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Acetic anhydride preparation
[rquote=698923&tid=9&author=hedgeberg]@greenlight try seeing if the distillate solidifies if ... |
8-2-2025 at 08:50
by: greenlight |
Acetic anhydride preparation
@hedgeberg, the end product did have a vinegary smell, you could be correct as it doesn't fume HCl a ... |
3-2-2025 at 09:53
by: greenlight |
Step 3: Benzyl alcohol route to acetic amhydride failure
Attempted to distill a mixture of the "benzoyl chloride?" produced in the previous step with anhydro ... |
19-1-2025 at 10:01
by: greenlight |
Original Destructions
Wow, is the back of the phone plastic or metal?
How thick is that metal shielding in the middle cir ... |
15-1-2025 at 09:16
by: greenlight |
Step 2: Benzyl alcohol route to acetic anhydride
Used the well written method from this thread to go from benzaldehyde to benzoyl chloride:
https:// ... |
15-1-2025 at 09:02
by: greenlight |
"Potassium pernitrate KNO4" at blast-tec.com, formerly pyrohub.com
[rquote=698138&tid=160748&author=Bedlasky]Apparantly it is gimmick to get around the restric ... |
5-1-2025 at 13:28
by: greenlight |
long-term storage of mercury fulminate
Was that the the primary reason for its discontinuation? Compromising the structural integrity of b ... |
4-1-2025 at 05:37
by: greenlight |
long-term storage of mercury fulminate
Mercury fulminate is not used in primers at all anymore as far as I know. Bullet primer composition ... |
2-1-2025 at 08:17
by: greenlight |
Substituting nitric acid with ammonium nitrate
I wrote that in a confusing way and missed out an important word.
139.67 grams ammonium nitrate a ... |
25-12-2024 at 10:00
by: greenlight |
Substituting nitric acid with ammonium nitrate
The reaction equation for the production of nitric acid from ammonium nitrate and 98% sulfuric acid ... |
23-12-2024 at 00:11
by: greenlight |
HMX via nitrolysis of DPT
To ensure accurate results, the nitrolysis was repeated a second time with phosphorus pentoxide to c ... |
21-12-2024 at 04:42
by: greenlight |
Is nuclear weapon miniaturisation driving institutional EM research?
Yes, the properties between CL-20 and RDX would only be apparent to someone working in the field com ... |
18-12-2024 at 19:21
by: greenlight |
Is nuclear weapon miniaturisation driving institutional EM research?
I believe there is a still large portion of EM research being dedicated to chemical explosives.
O ... |
18-12-2024 at 08:46
by: greenlight |
HMX via nitrolysis of DPT
Two nitrolysis reactions were run side by side with the DPT this time to examine whether the presenc ... |
17-12-2024 at 00:52
by: greenlight |
Step 1: Benzyl alcohol route to acetic amhydride
Okay, so far I have done the following:
Prepared a dilute aqueous solution of 78 ml of 70% nitric ... |
10-12-2024 at 22:12
by: greenlight |
Substituting nitric acid with ammonium nitrate
[rquote=697391&tid=160733&author=Sir_Gawain][rquote=697387&tid=160733&author=greenli ... |
7-12-2024 at 08:06
by: greenlight |
Substituting nitric acid with ammonium nitrate
I see @underminebrianeverglades beaten me to it and also been kind enough to crunch the numbers for ... |
6-12-2024 at 11:13
by: greenlight |
Substituting nitric acid with ammonium nitrate
The examples you listed are three different types of nitration:
RDX and HMX is N-nitration (NO2 b ... |
6-12-2024 at 11:10
by: greenlight |
HMX via nitrolysis of DPT
Final yield of DPT is 13.00 grams. It is an off-white light brown colour,.
A fresh batch of fuming ... |
2-12-2024 at 10:16
by: greenlight |
Short question / quick answer - Thread
[rquote=697150&tid=26572&author=dettoo456]Some here may still have access via university acc ... |
28-11-2024 at 18:34
by: greenlight |
Short question / quick answer - Thread
Just out of curiosity, has anyone here ever subscribed to the international journal of propellants, ... |
28-11-2024 at 04:19
by: greenlight |
Acetic anhydride preparation
Stepwise, yes the sulfur chloride route is less intricate.
I'm not sure how the yields or time woul ... |
27-11-2024 at 09:06
by: greenlight |
Acetic anhydride preparation
Is it viable to go from benzyl alcohol to benzaldehyde, then to benzoyl chloride, then reaction with ... |
26-11-2024 at 10:04
by: greenlight |
Unconventional Shaped Charges
[rquote=697043&tid=10575&author=Laboratory of Liptakov]Thanks, PLSHY . You use even dioctyls ... |
25-11-2024 at 09:47
by: greenlight |
Unconventional Shaped Charges
I will download it and translate and have a read of it  .
1.58 g/cm³ is great work. I could on ... |
25-11-2024 at 09:45
by: greenlight |
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