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Author: Subject: Phenyloxlate ester
darkflame89
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[*] posted on 3-4-2004 at 00:17
Phenyloxlate ester


Anyone knows how i can synthesise phenyl oxalate ester from OTC materials?? Thz in advance



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The_Davster
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[*] posted on 3-4-2004 at 10:26


I'm not sure on this but could one may be able use aspirin, sulfuric acid and oxalic acid. Using a standard esterfication reaction procedure. however I am not sure that the other functional groups on aspirin's benzene ring would be removed.
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Marvin
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[*] posted on 3-4-2004 at 21:19


The reaction generally used is phenol + oxalyl chloride together with a non water producing base like diethylamine. Reactions of this nature are used to make the active compounds in lightsticks.
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darkflame89
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[*] posted on 4-4-2004 at 00:29


Yep thats want i want to do..Make my own lightsticks:D! But unfortunately i can't find phenols and such organic compounds. Sigh, i will have to shelve this idea:(



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