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Have any of the sciencemadness members discovered anything?
I was replying (regarding animal testing) to JJay, who had suggested that going from in synthesis, i ...
26-7-2017 at 15:20
by: tsathoggua1
Have any of the sciencemadness members discovered anything?
Well to me, animal testing is extremely unethical especially for that kind of project. They can't co ...
25-7-2017 at 13:27
by: tsathoggua1
Bisulfite adducts, iodide adducts, solubility (ketones, aldehydes)
Whilst I have heard much about the use of bisulfite adducts and to a far lesser degree the use of N ...
24-7-2017 at 13:23
by: tsathoggua1
Wanted-bis-BOC L-arginine, protected at guanidine
Thank you. I'm totally new to peptide sythesis, this would be my first.

I observed an interesting ...
24-7-2017 at 10:58
by: tsathoggua1
Pyrolytic production of scopolamine from OTC precursor
Also, as far as new age bollocks goes, that oil may in fact have some oneirogenic properties.

Bre ...
24-7-2017 at 10:42
by: tsathoggua1
Pyrolytic production of scopolamine from OTC precursor
I could have a crack at this. Not that I'd intend on ingesting more than milligram quantities as an ...
24-7-2017 at 10:14
by: tsathoggua1
Everyday Chemistry
Nothing special.

Got some 1-phenyl-2-nitropropene to recrystallize, that was found quite by chan ...
24-7-2017 at 09:57
by: tsathoggua1
Growing Crystals in Gels
Mercury crystals? presumably its still a liquid in the gel, or a Hg salt, no?

I'd be interested t ...
24-7-2017 at 09:41
by: tsathoggua1
Detritus from Repair tungsten wedding ring
Zed-probably because that dirty allah-loving bastard undoubtedly forced her into 'marriage', along w ...
24-7-2017 at 09:31
by: tsathoggua1
Have any of the sciencemadness members discovered anything?
Also, soon as Tsath' gets some more nitromethane and nitroethane he will be getting to finish up on ...
24-7-2017 at 09:25
by: tsathoggua1
Have any of the sciencemadness members discovered anything?
What about Nurdrage? and both his synthesis/purification of 1,4-dioxane from antifreeze and drain cl ...
24-7-2017 at 09:16
by: tsathoggua1
What have i done
ICl in aqueous solution? how is that even possible? one thing is for pretty much sure, that it is no ...
20-7-2017 at 23:15
by: tsathoggua1
new toys
I'd be interested in tall thin fritted buchners myself.
20-7-2017 at 23:07
by: tsathoggua1
Last chemical order?
ebay, last time, for the THF.
20-7-2017 at 13:11
by: tsathoggua1
Use of K2CO3 instead of pyridine etc. as sacrificial base acid halide Ar-OH
ATM, have no pyridine or 4-DMAP (although the latter is going to be on the shopping list) so organic ...
20-7-2017 at 09:48
by: tsathoggua1
Ultrahigh-purity CHBr3 preparation (interesting use, 1atm synthetic ultrananocrystalline hexagonal diamond
I already have sulfuric better than that (although given the current political climate, with the kne ...
20-7-2017 at 02:19
by: tsathoggua1
Last chemical order?
2.5 liters of THF, some Zn, as fine dust (mesh size unknown, carries a warning about self-heating a ...
19-7-2017 at 04:58
by: tsathoggua1
Ultrahigh-purity CHBr3 preparation (interesting use, 1atm synthetic ultrananocrystalline hexagonal diamond
Alright, so. Last night I read a very interesting article, which I wrote up about and tried to post, ...
19-7-2017 at 04:31
by: tsathoggua1
Hexane as torch fuel?
You might want to avoid hexane actually. n-hexane at least. It is unusually toxic for a hydrocarbon ...
18-7-2017 at 12:33
by: tsathoggua1
lab safety equipment
Well if your brain is desembodied YOU aren't going to do very much with it, unless you were born wit ...
18-7-2017 at 12:25
by: tsathoggua1
eBay seller deschem
How come you prefer the smaller form? I quite like the 24/40 size. although some of mine is in 24/29 ...
18-7-2017 at 12:19
by: tsathoggua1
iodine monochloride (wijs)& trichloroethane1,1,1 UK
Does cooling down make for a good way to precipitate it (either relying on Cl2 stabilization in solu ...
18-7-2017 at 12:15
by: tsathoggua1
Testing Ceramics resistance to acids and bases
If you made HNO3 in-situ from a nitrate and H2SO4, does that not count as mixed acid? You could try ...
18-7-2017 at 09:45
by: tsathoggua1
Sulfuric acid distillation: heating routes?
I'm not surprised your posterior was twitching, situated on a propane burner;) that would make most ...
18-7-2017 at 09:42
by: tsathoggua1
iodine monochloride (wijs)& trichloroethane1,1,1 UK
Don't know about Wijis, but do you mean that the solution doesn't store well? or ICl does not. Mine ...
18-7-2017 at 09:12
by: tsathoggua1
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