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Isopropyl salicylate sensitivity
[rquote=692296&tid=160275&author=DraconicAcid]Anyway, what did it smell like? We all know t ... |
7-4-2024 at 19:27
by: night429 |
Isopropyl salicylate sensitivity
[rquote=692260&tid=160275&author=Dr.Bob]isopropyl alcohol is pretty sterically hindered, so ... |
7-4-2024 at 16:07
by: night429 |
Isopropyl salicylate sensitivity
I recently made isopropyl salicylate following a [url=https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9 ... |
5-4-2024 at 22:33
by: night429 |
Aluminum soaps
Also, here's a picture of the product I made that I forgot to post in the original text.
[file]1 ... |
5-3-2024 at 11:36
by: night429 |
Aluminum soaps
[rquote=691357&tid=160201&author=EF2000]Only use that comes to mind is old fashioned napalm. ... |
5-3-2024 at 11:35
by: night429 |
Aluminum soaps
I've been testing some aluminum soaps from a few fats and oils I have on hand. I decided to detail t ... |
5-3-2024 at 01:36
by: night429 |
A failed attempt at p-hydroxybenzoic acid
[rquote=690537&tid=160131&author=clearly_not_atara]
EDIT: Oh, I see. You didn't measure the ... |
31-1-2024 at 00:47
by: night429 |
A failed attempt at p-hydroxybenzoic acid
[rquote=690449&tid=160131&author=bnull]What follows is a speculation.
You deviated substa ... |
29-1-2024 at 00:54
by: night429 |
A failed attempt at p-hydroxybenzoic acid
I was following the procedure per [url=http://www.orgsyn.org/demo.aspx?prep=CV2P0341]orgsyn[/url].
... |
26-1-2024 at 01:27
by: night429 |
Calcium cyanurate ---> Cyanamide
I recently produced calcium cyanamide by this method (ammoniacal silver nitrate produced the charact ... |
12-4-2023 at 19:52
by: night429 |
Tetraamminecopper(ii) Picrate - Synthesis and Characterization
I made a mention of this compound last year in the exotic primaries thread, but figured that I may a ... |
28-12-2022 at 01:12
by: night429 |
Exotic Primaries - Complex Salts
I've seen it mentioned once in this thread, but I made (what I believe to be) tetraamminecopper (ii) ... |
28-12-2021 at 22:05
by: night429 |
magnesium from soda cans
[rquote=665162&tid=157921&author=Fulmen]Sorry, but that won't work. Magnesium reacts with wa ... |
11-9-2021 at 09:09
by: night429 |
My attempt at the Skraup quinoline synthesis
Alright, thanks! I'm looking forward to hearing of the results of your Skraup and trinitrotoluene pr ... |
25-8-2021 at 18:02
by: night429 |
My attempt at the Skraup quinoline synthesis
[rquote=664509&tid=157858&author=Fery]Hi night429, very nice!
So you got a mixture of quino ... |
25-8-2021 at 07:31
by: night429 |
My attempt at the Skraup quinoline synthesis
A few months ago, I got the idea to do the Skraup synthesis. The general procedure I followed was th ... |
24-8-2021 at 21:14
by: night429 |
Why are sulfuric acid ratios the same for nitrate salt and nitric acid?
[rquote=663835&tid=156787&author=caterpillar]I made TNP via H2SO4 + KNO3 and definitely coul ... |
10-8-2021 at 17:32
by: night429 |
Accidentally making potassium picrate(?)
Yesterday, I tried to make some picric acid from a procedure that has been successful in the past, b ... |
5-6-2021 at 14:00
by: night429 |
Azo dye: p-aminophenol and 4-chloro-2-nitrophenol
It's interesting that there's the possibility of both inter- and intramolecular anhydride formations ... |
17-5-2021 at 13:03
by: night429 |
Azo dye: p-aminophenol and 4-chloro-2-nitrophenol
Hey Fery, Yep, you do get 6-hydroxyquinoline! I'm following the 8-hydroxyquinoline prep from Vogel, ... |
17-5-2021 at 08:49
by: night429 |
Azo dye: p-aminophenol and 4-chloro-2-nitrophenol
Thanks Boffis, I'll have to try that instead for the hydrochloride! I haven't done too much research ... |
16-5-2021 at 23:44
by: night429 |
Azo dye: p-aminophenol and 4-chloro-2-nitrophenol
Huh, I've found that p-aminophenol doesn't discolor at all when stored as the freebase... just stays ... |
16-5-2021 at 20:51
by: night429 |
Azo dye: p-aminophenol and 4-chloro-2-nitrophenol
Hi pumpkins, I should really try that. I thought that the one-pot would have been less work, but it ... |
16-5-2021 at 17:45
by: night429 |
Synthesis of 4-chloro-2-nitrophenol
Thanks Boffis! That makes sense, and I know practically nothing about actual dye processes. I tested ... |
11-5-2021 at 10:14
by: night429 |
Synthesis of 4-chloro-2-nitrophenol
So, after a couple of months, I finally decided to revisit this. I don't know what happened, but I g ... |
9-5-2021 at 19:35
by: night429 |
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