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doubt about a reaction (alkyl nitrites)
I can confirm that n-butylalcohol works like a charm in making the nitrite ester. So, there must be ...
19-1-2017 at 23:36
by: woelen
re-use NO2 and Cl2
[rquote=472346&tid=71416&author=clearly_not_atara]If your anhydride-forming equation is form ...
19-1-2017 at 23:33
by: woelen
Elemental Thallium under glycerol
Thallium does not react with alcohols. Even with water it hardly reacts. It could be stored under wa ...
19-1-2017 at 14:19
by: woelen
re-use NO2 and Cl2
Well, if you phrase it that way . . .

I would explain it somewhat differently.

A 2 : 1 molar ...
19-1-2017 at 14:12
by: woelen
Elemental Thallium under glycerol
Thallium must be stored under glycerol or some other alcohol. Glycerol is non-volatile, non-toxic, a ...
19-1-2017 at 08:16
by: woelen
Metals in their gaseous states?
What I meant with my remark about colors of gaseous metals is that you will not observe a colored ga ...
18-1-2017 at 01:38
by: woelen
Metals in their gaseous states?
You cannot smell hot gaseous metals. As soon as these metal gases are exposed to cold air, they cond ...
17-1-2017 at 03:40
by: woelen
Diphenylmorpholine's collected organic chem and drug related conjecture threads
You almost certainly will not have a clean alkane solvent. I am quite sure that the mix will contain ...
10-1-2017 at 08:22
by: woelen
Is it possible to make CuCl2 from Chloroform or DCM?
This type of reactions sometimes is useful for making anhydrous, or near anhydrous metal chlorides. ...
10-1-2017 at 08:13
by: woelen
Diphenylmorpholine's collected organic chem and drug related conjecture threads
No one is waiting for this kind of blurp.
Bad grammar, tons of spelling errors, no/poor punctuation ...
10-1-2017 at 00:14
by: woelen
thallium chemistry
The dissolving in hydrochloric acid is easiest, due to complex formation of TlCl4(-). In nitric acid ...
5-1-2017 at 14:23
by: woelen
thallium chemistry
I decided to start the year with some new and uncommon chemistry. I have some thallum(I) nitrate and ...
5-1-2017 at 11:41
by: woelen
synthesis of methyl chloride with phosphorus trichloride
I have tried the chlorination of alkanes (methane, propane, butane) from a flame. It does not work. ...
22-12-2016 at 04:20
by: woelen
EU seller , HNO3, HF etc. via eBay
This seller is around already for quite some time. I'm quite sure it is not a sting, but it is not i ...
20-12-2016 at 23:55
by: woelen
Potassium nitrite solution
Potassium nitrite is much more hygroscpoic than sodium nitrite. If you keep potassium nitrite in con ...
19-12-2016 at 00:00
by: woelen
Heavy metal chlorites
I have left the material to evaporate and dry. A white solid remains behind, but this solid does not ...
18-12-2016 at 05:43
by: woelen
Mad Scientist of the Year Award - some pictures
I received the trophy in good order. Thanks aga!

I made a little wooden shelf so that it can be p ...
18-12-2016 at 05:32
by: woelen
Heavy metal chlorites
Right now, I have the clear liquid, spread out in a petri dish in a dry and fairly warm place (40 C ...
16-12-2016 at 10:09
by: woelen
Heavy metal chlorites
I added some EDA to the remaining amount of my Pb(ClO2)2. I first added the solid to some water and ...
14-12-2016 at 11:06
by: woelen
Heavy metal chlorites
Yeah, you're right. I must have been sleeping while writing the previous post ;)

I will do this e ...
14-12-2016 at 03:00
by: woelen
Bromoacetone from Copper (II) Bromide
The copper is reduced to copper(I) and this apparently forms a complex with acetone.

I think that ...
14-12-2016 at 02:49
by: woelen
Heavy metal chlorites
EDA dichlorite would be very interesting. How would you make this compound? Adding a chlorite salt t ...
13-12-2016 at 10:05
by: woelen
Heavy metal chlorites
The reaction with the hydrazine is not really violent, it just is fast. The yellow solid, when added ...
13-12-2016 at 01:33
by: woelen
Heavy metal chlorites
Right now, I have the Pb(ClO2)2 standing for two weeks and it still is as good as when I made it. Th ...
12-12-2016 at 07:41
by: woelen
Mad Scientist of the Year Award #2
Make it a shared second place! No need to make a clear distinction, we both have done a lot of home ...
10-12-2016 at 14:36
by: woelen
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