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Mr. Anonymous: azo-clathrate primaries
Should the synthesis of the azo-clathrate be done under reflux as to not lose any water? or is that ... |
15-8-2011 at 14:22
by: krazypunk50 |
Polyisobutylene Extraction?
...and if this has been answered somewhere else please let me know. |
28-3-2011 at 14:27
by: krazypunk50 |
Polyisobutylene Extraction?
I recently extracted what I think is polyisobutylene from blu tack. My extraction is as follows:
... |
27-3-2011 at 10:32
by: krazypunk50 |
Nitric Acid Distillation Chemical Cleanup
The last time i tried acetic acid (and i did use vinegar 5%) nothing happened but this time I boiled ... |
19-9-2010 at 07:59
by: krazypunk50 |
Nitric Acid Distillation Chemical Cleanup
Neither hydrochloric acid nor acetic acid worked. And i also tried acetone and ethanol just in case ... |
18-9-2010 at 12:08
by: krazypunk50 |
Nitric Acid Distillation Chemical Cleanup
hissingnoise, if this is a calcium based contaminant, would it be a nitrate since it has gone throug ... |
17-9-2010 at 11:40
by: krazypunk50 |
Nitric Acid Distillation Chemical Cleanup
(if the answer to this question was already stated in an old topic, please delete this. I've looked ... |
16-9-2010 at 14:28
by: krazypunk50 |
RDX KA Method (big big problem)
Yes I did use that synthesis and you can find it on this website:
http://www.whitehonor.com/Kitc ... |
10-9-2010 at 18:20
by: krazypunk50 |
RDX KA Method (big big problem)
A few days ago I had a go at the KA method of producing rdx. the synthesis went as follows:
Disso ... |
9-9-2010 at 19:24
by: krazypunk50 |
RDX E method
I saw that episode! I believe they used hexamine with "strong" nitric acid and some other additives. ... |
22-7-2010 at 06:34
by: krazypunk50 |
RDX E method
Okay if this synthesis is always going to be low yield, I won't bother with the E method. Have you t ... |
15-7-2010 at 19:01
by: krazypunk50 |
RDX E method
I noticed the rhomboid crystals, too, when I was recrystallizing. I have one question about the defl ... |
13-7-2010 at 07:26
by: krazypunk50 |
RDX E method
I used 130ml AA, 52.5g NH4NO3, and 19g paraformaldehyde. My yield before recrystallization-13.4g. af ... |
12-7-2010 at 19:38
by: krazypunk50 |
RDX E method
The first time I tried the synthesis, I did not use BF3 because it was not listed in my synthesis. B ... |
11-7-2010 at 13:16
by: krazypunk50 |
RDX E method
Okay so the synthesis calls for the addition of 4% boron trifluoride. If I were to use the etherate, ... |
11-7-2010 at 07:25
by: krazypunk50 |
RDX E method
In the process, one of the chemicals needed is boron trifluoride. Do I need the actual gas or someth ... |
10-7-2010 at 20:09
by: krazypunk50 |
