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Measuring pH in a Chlorate cell sorry to necro this but I am currently actually working on a 100A chlorate cell and the way pH measu ...	23-4-2024 at 15:01 by: mysteriusbhoice
Electrolysis of Sodium Bisulfate to form Sodium Persulfate yea the gypsum itself actually acts like more than just a diaphragm it can actually act as a cation ...	20-4-2024 at 17:11 by: mysteriusbhoice
Electrolysis of Sodium Bisulfate to form Sodium Persulfate MgSO4 is better because it also stops reduction of chlorate by the coating of ion conductive Mg(OH)2 ...	11-4-2024 at 16:29 by: mysteriusbhoice
Electrolysis of Sodium Bisulfate to form Sodium Persulfate you dont need persulfate to make perchlorates and making persulfate is HARDER than perchlorates as i ...	7-4-2024 at 23:04 by: mysteriusbhoice
Questions in electroplating to plate on aluminum you need to first do zincate bath then finally a layer of whatever metal you wa ...	8-2-2024 at 14:22 by: mysteriusbhoice
Can KBH4 substitute NaBH4 in ethanol/methanolic solutions for reduction of ketones to alcohol. I found that KBH4 is half the price of NaBH4 (which is always out of stock) atleast where im at and ...	12-1-2024 at 15:18 by: mysteriusbhoice
NaBH4 now on DEA Special Surveillance List reject borohydride accept poisoned palladium catalyst for selective reductions eg Co-Pd.	6-1-2024 at 17:42 by: mysteriusbhoice
Glyoxylic acid synthesis - starting w/ oxalic :: w/o PbO2 graphite works because this is a reduction reaction so using PbO2 which will oxidize the fk out of t ...	1-1-2024 at 00:22 by: mysteriusbhoice
chlorination of ethylene glycol I am really more interested in making ethyl chlorohydrin rather than dichloroethane because I can si ...	24-12-2023 at 00:33 by: mysteriusbhoice
chlorination of ethylene glycol [rquote=5048&tid=583&author=DDTea]I know that by reacting HCl gas with boiling Ethylene Glyc ...	22-12-2023 at 19:07 by: mysteriusbhoice
Electroplating of Nickel, waterless / organic solvent / possibly ionic liquids. why not use an actually conductive liquid like propylene carbonate or acetonitrile as your electroly ...	26-11-2023 at 15:13 by: mysteriusbhoice
NaClO3 by electrolysis NaClO is oxidized directly if pH is above 9 to NaClO3 and this is the reaction mechanism that most a ...	22-10-2023 at 20:03 by: mysteriusbhoice
Nitric acid from mild electrochemistry for this version you can oxidize it using whatever anode really I will try with PbO2 and membrane is ...	15-10-2023 at 20:46 by: mysteriusbhoice
Nitric acid from mild electrochemistry If you want the TLDR of the paper here are the 2 relevant graphs for scale up. Figure E is applied ...	15-10-2023 at 01:14 by: mysteriusbhoice
Nitric acid from mild electrochemistry I got access to the full paper and sadly from what I read you need to run at 1.2V across the cell wh ...	14-10-2023 at 17:37 by: mysteriusbhoice
Proper electrode material for arc melting steel if you have inert gas you can probably use tungsten as your electrode	16-9-2023 at 14:57 by: mysteriusbhoice
Ir-Ta vs Ir-Ru MMO you cannot unpower an Ir-Ru anode while its in solution its better to have a pump drain the electrol ...	10-9-2023 at 14:38 by: mysteriusbhoice
Ir-Ta vs Ir-Ru MMO [rquote=687315&tid=158001&author=chemistry4frog]wait am i mixed up, in a chloro alkali cell, ...	9-9-2023 at 17:07 by: mysteriusbhoice
Ir-Ta vs Ir-Ru MMO the anode chamber must not reach pH of 10 or it will cause RuO4 to be formed at the anode as the cel ...	6-9-2023 at 17:29 by: mysteriusbhoice
Nafion Cell for Chloro Alkali The cement membranes are less conductive if they are too thick but are very robust. I recommend addi ...	22-8-2023 at 20:23 by: mysteriusbhoice
Nafion Cell for Chloro Alkali [rquote=686886&tid=159817&author=chemistry4frog] can lead dioxide be used as an anode in th ...	22-8-2023 at 01:48 by: mysteriusbhoice
Nafion Cell for Chloro Alkali ive ran these before and iodized salt isnt usually the problem as there are mentions of Ir-Ru making ...	21-8-2023 at 02:32 by: mysteriusbhoice
DIY Divided electrochemical cell with stirring and cooling cement takes a few days to cure completely I would let it set for a day and put it underwater for 1 ...	17-8-2023 at 18:09 by: mysteriusbhoice
DIY Divided electrochemical cell with stirring and cooling if the cylinder was made of ionomer cement I wonder how much higher the current can be pushed thru.	14-8-2023 at 15:44 by: mysteriusbhoice
Homemade carbon electrodes add maybe SnO2 but it may reduce to tin in that environment sadly. Pb salts are another option as it ...	16-6-2023 at 18:26 by: mysteriusbhoice
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