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Hydride Embrittlement of Titanium Cathode.
Ti is quite suceptible to hydrogen uptake and embrittlement. Electrochemical H2 production creates a ...
7-8-2020 at 02:14
by: markx
Some basic questions and clarifications on NaCl chlorate cell and potassium chlorate

[quote]
And oh yeah it was chlorate. Stirred up a teaspoon of the extracted and ground powder wit ...
5-8-2020 at 08:09
by: markx
Some basic questions and clarifications on NaCl chlorate cell and potassium chlorate
Stainless steel is incompatible with halogen bearing solutions, like the one originating from a chlo ...
1-8-2020 at 12:12
by: markx
Perchlorate cell additives for Pt anode
[rquote=641902&tid=155572&author=Benignium]

@markx, do you have pictures of your anode pr ...
31-7-2020 at 03:51
by: markx
Some basic questions and clarifications on NaCl chlorate cell and potassium chlorate
[rquote=641821&tid=155898&author=Junk_Enginerd]Once I had added the 60/40 salt and noted a c ...
30-7-2020 at 03:36
by: markx
Perchlorate cell additives for Pt anode
[rquote=641756&tid=155572&author=mysteriusbhoice]I wonder how much chloroplatinic acid costs ...
29-7-2020 at 14:27
by: markx
Perchlorate cell additives for Pt anode
Good job! And congratulations on a successfull conversion run! :)

The fluffy percipitate is wel ...
28-7-2020 at 01:44
by: markx
Is Peroxide in Ethanol and issue for distillation?
[rquote=641489&tid=155868&author=Syn the Sizer]People drink peroxide in 30% conc. and the hi ...
26-7-2020 at 22:36
by: markx
More on PbO2 electrodes
This somewhat resembles the picture that I saw when my coatings disintegrated, but in my case there ...
17-7-2020 at 01:47
by: markx
Perchlorate cell additives for Pt anode
Connections to Ti electrodes tend to passivate, especially if the contact surface is negligible like ...
17-7-2020 at 01:36
by: markx
More on PbO2 electrodes
[rquote=639757&tid=2465&author=nitro-genes]Well....not sure if stunning progress is the righ ...
3-7-2020 at 15:14
by: markx
More on PbO2 electrodes
[rquote=639619&tid=2465&author=nitro-genes]The GSLD anode of a few posts above (shiny and de ...
3-7-2020 at 04:45
by: markx
More on PbO2 electrodes
[rquote=638517&tid=2465&author=nitro-genes]@Markx

After reading through the pulse reverse ...
3-7-2020 at 03:46
by: markx
More on PbO2 electrodes
[rquote=634471&tid=2465&author=nitro-genes]interesting comment on the reconditioning of the ...
22-4-2020 at 04:18
by: markx
More on PbO2 electrodes
You may want to keep on going with the electrolysis longer than 48h. In my experiments with Pt based ...
20-4-2020 at 01:34
by: markx
More on PbO2 electrodes
[rquote=632495&tid=2465&author=yobbo II]
Magnetite can be used for making chlorate. It only ...
13-3-2020 at 04:55
by: markx
More on PbO2 electrodes
I deposited an intermediate Pt layer on Ti before the lead dioxide deposition process was applied. F ...
14-2-2020 at 13:08
by: markx
More on PbO2 electrodes
[rquote=630595&tid=2465&author=Σldritch]Really nice work markx, i was just wondering, did y ...
14-2-2020 at 11:24
by: markx
Sensitivity of chlorate explosives/cheddite.
Chlorate mixes with liquid hydrocarbons tend not to be very sensitive towards mechanical manipulatio ...
15-1-2020 at 06:19
by: markx
Crystallization Techniques
Working with clean glassware, thoroughly filtered solutions (lack of cristallisation centers) and gi ...
12-1-2020 at 03:35
by: markx
Removing charcoal from evaporating dish
[rquote=629134&tid=154690&author=metalresearcher]Recntly

Use piranha water (H2SO4 + 30% ...
8-1-2020 at 01:58
by: markx
Hands aren’t the same as soft skin!
Sulfuric is nasty stuff! I always get a feeling that I itch all over when I work with it, although t ...
8-1-2020 at 00:06
by: markx
Best Graphite anode recipe (chlorate electrolysis)
[rquote=629079&tid=154683&author=Bogdonovan]Hello everyone, ive given up on trying to make c ...
6-1-2020 at 23:50
by: markx
Improvising The Bucket Still
In essence you have a simple distillation setup made from two buckets. The inner one with the submer ...
24-12-2019 at 11:21
by: markx
How do you occupy yourself during a distillation?
[rquote=626746&tid=154474&author=Herr Haber]All of the above & TV shows.

I do also so ...
25-11-2019 at 23:39
by: markx
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