arkoma
Forum Redneck
Posts: 1420
Registered: 3-2-2014
Location: Red River Bottoms
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Mood: Grateful passenger of StarShip EARTH
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first dean stark.
Getting a trip phasic liquid in my receiver. Water, "dirty toluene"?, Clean top later?
Top picture my makeshift setup. Clausen just in their to give me more reach.
[Edited on 12-19-2020 by arkoma]
| Quote: | Travel is fatal to prejudice, bigotry, and narrow-mindedness, and many of our people need it sorely on these accounts.
Mark Twain |
I'm with /ORG. Mandatory LSD.
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j_sum1
Administrator
Posts: 5364
Registered: 4-10-2014
Location: Oz
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Mood: It's raining. Not necessarily a metaphor.
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That's one hell of a way to use a Claisen adapter.
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arkoma
Forum Redneck
Posts: 1420
Registered: 3-2-2014
Location: Red River Bottoms
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Mood: Grateful passenger of StarShip EARTH
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it works!! I've gotten pretty creative with my kit over the years.
| Quote: | Travel is fatal to prejudice, bigotry, and narrow-mindedness, and many of our people need it sorely on these accounts.
Mark Twain |
I'm with /ORG. Mandatory LSD.
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karlos³
International Hazard
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Registered: 10-1-2011
Location: yes!
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Mood: verrückt & wissenschaftlich
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Agreed, thats pretty creative and looks really adventurous.
But hey as long as it works?
Did you write "its not a meth lab" on the whiteboard in the background? 
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arkoma
Forum Redneck
Posts: 1420
Registered: 3-2-2014
Location: Red River Bottoms
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Mood: Grateful passenger of StarShip EARTH
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Very astute observation! It's not a meth lab. Any "meth cooks" I ever knew were working with coffeepots, duct tape, garden hose and kitty litter.
They certainly don't have a Corning PC-351!
This Dean-Stark all of a sudden makes sense to me now of how its yanks the water, after sitting here and watching it. Running Dougs Lab procedure for
p-toluenesulphonic acid. another 45 minutes of reflux.....hopefully. Still getting some water coming over.
| Quote: | Travel is fatal to prejudice, bigotry, and narrow-mindedness, and many of our people need it sorely on these accounts.
Mark Twain |
I'm with /ORG. Mandatory LSD.
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RustyShackleford
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Registered: 10-12-2020
Location: Northern Europe
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I used the setup here on the right for the same reaction. It worked and quite well, but it was some hassle getting the temperature right so it was
nicely flowing through the side arm and not bubbling and stuff.
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arkoma
Forum Redneck
Posts: 1420
Registered: 3-2-2014
Location: Red River Bottoms
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Mood: Grateful passenger of StarShip EARTH
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Well, I've got a yield. Working up now.
| Quote: | Travel is fatal to prejudice, bigotry, and narrow-mindedness, and many of our people need it sorely on these accounts.
Mark Twain |
I'm with /ORG. Mandatory LSD.
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SuperOxide
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Registered: 24-7-2019
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Damn, that's genius! lol. I was tempted to buy a DS apparatus, but I think your setup may suffice for my setup, haha.
I didn't even notice that was there, lol. I thought it was just a short straight glass piece. But it looks closed off.
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Fyndium
International Hazard
Posts: 711
Registered: 12-7-2020
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Well, that trap at least has decent volume for larger extractions.
It's funny how one can build up pretty much any kind of apparatus imaginable with all the glass parts there are.
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