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Synthesis and some properties of 2-amino 4,6-dinitroresorcinol and 2-diazo 4,6-dinitroresorcinol
Here a rough first version of the copper/ascorbic mediated reduction of styphnic acid to styphnamic ...
18-2-2019 at 14:14
by: nitro-genes
DDNP & related compounds: The über thread!
Yes, been wondering the same. Similarly to lead azide, the potassium salt of 2-DDNR is described by ...
16-2-2019 at 12:44
by: nitro-genes
DDNP & related compounds: The über thread!
Judging by the high solubility of the potassium salt they obtained (not much evidence though), it se ...
15-2-2019 at 18:11
by: nitro-genes
DDNP & related compounds: The über thread!
Uploaded the relevant abstract, you were clearly busy... :P



[Edited on 14-2-2019 by nitro-genes ...
14-2-2019 at 12:12
by: nitro-genes
DDNP & related compounds: The über thread!
Not 100% sure, though I'm not 100% sure the earth isn't flat either :P. The melting point of styphn ...
14-2-2019 at 06:56
by: nitro-genes
DDNP & related compounds: The über thread!
The electronic structure of diazophenols have been reviewed a couple of times. None of them mention ...
13-2-2019 at 18:04
by: nitro-genes
DDNP & related compounds: The über thread!
Indeed, but then again...there aren't many things I wouldn't want to add to concentrated nitric. :)
...
12-2-2019 at 16:22
by: nitro-genes
DDNP & related compounds: The über thread!
Not sure how readily and stable nitro-nitroso substitution of the 5 position for 4,6-dinitropyrogall ...
11-2-2019 at 08:31
by: nitro-genes
Selective reduction of nitrotoluenes with Na2S
Do you have the reference for selective reduction of paranitrotoluene using sulfides? Only knew that ...
9-2-2019 at 05:22
by: nitro-genes
DDNP & related compounds: The über thread!
Somewhat offtopic:

It seems the amino group of styphnamic acid (2-amino 4,6-dinitroresorcinol) is ...
7-2-2019 at 13:46
by: nitro-genes
Benzoquinone from Paracetamol
Not of much help, though since you started with 80 ml 50% sulfuric, and collected about 40 ml distil ...
5-2-2019 at 14:08
by: nitro-genes
DDNP & related compounds: The über thread!
Not sure if any of the transitions metals would make suitable salts, I wonder if these would be very ...
2-2-2019 at 14:52
by: nitro-genes
DDNP & related compounds: The über thread!
The lithium and rubidium salts might be interesting as well, very probable these were made in some l ...
31-1-2019 at 10:53
by: nitro-genes
DDNP & related compounds: The über thread!
My guess would be that due to the nitro groups, the ring system is too electron deficient for formal ...
31-1-2019 at 06:21
by: nitro-genes
PTFE near miss – split from Life after detonation
Holy shit, sounds like a nasty experience! Good that you were not in the direct vicinity when it dec ...
30-1-2019 at 06:14
by: nitro-genes
Reactive Liners
Agreed, in case of the vulcan SC, the liner is probably not composed of two separate materials that ...
27-1-2019 at 05:40
by: nitro-genes
Short question / quick answer - Thread
Planning to write sort of an more in depth essay about the copper/ascorbic reduction with some addit ...
25-1-2019 at 10:39
by: nitro-genes
Reactive Liners
Really nice application of reactive liners seems the vulcan charge, developed by Dr. Sidney Alford. ...
25-1-2019 at 07:47
by: nitro-genes
DDNP & related compounds: The über thread!
It depends on the isomer, o-DDNP often precipitates as more of a bright yellow colour, while there i ...
22-1-2019 at 13:46
by: nitro-genes
DDNP & related compounds: The über thread!
Almost everything I made over the last couple of years was yellow of some sorts, which compound are ...
17-1-2019 at 00:32
by: nitro-genes
PETN-based Cast Explosives
Wasn't sure which topic was most suitable to post the article about the sensitivity of molten ETN, m ...
17-1-2019 at 00:26
by: nitro-genes
Reactive Liners
Isn't the dragons breath munition zirconium based as well? How much of the burning zirconium would a ...
17-1-2019 at 00:09
by: nitro-genes
Methyl Ethyl Ketone Peroxide
MEKP is commonly used as a hardener for epoxy resins, I think going through some material safety dat ...
17-1-2019 at 00:04
by: nitro-genes
DDNP & related compounds: The über thread!
Last bit of isopicramic needed to get rid of...

Set out to make made some very pure p-DDNP (4-dia ...
14-1-2019 at 16:04
by: nitro-genes
DDNP & related compounds: The über thread!
Again, for anyone experimenting with the salts of DDNR, [b]be extremely careful handling these compo ...
14-1-2019 at 08:32
by: nitro-genes
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