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Learning to respect NBS the hard way
Sauron: Yes, of course it was my fault. First and foremost because I did not take the necessary safe ... |
27-11-2007 at 02:44
by: jam640 |
Learning to respect NBS the hard way
I have attached the full article now.
And it actually gives a caution of the reaction between NIS a ... |
26-11-2007 at 05:37
by: jam640 |
Learning to respect NBS the hard way
Sorry Sauron, I didn't have SciFinder access when I looked it up earlier today so I just did hasty G ... |
26-11-2007 at 05:32
by: jam640 |
Learning to respect NBS the hard way
Sauron: No, it was not a direct scale-up of solvents but an apparently somewhat optimistic estimatio ... |
26-11-2007 at 04:45
by: jam640 |
Learning to respect NBS the hard way
Yes, I don't know. It just strikes me as very odd that the reaction had been going with slight heati ... |
26-11-2007 at 02:59
by: jam640 |
Learning to respect NBS the hard way
Yes, I agree with both.
Accidents and chemistry go hand in hand, although you should always take th ... |
26-11-2007 at 01:45
by: jam640 |
Learning to respect NBS the hard way
It was butyrophenone.
From an reference (I can look it up later) which said diethyl ether worked be ... |
25-11-2007 at 00:07
by: jam640 |
Learning to respect NBS the hard way
Thank you, I'm calmer now. 
I really appreciate your posts.
You just get so paranoid and panicy ... |
24-11-2007 at 13:41
by: jam640 |
Learning to respect NBS the hard way
I would really really appreciate an prompt reply if anyone has knowledge of the compound in question ... |
24-11-2007 at 13:11
by: jam640 |
Learning to respect NBS the hard way
I'm getting a bit paranoid about the health effects.
I inhaled some, of course.
It was butyropheno ... |
24-11-2007 at 12:09
by: jam640 |
Learning to respect NBS the hard way
The funny thing is that the reaction stampeded after several hours, after I had turned of the heatin ... |
24-11-2007 at 10:45
by: jam640 |
Learning to respect NBS the hard way
Oh boy.
I'm still kinda shaking. 
I decided to do a reaction I'd wanted to do for a long time to ... |
24-11-2007 at 10:43
by: jam640 |
1,3,5-Tris-(4-carboxyphenyl)benzene, please help!!!
Yes, organolithiums tend to be _very_ sensitive to oxygen/water contant and slightest impurity may f ... |
15-11-2007 at 14:01
by: jam640 |
1,3,5-Tris-(4-carboxyphenyl)benzene, please help!!!
Probably according to Journal of the American Chemical Society, 126(3), 884-890; 2004.
1. Is your i ... |
15-11-2007 at 02:59
by: jam640 |
Flammable limits and safety of diethyl ether
No, of course the fume concentration would be very much higher closer to the source but in _theory_ ... |
7-11-2007 at 12:33
by: jam640 |
Flammable limits and safety of diethyl ether
I was curious on how much diethyl ether gas that had to be present for a flammable/explosive mixture ... |
7-11-2007 at 03:46
by: jam640 |
Storage of Di-ethylether
I remember when I started studying chemistry how scared I was of using diethyl ether due to the pero ... |
5-11-2007 at 07:01
by: jam640 |
is 2,5-dimethoxyphenyl-2-nitroethane a white solid at r.t.?
Yes, most likely boron salts. They have a tendency to precipitate after a while unless extensive car ... |
29-10-2007 at 10:09
by: jam640 |
2-bromonaphthalene from naphthalene
freepatentsonline have a bit confusing website layout. I do not know if you really have a problem or ... |
23-10-2007 at 03:18
by: jam640 |
achiral molecules and chiral crystals
If you have access to Cambridge Structural Database you may do a search for compounds that crystalli ... |
22-10-2007 at 07:35
by: jam640 |
Need Pd/C, Thionyl Chloride, V, Ir, Pt etc...
The level of maturity has really sunken to a new low on this board lately...
Can't the people who d ... |
22-10-2007 at 00:23
by: jam640 |
predicting degree of unsaturation
The degree of unsaturation is a very simplified way of calculating the amount of multiple bonds pres ... |
21-10-2007 at 00:04
by: jam640 |
carboxylic acid functional group
Carbonic acid is carbon dioxide dissolved in water.
And that is not a mechanism, but a chemical equ ... |
18-10-2007 at 09:17
by: jam640 |
Solubility of NBS and succinimide in diethyl ether
Because I am not at the laboratory (late night here), and I am an impatient bastard who likes to rid ... |
17-10-2007 at 10:07
by: jam640 |
Solubility of NBS and succinimide in diethyl ether
Does anyone have empirical data on the solubility of n-bromosuccinimide and succinimide in diethyl e ... |
17-10-2007 at 09:48
by: jam640 |
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