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Phenylaceton (P2P), simple preperation
In breaking bad WW uses thorium dioxide as a catalyst for the reaction, not as a stoichiometric reag ...
27-2-2021 at 18:48
by: njl
Hinmeijer/Anulab is gone
I think Tsjerk meant a precursor to a chemical weapon IE phosphorus oxychloride
27-2-2021 at 14:24
by: njl
White growth on unopened container of chlorotrimethylsilane
Only the NH4Cl will, but everything else is harmless and can be wiped off with paper.
27-2-2021 at 14:18
by: njl
White growth on unopened container of chlorotrimethylsilane
I envy your access to silanes. Pictures would help more experienced members help you. My first guess ...
26-2-2021 at 12:53
by: njl
Weird precipitate (tin-carbonate?)
I don't think tin carbonates are stable and instead decompose into oxides. You probably have a tin o ...
25-2-2021 at 08:19
by: njl
OTC Oxalyl Chloride?
If you want to add a radical scavenger you're really getting away from the OTC premise. Phosgene isn ...
22-2-2021 at 10:20
by: njl
OTC Oxalyl Chloride?
The link you have to organic-chem doesn't work for me. MTBE isn't exactly otc since I don't think yo ...
22-2-2021 at 07:45
by: njl
Question about pressure
Is that glass or plastic? Either way stirring shouldn't be a problem. Now, do you mean that during t ...
21-2-2021 at 13:31
by: njl
What is this urea stuff I found
Unless you're in North Korea you should be able to find more info on [i]one of the most integral com ...
20-2-2021 at 14:39
by: njl
Anyone have a simple tetrapropylammonium bromide?
I doubt the procedure would be very different for propyl alcohol. I also don't think IPA would be a ...
20-2-2021 at 07:48
by: njl
NiCl2 Weirdness
@Panache Thank you. The point of stirring would be to create an even suspension of the metal in solu ...
20-2-2021 at 07:44
by: njl
Separation of nitrotoluene isomers
Yeah, could be contamination. Depending on the actual procedure followed there could still be sulfat ...
19-2-2021 at 08:14
by: njl
Recovery of Pb and NaOH from Sodium Plumbite
Fluorite loves 10 year olds I guess
19-2-2021 at 08:11
by: njl
Amidation of cinnamic acid using CDMT
15 days with or without heating/agitation?
18-2-2021 at 08:10
by: njl
Acetic anhydride preparation
Please elaborate...
17-2-2021 at 17:44
by: njl
Dimethyl Carbonate
I recently received a jug of paint stripper that is ~50 percent dimethyl carbonate. Remainder is dio ...
17-2-2021 at 17:37
by: njl
Beta-Alanine amino acid copper salt
I'm not sure if chirality is the right term, but that type of isomerism can actually effect reaction ...
17-2-2021 at 11:02
by: njl
Benzoyl chloride + 4-Aminoadamantan-1-ol
No specific ref, but I think that once the amine salt is formed the alcohol can be halogenated a la ...
16-2-2021 at 07:15
by: njl
Benzoyl chloride + 4-Aminoadamantan-1-ol
Maybe chlorinate with HCl to get 4-Aminoadamantan-1-chloride, followed by reaction with sodium benzo ...
14-2-2021 at 19:27
by: njl
Benzoyl chloride + 4-Aminoadamantan-1-ol
The amine shown in the procaine synthesis is tertiary so it can't be acylated by benzoyl chloride, 4 ...
14-2-2021 at 14:28
by: njl
NiCl2 Weirdness
@Lion will do.

@Boffis lighten up a little... it's impossible to over engineer something done pur ...
14-2-2021 at 07:51
by: njl
NiCl2 Weirdness
I'm having some trouble with a batch of nickel chloride I just made. I did not follow a procedure re ...
13-2-2021 at 10:48
by: njl
Acetic anhydride preparation
Can't remember where but I think I remember a prep for isopropenyl acetate that involved bubbling MA ...
11-2-2021 at 05:51
by: njl
Acetic Anhydride from Zinc Acetate?
It would have cost you nothing to not say that.
9-2-2021 at 09:12
by: njl
A new way to make NCl3?
Yeah, but the chlorination of ammonia is the standard method for NCl3. How is this new?
9-2-2021 at 08:16
by: njl
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