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Science in danger - epa ordered to take down climate change page
Frankly,

Publicly funded science, is for the most part, one big circle jerk.

They heyday of sc ...
26-1-2017 at 22:09
by: mnick12
HNMR Services for Hire
Hey Steam,

This is great! I have access to NMR right now, but it won't always be that way! It is ...
26-1-2017 at 22:03
by: mnick12
Reaction of pyridine with [Cu(Cl)2(H2O)2] product is pyridine complex or the hydroxide ?
[rquote=472777&tid=71898&author=DraconicAcid][rquote=472776&tid=71898&author=mnick12 ...
24-1-2017 at 20:30
by: mnick12
Reaction of pyridine with [Cu(Cl)2(H2O)2] product is pyridine complex or the hydroxide ?
Its for sure the dichloride.

the pka of the pyrdidinium ion is less than 0 IIRC, there is practic ...
24-1-2017 at 19:34
by: mnick12
The problem with niobium
The bummer is, you probably are not going to be doing any cool catalysis with aqueous niobium compou ...
24-1-2017 at 19:04
by: mnick12
Used uv vis experiences
Thanks phlogiston,

I would like the computer interface for a number of reasons. As you mentioned ...
7-9-2016 at 19:50
by: mnick12
Used uv vis experiences
Has anyone here ever purchased a used uv vis spectrometer?

The reason why I ask, is I am in the m ...
6-9-2016 at 15:35
by: mnick12
How does enzyme phenylalanine hydroxylase generate tyrosine
Well from 5 minutes of googling it looks like hydroxylation occurs through a Fe(iv)-oxo intermediate ...
13-4-2016 at 22:22
by: mnick12
What makes things poisonous
Yes, like the others said its very broad.

From observation though many of the highly acutely tox ...
12-4-2016 at 13:55
by: mnick12
glass eating microbes
Dont think they exist.

Some plants and diatoms use silica compounds as part of there cel wall, bu ...
10-2-2016 at 11:17
by: mnick12
Preparation of 3-methoxybenzoic acid
Hmmm if you want to make 3-methoxybenzoic acid, I would start from methyl benzoate.

Nitration of ...
2-1-2016 at 13:10
by: mnick12
Alternate solvent for grignard
Pyridine and N-methylpyrolidine are probably gunna give junk, and will be a pain to remove from your ...
11-12-2015 at 23:40
by: mnick12
Facile, Efficient nitration of Phenol to 2,4-dinitrophenol
Uhhhhhh, there must be something wrong here or the article is complete bs.

Using a mixture of eth ...
6-12-2015 at 15:33
by: mnick12
CO in organic chemistry
Yeah the carbonylation of methanol is pretty tough without high pressures.

However CO insertion i ...
28-11-2015 at 18:04
by: mnick12
Looking for synthesis of 1-bromo-2,6-diisopropylbenzene
Well I decided to give in and wash with an aqueous thiosulfate solution, and it cleared the iodine r ...
22-7-2015 at 18:25
by: mnick12
Are the non-binding groups of coordination complexes reactive?
In almost every case I can think of, trying to modify a ligand such a PPh3 when it is bound to a met ...
27-5-2015 at 19:50
by: mnick12
Very old Ethyl Ether
Ya it is not a rumor,

Luckily most ether has BHT or something similair to scavenge for reactive o ...
17-5-2015 at 21:37
by: mnick12
Diazonium Question
This should be in the beginings sections.

I just did a diazo reaction a few weeks ago with 2,6-di ...
11-5-2015 at 10:15
by: mnick12
Difficulty forming metal-amino acid chelate, advice needed
Try the dimethoxyethane complex of NiCl2 in something like ether or THF, the aqua may be competing.
1-5-2015 at 18:12
by: mnick12
Removing iodine
Well,

I decided to make to make the iodobenzene instead, since no Cu salts are needed and you can ...
27-4-2015 at 20:52
by: mnick12
Looking for synthesis of 1-bromo-2,6-diisopropylbenzene
[rquote=400190&tid=62044&author=Chemosynthesis][rquote=400176&tid=62044&author=CuReU ...
8-4-2015 at 15:08
by: mnick12
Looking for synthesis of 1-bromo-2,6-diisopropylbenzene
Hi,

So I am looking to make a ligand from 1-bromo-2,6-diisopropylbenzene. Unfortunatly the materi ...
6-4-2015 at 20:28
by: mnick12
Nitrocyclohexane Synthesis Via double displacement reaction
[rquote=398870&tid=61939&author=Etaoin Shrdlu]Apparently, sodium nitrite in DMF works great ...
28-3-2015 at 15:28
by: mnick12
Nitrocyclohexane Synthesis Via double displacement reaction
[rquote=398854&tid=61939&author=Etaoin Shrdlu][size=-2]Hmmmm, I'm not as sure as you are tha ...
28-3-2015 at 13:29
by: mnick12
Nitrocyclohexane Synthesis Via double displacement reaction
Thats not going to work.

It looks like you are proposing an SN2 reaction.

A couple of things t ...
27-3-2015 at 22:43
by: mnick12
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