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Question about Ullmann type coupling
I'm looking into the feasibility of synthesizing N-(2-carboxyphenyl)glycine from glycine and 2-bromo ... |
31-8-2023 at 13:44
by: tyro |
Acetic anhydride preparation
clearly_not_atara - Apologies for resurrecting a previously disproven route. I've read through this ... |
15-8-2023 at 16:54
by: tyro |
Acetic anhydride preparation
[rquote=684457&tid=9&author=dettoo456][rquote=683127&tid=9&author=BAV Chem][rquote=6 ... |
15-8-2023 at 09:29
by: tyro |
Predictive modeling for electrophilic substitutions
I came across a neat bit of software recently and didn't find any posts about it here. Apologies if ... |
10-7-2023 at 17:23
by: tyro |
Ethyl Pyruvate from Calcium Pyruvate
Hi AvBaeyer!
I certainly have considered this, and it very well may come to that. But, I have the ... |
21-4-2023 at 19:44
by: tyro |
Ethyl Pyruvate from Calcium Pyruvate
I've seen a few threads here which discuss/demonstrate producing ethyl formate without the aid of st ... |
21-4-2023 at 15:11
by: tyro |
Ethyl Pyruvate from Calcium Pyruvate
Hi Boffis! Thanks, this is definitely a tricky one.
With regard to using HCL: I've thought about ... |
20-4-2023 at 07:41
by: tyro |
Preparation of Ketones by Calcium salt Pyrolysis
Thanks for this! I've been interested in pyrolysis reactions in the past. Great to see some well-doc ... |
19-4-2023 at 19:46
by: tyro |
Ethyl Pyruvate from Calcium Pyruvate
I've been working on ways to obtain ethyl pyruvate from calcium pyruvate over the past couple months ... |
17-4-2023 at 20:38
by: tyro |
Nitroethane route
Funny, I posted on this scheme recently.
https://www.sciencemadness.org/whisper/viewthread.php?ti ... |
9-3-2023 at 20:15
by: tyro |
Interesting route to 4-methoxyphenol
@Benignium - I actually found inspiration/motivation to pursue the paracetamol angle from a side not ... |
4-2-2023 at 09:33
by: tyro |
The Kolbe Electrolysis and Organic Electrosynthesis thread
Apologies for resurrecting an absolutely ancient thread.
I wanted to share some information I cam ... |
1-2-2023 at 10:42
by: tyro |
Attempt with acetaminophen
Last weekend I got around to running a trial on the nitrosation and decomposition of acetaminophen i ... |
31-1-2023 at 18:28
by: tyro |
Sodium Borohydride synthesis at room temp
The documentation on the manufacturer's site (Dernord, in this case) rates these pieces at a max of ... |
29-12-2022 at 21:59
by: tyro |
Methyldioxymethylxanthines and MDephedrines
I'm no pharmacokineticist, but I believe it's been stated before: translating functional groups from ... |
28-12-2022 at 22:20
by: tyro |
Preparation of NaBH4
I was investigating a few different routes: milling magnesium, borax, and sodium carbonate in a ball ... |
28-12-2022 at 21:28
by: tyro |
Interesting route to 4-methoxyphenol
Thanks for your reply, clearly_not_atara!
I actually was reading the [url=https://www.sciencemadn ... |
14-12-2022 at 11:28
by: tyro |
Interesting route to 4-methoxyphenol
Apologies, I had a typo and it seems I can no longer edit it. N-nitrosylation should be N-nitrosatio ... |
14-12-2022 at 07:37
by: tyro |
Another potentially interesting route..
I'm currently working out another potentially interesting route to 4-methoxyphenol, starting from p- ... |
12-12-2022 at 23:20
by: tyro |
Interesting route to 4-methoxyphenol
[b]Fery[/b] - Glad you chimed in! I've come across a number of your posts prior to becoming active o ... |
12-12-2022 at 21:21
by: tyro |
A foray into phenethylamines of the Shulgin kind
[quote]
The methylation of 4-methoxyphenol seems to be about as pleasant as methylations get: the p ... |
12-12-2022 at 20:32
by: tyro |
Interesting route to 4-methoxyphenol
The following publication details an approach to the monoetherification of 1,4-hydroquinone and vari ... |
10-11-2022 at 16:49
by: tyro |
p-Toluenesulphonic acid → 4-anisaldehyde
How about the manganese ammonium alum or other elecrolytic methods mentioned in the toluene->benz ... |
8-10-2022 at 09:13
by: tyro |
Sodium Borohydride synthesis at room temp
I'm in the process of prototyping a vibrating ball mill using (relatively) readily available parts, ... |
18-3-2022 at 10:47
by: tyro |
Sodium Borohydride synthesis at room temp
[rquote=671768&tid=158235&author=Mateo_swe]I looked into making Sodium Borohydride using a D ... |
15-3-2022 at 13:49
by: tyro |
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