2-Propanol
[rquote=505698&tid=80230&author=Texium (zts16)]
Edit: Sniped by CNA who clearly is more fam ...
2-2-2018 at 13:30
by: clearly_not_atara
1-Propanol from 2-Propanol
Basically it's impossible. The reaction JJay is thinking of is the addition of bromine radicals to a ...
2-2-2018 at 12:04
by: clearly_not_atara
Religion thought as science
[rquote=505540&tid=79610&author=DrP] Will you answer honestly and engage in reasonable discu ...
1-2-2018 at 13:12
by: clearly_not_atara
Everyday Chemistry
Everyone is familiar with grits right? If you're not, it's like the corn version of steelcut oats. A ...
1-2-2018 at 12:27
by: clearly_not_atara
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