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Author: Subject: Is this TNT?
Zyklon-A
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[*] posted on 3-1-2014 at 15:52


Try it again, with a stronger blasting cap of course.



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Turner
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[*] posted on 3-1-2014 at 16:03


Yes, I tried w/ around 100mg of SADS in the cap and only a very small, weak pop was made, I got up and saw bits of TNT and pieces of plastic scattered.



[Edited on 4-1-2014 by Turner]
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DubaiAmateurRocketry
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[*] posted on 3-1-2014 at 16:28


try it again with a larger batch then. With a booster if you can. TNT is an insensitive explosive.
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Zyklon-A
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[*] posted on 3-1-2014 at 16:40


Did you recover any TNT that was scattered from the blast?



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Turner
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[*] posted on 3-1-2014 at 17:18


I need a 1000ml pyrex beakers, I might try a jar but how would this do on a hot plate? I had to dump some remaining acid for the TNT nitration because my beaker got full.

I might try again, but it's so tedious, time consuming and complex making TNT and then worrying if your product is at the correct nitration level.

Here is the video anyways:

<iframe sandbox width="560" height="315" src="//www.youtube.com/embed/_Vvmfkk-fac" frameborder="0" allowfullscreen></iframe>

later this winter I'll do something more.
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Zyklon-A
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[*] posted on 3-1-2014 at 17:59


I've had a household jar crack on a hot plate before, it wasn't a big deal for me, but I wasn't heating explosives. I think you should get a 1000ml pyrex beaker, best to be safe then sorry, if the jar did crack and the TNT spilled on the hot plate it would just catch fire and burn, not explode right?
Here's something that you might want to read, an accident because of faulty glassware, be careful.:)

[Edited on 4-1-2014 by Zyklonb]




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Ral123
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[*] posted on 3-1-2014 at 20:19


I'm sorry for the fail bro, how was your blast cap made?
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Turner
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[*] posted on 3-1-2014 at 20:31


.8g ETN pressed heavily into a plastic tube and .1g SADS pressed on top, fuse sits on this. Didn't get enough acetylide into the cap.
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[*] posted on 4-1-2014 at 02:19


If you've compressed the ETN with a wooden rod and a rubber hammer, that might have made it not go off from the pop of the SADS. I'm not sure if the SADS detonated at all in such small amounts. Did you have tamping above it, like epoxy or some paper piece. Do you suspect lower nitrates in the ETN?
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Turner
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[*] posted on 4-1-2014 at 08:25


I have used a cap with similar configuration before, the SADS is pressed firmly on top of the etn so there is like a pellet of etn and SADS stuck together. I highly doubt lower nitrates of etn. I think there just wasn't enough primary to continue the explosive train.
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Ral123
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[*] posted on 4-1-2014 at 11:18


Bad luck bro.
"Make it strong enough and then make it twice as strong"
-John Moses Browning
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Zyklon-A
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[*] posted on 4-1-2014 at 11:20


Good advice Ral123, make it powerful.

[Edited on 4-1-2014 by Zyklonb]




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bfesser
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4-1-2014 at 11:46
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