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Vanillin ring closure
[rquote=630429&tid=154810&author=njl]I'd like to preface this by saying my question definite ...
3-2-2020 at 11:42
by: myr
Methylthiomethylation of Vanillin: Help understanding a French procedure
The attachment is broken, looks like. Attempt 2.

http://www.filedropper.com/academiedesbpt6k4802 ...
24-12-2019 at 08:48
by: myr
Methylthiomethylation of Vanillin: Help understanding a French procedure
Hello,

After considerable effort I was able to find the following paper (attached below) which de ...
24-12-2019 at 08:45
by: myr
Aspartic Acid Degredation Failure
The reaction did work at first, transient orange color and lots of gas emitted.

Has anyone tried ...
28-11-2019 at 11:17
by: myr
Aspartic Acid Degredation Failure
The following procedure, from the paper 'Biobased synthesis of acrylonitrile from glutamic acid' was ...
28-11-2019 at 11:15
by: myr
Where to get cheap TLC plates?
Hello,

I was looking to buy TLC plates- but all the ones I found were surprisingly expensive, man ...
19-10-2019 at 04:52
by: myr
Sodium Borohydride Group Buy
I would be interested
21-9-2019 at 07:31
by: myr
Help with the workup of 4-methoxyanisole
Hello,

Recently I attempted to prepare the dimethyl ether of hydroquinone, or 1-4 dimethoxybenzen ...
19-6-2019 at 09:09
by: myr
Notre Dame Smoke
The enormity of the tragedy cannot possibly be overstated, and I am only thankful that (to the best ...
15-4-2019 at 18:54
by: myr
3,4,5-trimethoxyphenylacetonitrile hydrogenation problems
Tetrabutylammonium borohydride will work (but doing so is 100% illegal.)
25-1-2019 at 06:55
by: myr
Ideas for Cold Weather Chemistry, Unlimited Chilling is Free in Winter take advantage of it
Trimethylsulfonium bromide!
5-1-2019 at 14:04
by: myr
NaH2PO2 from China on Ebay?
I have now hidden my email address (why it was shown in the first place is beyond me) and your point ...
24-12-2018 at 10:50
by: myr
NaH2PO2 from China on Ebay?
Hello,

I was wondering if anyone had any experience with ordering hypophosphite from Ebay. There ...
23-12-2018 at 06:25
by: myr
I want some cyanide, should I choose NaCN or KCN?
For what reason, exactly, do you want cyanide for?

KCN is cheaper on Sigma-Aldrich.
6-12-2018 at 18:27
by: myr
Preparation of trimethylsulfoxonium?
[rquote=555301&tid=106223&author=UC235]Your first reference is using trimethylsulfonium, S(M ...
23-11-2018 at 06:07
by: myr
Preparation of trimethylsulfoxonium?
Trimethylsulfoxonium is a rather useful reagent, allowing for the easy synthesis of epoxides and cyc ...
22-11-2018 at 11:17
by: myr
Trying out a stille coupling reaction
I do not believe any diagrams are needed here. All the reactants are very clearly defined in a well- ...
10-11-2018 at 08:50
by: myr
Aluminium isopropoxide - reaction with water
Wash with a little dry solvent miscible with water that has a decently high vapor pressure- acetone, ...
25-10-2018 at 09:08
by: myr
Preparation of nitroethane
Have you considered using phase-transfer catalysis? I know longer-chain nitroalkanes can be made wit ...
17-10-2018 at 11:09
by: myr
Demethylation of Vanillin and Eugenol
Do you have the capacity to carry out TLC plates?
9-10-2018 at 07:35
by: myr
Demethylation of Vanillin and Eugenol
I would recommend extraction with ethyl acetate- worked very nicely for 5-hydroxyvanillin, might wor ...
1-10-2018 at 16:25
by: myr
Help with benzyl isoeugenol
After the isomerization of benzyleugenol (from benzyl tosylate [from tosyl chloride]) with KOH in de ...
23-9-2018 at 11:01
by: myr
Demethylation of Vanillin and Eugenol
Have you seen the paper for AlI3/tetrabutylammonium? Xylene or toluene should substitute nicely for ...
18-9-2018 at 15:02
by: myr
Simple organofluorines?
I hope this can be useful. My original idea was addition of HF across an alkene, but this is impossi ...
7-8-2018 at 09:00
by: myr
S-Isopropylisothiouronium bromide
I would like to present my preliminary findings, and ask for further advice.

S-Isopropylisothiour ...
6-8-2018 at 06:55
by: myr

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