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Nitroalkane syntheses ?
If i try to do nitration of butane with NO2 in regular steel pipes can they sustain that for just on ...
21-2-2017 at 17:28
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Ok,when you have calcium ethyl sulfate,how you add sodium carbonate,in solution or in powder form?
...
21-2-2017 at 17:24
by: sulfuric acid is the king
abnormal nitration of styrene
Yes i know for condensation reaction,but i don't have nitroalkanes...
This second reaction that you ...
20-2-2017 at 06:14
by: sulfuric acid is the king
abnormal nitration of styrene
Why not when it's very interesting :D
I though to distill/steam distill to obtain b nitro,but i thi ...
19-2-2017 at 12:16
by: sulfuric acid is the king
abnormal nitration of styrene
More info please.
Physical properties of other products of this reaction etc...
19-2-2017 at 10:37
by: sulfuric acid is the king
Sodium Ethyl Sulfate
I found this "With excess sulfuric acid, the equilibrium can
be shifted to the right."
But how muc ...
19-2-2017 at 03:45
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Really?Nice then...I must try...
I added calcium carbonate but it was mess...
You have good expiri ...
18-2-2017 at 13:16
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Hmmm so you have done it by acid alcohol methode...
Great.But can you tell me some details...Percen ...
18-2-2017 at 08:23
by: sulfuric acid is the king
Sodium Ethyl Sulfate
[rquote=445013&tid=1113&author=JJay]Oh and of course, here is a picture of the crude product ...
18-2-2017 at 07:21
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Where can i get solubility table for NaEtSO4?
Do you have more info now?
16-2-2017 at 16:03
by: sulfuric acid is the king
Sodium Ethyl Sulfate
You got crystals,but i got nothing,and now temperature of the solution is little above zero,and noth ...
16-2-2017 at 15:32
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Near anhydrous,about 15-20C before adding distilled water which was at room temperature.
I will sa ...
16-2-2017 at 14:05
by: sulfuric acid is the king
Sodium Ethyl Sulfate
I am back :D
I had no time for foruming...
Ok,today i made EtSO4 by acid/ethanol mehod,i neutraliz ...
16-2-2017 at 08:08
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Simply.When i said totally used i thought reacted to form ethylsulfuric acid,diethyl sulfate,diethyl ...
15-1-2017 at 15:20
by: sulfuric acid is the king
Sodium Ethyl Sulfate
@JJay
Thanks so much.
Is there any method to know when is sulfuric acid totally used?
And what ab ...
15-1-2017 at 09:00
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Aha,thanks.
But do i need oleum or just concetrated acid,what about ethanol,must be anhydrous or ca ...
14-1-2017 at 16:47
by: sulfuric acid is the king
Sodium Ethyl Sulfate
I have both.
Btw i wonder which method JJay use,'couse of materials...
14-1-2017 at 15:24
by: sulfuric acid is the king
Sodium Ethyl Sulfate
But which method do you use then?

[Edited on 14-1-2017 by sulfuric acid is the king]
14-1-2017 at 05:16
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Bisulfate route is from the patent.
The legend says even hydrated bisulfate takes water from the al ...
13-1-2017 at 16:15
by: sulfuric acid is the king
Sodium Ethyl Sulfate
[rquote=471732&tid=1113&author=JJay]I'm not really sure... I haven't tried it in quite some ...
13-1-2017 at 11:17
by: sulfuric acid is the king
Sodium Ethyl Sulfate
Hmm...So i will need to use vacuum,or some recrystallization...
But i don't have any data on NaEtSO ...
11-1-2017 at 16:11
by: sulfuric acid is the king
Sodium Ethyl Sulfate
I willl make it by neutralizing mix of ethanol/ethylsulfuric acid,then filter off unreacted bicarbon ...
11-1-2017 at 13:41
by: sulfuric acid is the king
Sodium Ethyl Sulfate
[rquote=444964&tid=1113&author=JJay]It looks like I am the only one interested in this topic ...
11-1-2017 at 10:51
by: sulfuric acid is the king

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