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Steam distillation tubing size?
[rquote=640280&tid=155760&author=CouchHatter]Consistent rate of steam generation matters mor ...
10-7-2020 at 07:01
by: monolithic
Ammonium Nitrate Purity?
Did you order this on Amazon? I just did the same, hope the purity can be improved through recrystal ...
9-7-2020 at 07:33
by: monolithic
U.S. based suppliers that will sell to individuals?
I've had good luck with Consolidated Chemical and Chemsavers. The latter will charge you an addition ...
8-7-2020 at 15:45
by: monolithic
Short question / quick answer - Thread
Are there any good books that cover practical syntheses and applications of energetic materials? I'v ...
25-6-2020 at 18:52
by: monolithic
Acetic anhydride preparation
[rquote=638561&tid=9&author=Waffles SS]Or why someone didnt try NaPO3(Sodium Metaphosphate) ...
23-6-2020 at 18:07
by: monolithic
Disappointing results with 3A molecular sieves
You might find this paper interesting: https://sci-hub.tw/10.1021/jo101589h

Fines can be an issue ...
20-6-2020 at 04:04
by: monolithic
how to pump nitric acid?
Venturi pump if you have access to compressed air but it's not going to be quiet or clean. Industria ...
19-6-2020 at 14:00
by: monolithic
CHP from KClO4?
Does anyone have the primary reference for CHP synthesis? Maybe I'm not looking in the right place b ...
19-6-2020 at 08:54
by: monolithic
Vacuum and fractional distillation
Those types of gauges aren't very accurate especially when you're trying to resolve a few mm Hg. You ...
15-6-2020 at 10:56
by: monolithic
Sep funnels and vacuum?
I've seen them used under vacuum like in this video https://www.youtube.com/watch?v=lBNhu4kJ4Mc

T ...
13-6-2020 at 11:00
by: monolithic
Inner Sleeve for 1L heating mantle
[rquote=638101&tid=155552&author=Sulaiman][rquote=638035&tid=155552&author=Mateo_swe ...
11-6-2020 at 04:45
by: monolithic
Inner Sleeve for 1L heating mantle
A heating element at reduced voltage won't run as hot. I have a 120V mantle which can hit 400-500 C ...
10-6-2020 at 17:14
by: monolithic
Inner Sleeve for 1L heating mantle
[rquote=637906&tid=155552&author=Mateo_swe]
I plan to drive it with either a variac or more ...
9-6-2020 at 04:37
by: monolithic
Simplest "power solvent" synthesis?
I think chloroform is the simplest and easiest solvent synthesis. If you buy bleach for pools it's u ...
7-6-2020 at 07:54
by: monolithic
Problems with wet chemical sodium synthesis
I bought new magnesium and it was very fine, curly shavings like your second video. I didn't even bo ...
4-6-2020 at 15:44
by: monolithic
Diaphragm pump + aspirator no B.P. change?
Trying orienting your aspirator so it is ejecting water straight down.
4-6-2020 at 13:54
by: monolithic
dumb question
Solvents and commodity chemicals are unprofitable. I think some people make a small profit selling s ...
29-5-2020 at 05:50
by: monolithic
Problems with wet chemical sodium synthesis
For anyone else trying this reaction, I would not recommend magnesium powder/dust unless you have ve ...
24-5-2020 at 13:42
by: monolithic
Latest chemical order?
[rquote=636733&tid=9890&author=j_sum1]A couple of kg of zinc ordered off ebay which I intend ...
23-5-2020 at 20:47
by: monolithic
Synthesising 1,4 Dioxane
As a follow up to my last post, I tried fractionally distilling the ethylene glycol + H2SO4. This br ...
23-5-2020 at 20:22
by: monolithic
Synthesising 1,4 Dioxane
I filled a 1000 ml round bottom flask, set up for simple distillation, with 350 ml of purified ethyl ...
22-5-2020 at 17:00
by: monolithic
sassafras extraction from roots - anyone have experience or know yeilds?
Seems like a lot of work but I imagine it smells amazing once separated and purified. I have a few t ...
22-5-2020 at 15:22
by: monolithic
Latest chemical order?
I just bought 64 oz of Liquid Lightning at WalMart. https://www.walmart.com/ip/Liquid-Lightning-Virg ...
22-5-2020 at 10:03
by: monolithic
Looking for Sudan III (Sudan Red) or substitutes...
[rquote=635567&tid=155341&author=nimgoldman]I am looking for Sudan III dye to use it as indi ...
22-5-2020 at 04:26
by: monolithic
Newe YouTube Video: Methyl Iodide Synthesis with Aluminum Foil
Nice video. If you have the time, I'm sure many of us would also appreciate a video on just your des ...
21-5-2020 at 04:43
by: monolithic
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