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Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638530&tid=155586&author=Boffis]@michaljemco; Thankyou for posting details of your p ...
17-6-2020 at 04:05
by: myr
Cyclic diester from 2,2'-oxydibenzoic acid?
[rquote=638465&tid=155586&author=michalJenco][rquote=638441&tid=155586&author=Boffis ...
16-6-2020 at 12:05
by: myr
bis(chloromethyl)ether from hexamine hydrolysis?
I wouldn't worry, as BCME is toxic due to it's reactivity, so it will react with the amine species i ...
18-5-2020 at 12:54
by: myr
2,4-dihydroxybenzoic acid from resorcinol
Nice reaction! Never heard of it, but worth trying.
Here's a rather old lit. review:
Lindsey, A. ...
15-5-2020 at 14:36
by: myr
Recrystallization solvent for a-methyl dehydrozingerone
Hello,

Recently I prepared a-methyldehydrozingerone in pretty OK yield using putative metaboric a ...
3-5-2020 at 05:16
by: myr
eBay messed up my order, what should I do with 50kg of ammonium nitrate?
I'd resell it, use it as fertilizer, keep it as a handy stockpile, bomb a government building, make ...
28-3-2020 at 06:48
by: myr
Vanillin ring closure
[rquote=630429&tid=154810&author=njl]I'd like to preface this by saying my question definite ...
3-2-2020 at 11:42
by: myr
Methylthiomethylation of Vanillin: Help understanding a French procedure
The attachment is broken, looks like. Attempt 2.

http://www.filedropper.com/academiedesbpt6k4802 ...
24-12-2019 at 08:48
by: myr
Methylthiomethylation of Vanillin: Help understanding a French procedure
Hello,

After considerable effort I was able to find the following paper (attached below) which de ...
24-12-2019 at 08:45
by: myr
Aspartic Acid Degredation Failure
The reaction did work at first, transient orange color and lots of gas emitted.

Has anyone tried ...
28-11-2019 at 11:17
by: myr
Aspartic Acid Degredation Failure
The following procedure, from the paper 'Biobased synthesis of acrylonitrile from glutamic acid' was ...
28-11-2019 at 11:15
by: myr
Where to get cheap TLC plates?
Hello,

I was looking to buy TLC plates- but all the ones I found were surprisingly expensive, man ...
19-10-2019 at 04:52
by: myr
Sodium Borohydride Group Buy
I would be interested
21-9-2019 at 07:31
by: myr
Help with the workup of 4-methoxyanisole
Hello,

Recently I attempted to prepare the dimethyl ether of hydroquinone, or 1-4 dimethoxybenzen ...
19-6-2019 at 09:09
by: myr
Notre Dame Smoke
The enormity of the tragedy cannot possibly be overstated, and I am only thankful that (to the best ...
15-4-2019 at 18:54
by: myr
3,4,5-trimethoxyphenylacetonitrile hydrogenation problems
Tetrabutylammonium borohydride will work (but doing so is 100% illegal.)
25-1-2019 at 06:55
by: myr
Ideas for Cold Weather Chemistry, Unlimited Chilling is Free in Winter take advantage of it
Trimethylsulfonium bromide!
5-1-2019 at 14:04
by: myr
NaH2PO2 from China on Ebay?
I have now hidden my email address (why it was shown in the first place is beyond me) and your point ...
24-12-2018 at 10:50
by: myr
NaH2PO2 from China on Ebay?
Hello,

I was wondering if anyone had any experience with ordering hypophosphite from Ebay. There ...
23-12-2018 at 06:25
by: myr
I want some cyanide, should I choose NaCN or KCN?
For what reason, exactly, do you want cyanide for?

KCN is cheaper on Sigma-Aldrich.
6-12-2018 at 18:27
by: myr
Preparation of trimethylsulfoxonium?
[rquote=555301&tid=106223&author=UC235]Your first reference is using trimethylsulfonium, S(M ...
23-11-2018 at 06:07
by: myr
Preparation of trimethylsulfoxonium?
Trimethylsulfoxonium is a rather useful reagent, allowing for the easy synthesis of epoxides and cyc ...
22-11-2018 at 11:17
by: myr
Trying out a stille coupling reaction
I do not believe any diagrams are needed here. All the reactants are very clearly defined in a well- ...
10-11-2018 at 08:50
by: myr
Aluminium isopropoxide - reaction with water
Wash with a little dry solvent miscible with water that has a decently high vapor pressure- acetone, ...
25-10-2018 at 09:08
by: myr
Preparation of nitroethane
Have you considered using phase-transfer catalysis? I know longer-chain nitroalkanes can be made wit ...
17-10-2018 at 11:09
by: myr
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