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Author: Subject: Acetonitrile form Ammonium acetate
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[*] posted on 15-10-2017 at 17:49


wrt acetonitrile, http://nopr.niscair.res.in/bitstream/123456789/30881/1/IJCT%...

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[*] posted on 10-11-2021 at 12:51


Quote: Originally posted by Formatik  
Quote:
Originally posted by Taoiseach
urea with acetic acid

Is acetic anhydride necessary for this reaction to work?


No, I don't think so. Gmelin says heating urea with AcOH to 110 deg.C. forms acetamide, pitty nothing further like reaction time, extraction, etc. but they reference: M.T. Dangyan (Bull. Armenian Branch Acad. USSR 1942 No. 9/10 (23/4), pg. 53/72), C.A. 1946 3399, and J.M. Das-Gupta (J. Indian Chem. Soc. 10 [1933] 117/23). These references, especially the first should have more details about this process.


Studies on the Decompositions and Reactions of Urea.Part II. Reactions of Urea with Acids , Anhydrides, etc.
By Jnanendra Mohon Das-Gupta.


J. Indian Chem. Soc. 10 [1933] 117

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