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DDNP & related compounds: The über thread!
There, I'm all done! :)


[file]74086[/file]

[Edited on 28-2-2019 by nitro-genes]
28-2-2019 at 07:06
by: nitro-genes
DDNP & related compounds: The über thread!
Final report on styphnamic and its diazoderivative...there, I'm all done! :)
28-2-2019 at 06:59
by: nitro-genes
Amateur Chemistry now vs several decades ago
When I was like 17 or 18, I bought 2 bags of ammonium nitrate fertilizer together with a friend of m ...
27-2-2019 at 10:24
by: nitro-genes
New proposal for EU regulations
Citing from the regulation proposal:

Making available, introduction, possession and use
1. Restr ...
23-2-2019 at 08:50
by: nitro-genes
DDNP & related compounds: The über thread!
Curiosity won again... Ok, one final experiment with the potassium salt! :D

The brown compact cr ...
23-2-2019 at 06:41
by: nitro-genes
DDNP & related compounds: The über thread!
@ Rosco....Yeah, I get the feeling there may be some hydrates involved here and there after all. I ...
22-2-2019 at 11:57
by: nitro-genes
The Wump Incident
J_Sum...Oef... painful to watch these glass shards...Hopefully the surgeon managed to pick all of th ...
22-2-2019 at 11:49
by: nitro-genes
Synthesis and some properties of 2-amino 4,6-dinitroresorcinol and 2-diazo 4,6-dinitroresorcinol
Here a rough first version of the copper/ascorbic mediated reduction of styphnic acid to styphnamic ...
18-2-2019 at 14:14
by: nitro-genes
DDNP & related compounds: The über thread!
Yes, been wondering the same. Similarly to lead azide, the potassium salt of 2-DDNR is described by ...
16-2-2019 at 12:44
by: nitro-genes
DDNP & related compounds: The über thread!
Judging by the high solubility of the potassium salt they obtained (not much evidence though), it se ...
15-2-2019 at 18:11
by: nitro-genes
DDNP & related compounds: The über thread!
Uploaded the relevant abstract, you were clearly busy... :P



[Edited on 14-2-2019 by nitro-genes ...
14-2-2019 at 12:12
by: nitro-genes
DDNP & related compounds: The über thread!
Not 100% sure, though I'm not 100% sure the earth isn't flat either :P. The melting point of styphn ...
14-2-2019 at 06:56
by: nitro-genes
DDNP & related compounds: The über thread!
The electronic structure of diazophenols have been reviewed a couple of times. None of them mention ...
13-2-2019 at 18:04
by: nitro-genes
DDNP & related compounds: The über thread!
Indeed, but then again...there aren't many things I wouldn't want to add to concentrated nitric. :)
...
12-2-2019 at 16:22
by: nitro-genes
DDNP & related compounds: The über thread!
Not sure how readily and stable nitro-nitroso substitution of the 5 position for 4,6-dinitropyrogall ...
11-2-2019 at 08:31
by: nitro-genes
Selective reduction of nitrotoluenes with Na2S
Do you have the reference for selective reduction of paranitrotoluene using sulfides? Only knew that ...
9-2-2019 at 05:22
by: nitro-genes
DDNP & related compounds: The über thread!
Somewhat offtopic:

It seems the amino group of styphnamic acid (2-amino 4,6-dinitroresorcinol) is ...
7-2-2019 at 13:46
by: nitro-genes
Benzoquinone from Paracetamol
Not of much help, though since you started with 80 ml 50% sulfuric, and collected about 40 ml distil ...
5-2-2019 at 14:08
by: nitro-genes
DDNP & related compounds: The über thread!
Not sure if any of the transitions metals would make suitable salts, I wonder if these would be very ...
2-2-2019 at 14:52
by: nitro-genes
DDNP & related compounds: The über thread!
The lithium and rubidium salts might be interesting as well, very probable these were made in some l ...
31-1-2019 at 10:53
by: nitro-genes
DDNP & related compounds: The über thread!
My guess would be that due to the nitro groups, the ring system is too electron deficient for formal ...
31-1-2019 at 06:21
by: nitro-genes
PTFE near miss – split from Life after detonation
Holy shit, sounds like a nasty experience! Good that you were not in the direct vicinity when it dec ...
30-1-2019 at 06:14
by: nitro-genes
Reactive Liners
Agreed, in case of the vulcan SC, the liner is probably not composed of two separate materials that ...
27-1-2019 at 05:40
by: nitro-genes
Short question / quick answer - Thread
Planning to write sort of an more in depth essay about the copper/ascorbic reduction with some addit ...
25-1-2019 at 10:39
by: nitro-genes
Reactive Liners
Really nice application of reactive liners seems the vulcan charge, developed by Dr. Sidney Alford. ...
25-1-2019 at 07:47
by: nitro-genes
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