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Ethyl Acetate? I've always shaken my impure EtOAc with a saturated CaCl2 solution and distilled after seperation gi ...	12-6-2011 at 14:41 by: rrkss
Drying Ether for Grignard When I ran my grignard, I used a molecular sieve to dry my ether and simply CaCl2 for the alkyl hali ...	11-3-2011 at 20:15 by: rrkss
Na2SO4 Its anhydrous form is very useful in drying organic liquids	25-2-2011 at 11:25 by: rrkss
NaOH in hotel swimming pool ? chlorine stays in solution as the hypochlorite ion when the water is alkaline and gases off as chlor ...	7-2-2011 at 11:30 by: rrkss
Chemicals in NZ. Not industrial qunatites [rquote=200308&tid=15391&author=mewrox99]Problem is I'm only 15 so I can't say I'm using it ...	1-2-2011 at 03:07 by: rrkss
Chemicals in NZ. Not industrial qunatites [rquote=200227&tid=15391&author=mewrox99]Yeah I was thinking about making it. Except to lega ...	31-1-2011 at 12:21 by: rrkss
Ethyl Acetate? if the azeotrope is water, you should see two layers form when you distill the ethyl acetate. My gu ...	17-1-2011 at 16:44 by: rrkss
Ethyl Acetate? It is, I just removed grease from one of my ties using some EtOAc, saved on a dry cleaning bill :-).	16-1-2011 at 09:28 by: rrkss
Ethyl Acetate? The easiest way to remove the ethanol is shake it with a saturated solution of CaCl2 and H2O. What ...	15-1-2011 at 19:55 by: rrkss
Make Potassium (from versuchschemie.de) [rquote=197956&tid=14970&author=mr.crow]tert-Butanol is really annoying. It came in a 1L bot ...	9-1-2011 at 19:11 by: rrkss
Make Potassium (from versuchschemie.de) [rquote=197412&tid=14970&author=garage chemist]I cleaned up my potassium pieces by melting t ...	5-1-2011 at 15:19 by: rrkss
Adding organics, CHCl3, and concentrated H2SO4? [rquote=197026&tid=15190&author=mario840]why not ?? just generate it from NaN3 and H2SO4 etc ...	1-1-2011 at 11:37 by: rrkss
Adding organics, CHCl3, and concentrated H2SO4? Distill the the darkened CHCl3 and try again with the more pure distilled product. Usually H2SO4 is ...	1-1-2011 at 11:31 by: rrkss
Synthesis of longer chain tertiary alcohols [rquote=196765&tid=15171&author=blogfast25]Does this mean that 3-methyl-3-pentanol would not ...	29-12-2010 at 11:05 by: rrkss
Synthesis of longer chain tertiary alcohols I've successfully synthesized 3-methyl-3-pentanol from ethyl magnesium bromide and ethyl acetate. B ...	29-12-2010 at 09:33 by: rrkss
Sciencemadness at risk -- your help wanted Your transaction ID for this payment is: 1BD88897F2718014D. $25.00 Merry Christmas and best of ...	25-12-2010 at 14:55 by: rrkss
Make Potassium (from versuchschemie.de) I've been looking at smokeless parrafin for tiki torches as a possible solvent. According to the MS ...	25-12-2010 at 14:18 by: rrkss
Possibly a Substitute for Shellsol http://www.homedepot.com/catalog/pdfImages/ab/ab478e2b-db4c-404d-8e43-06ad0670d085.pdf Looks like ...	22-12-2010 at 23:15 by: rrkss
Make Potassium (from versuchschemie.de) [rquote=195566&tid=14970&author=NurdRage][rquote=195563&tid=14970&author=Nicodem] Hi ...	22-12-2010 at 00:00 by: rrkss
Salting out Caffeine I'd use something insoluble in water. Caffeine is very soluble in chloroform and can be used as a s ...	19-10-2010 at 09:49 by: rrkss
Contact dermatits/allergies I had a bad case of contact dermatitis after cleaning something with ethyl acetate. I reccommend a ...	1-10-2010 at 20:42 by: rrkss
Butyric acid from potatoes and water If you can get your hands on 1-propanol. You can always react it with NaBr/H2SO4 to from 1 propyl b ...	28-9-2010 at 10:16 by: rrkss
Nitric Acid Distillation Chemical Cleanup Another easy way is to take some table salt, pour it in and add some ice. Then shake it around. Th ...	18-9-2010 at 23:38 by: rrkss
Nitric Acid Distillation Chemical Cleanup Try a little vinegar. Does a great job making things like this soluble.	17-9-2010 at 10:33 by: rrkss
The short questions thread (3) I use the jkem dvr to regulate my vacuum. Bought one off of ebay. It has two ports on the back. A ...	12-9-2010 at 14:50 by: rrkss
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