Mailinmypocket
International Hazard
Posts: 1351
Registered: 12-5-2011
Member Is Offline
Mood: No Mood
|
|
Looking for Phenol
My eBay source for phenol has went dry  does anyone here in Canada have a source
for phenol to refer me to? The chemical suppliers that deal with individuals don't carry it sadly. If anyone has the ability to purchase it and is
willing to forward it to me that could also be an option, for a surcharge for the trouble of course!
Thanks!
|
|
|
plante1999
International Hazard
Posts: 1936
Registered: 27-12-2010
Member Is Offline
Mood: Mad as a hatter
|
|
Well, if you like to make your own reagents, go buy a large bottle of aspirin (or buy sodium salicylate on ebay(cheaper)). And dry distill with sodium
hydroxide in a stochiometrical excess, you should get crude phenol, you can then purify by standard mean. Decarboxylation of salicylate is known, I
don't have a reference for it taught.
Hope it helped you somewhat.
I never asked for this.
|
|
|
Mailinmypocket
International Hazard
Posts: 1351
Registered: 12-5-2011
Member Is Offline
Mood: No Mood
|
|
Quote: Originally posted by plante1999  | Well, if you like to make your own reagents, go buy a large bottle of aspirin (or buy sodium salicylate on ebay(cheaper)). And dry distill with sodium
hydroxide in a stochiometrical excess, you should get crude phenol, you can then purify by standard mean. Decarboxylation of salicylate is known, I
don't have a reference for it taught.
Hope it helped you somewhat. |
Thanks! I do know of that route to phenol, and I do enjoy making my own reagents, but for phenol I just prefer buy it. I need about 250g or so for a
few runs making salicylaldehyde which will take enough time in itself. Making that much from salicylates would be a pain, and phenol is pretty cheap
too.
|
|
|
Vargouille
Hazard to Others
Posts: 380
Registered: 16-4-2012
Member Is Offline
Mood: No Mood
|
|
If you have a source of chlorobenzene, you could react that with sodium hydroxide to get your phenol. A procedure shouldn't be too hard to find.
|
|
|
Mailinmypocket
International Hazard
Posts: 1351
Registered: 12-5-2011
Member Is Offline
Mood: No Mood
|
|
| Quote: Originally posted by Vargouille | | If you have a source of chlorobenzene, you could react that with sodium hydroxide to get your phenol. A procedure shouldn't be too hard to find.
|
No chlorobenzene either, damn! Just found one eBay person that sells it 15$/15g, that's stupid, as if anyone would buy phenol at that price.
|
|
|
AndersHoveland
Hazard to Other Members, due to repeated speculation and posting of untested highly dangerous procedures!
Posts: 1986
Registered: 2-3-2011
Member Is Offline
Mood: No Mood
|
|
Looking for "fenol", you say?
Why, it's growing everywhere !
http://sphotos-b.xx.fbcdn.net/hphotos-snc6/8069_349283741816... 
[Edited on 17-3-2013 by AndersHoveland]
|
|
|
DraconicAcid
International Hazard
Posts: 4279
Registered: 1-2-2013
Location: The tiniest college campus ever....
Member Is Offline
Mood: Semi-victorious.
|
|
Isn't that fennel? You should never confuse phenol with phenyl.
Please remember: "Filtrate" is not a verb.
Write up your lab reports the way your instructor wants them, not the way your ex-instructor wants them.
|
|
|
Steve_hi
Hazard to Others
Posts: 196
Registered: 4-12-2010
Member Is Offline
Mood: No Mood
|
|
https://www.elementalscientific.net/store/scripts/prodList.a...
I just ordered some from elemental but I live near the border and pick it up down there it took those guys 3 weeks to ship it
I have 4oz comming.
They will ship into Canada but you have to phone and make arraingments. also I had to pay an additional 17.00 hazard shipping charge on top of the
dhipping charge
Qty Item Description Sub Total
1 CH6321-16 POTASSIUM CHLORIDE USP CRYSTALS, 16 oz. - $6.95
$6.95
1 CH1217-16 ALCONOX DETERGENT, 16 oz. - $8.00
$8.00
1 CH1031-16 ACETIC ACID GLACIAL, 16 oz. - $8.90
$8.90
1 CH2115-16 BOILING STONES, 16 oz. - $11.70
$11.70
2 CH5330-1 MERCURY METAL DISTILLED, 1 oz. - $7.50
$15.00
1 CH6066-16 PHOSPHORIC ACID REAGENT ACS 85%, 16 oz. - $9.25
$9.25
1 CH6430-16 POTASSIUM HYDROXIDE FLAKES, 16 oz. - $10.00
$10.00
1 CHV1139-4 METHYL-TERT BUTYL ETHER ACS, 4 oz. - $9.90
$9.90
1 CH4631-16 LACTIC ACID 85% PURIFIED, 16 oz. - $13.30
$13.30
1 CH3992-16 FORMIC ACID, 90% 16 oz. - $20.50
$20.50
1 CH2050-4 BENZOIC ACID CRYSTALS USP, 4 oz. - $6.99
$6.99
1 CH6112-4 PHTHALIC ACID ANHYDRIDE, 4 oz. - $9.65
$9.65
1 CH8309 TITANIUM METAL - $5.00
$5.00
1 CH6014-4 PHENOL CRYSTALS ACS, 4 oz. - $21.00
$21.00
Sub Total: $156.14
Shipping: $20.76
Tax: $0.00
*Adjustment: $17.00
Sub Total: $193.90
Total: $193.90
[Edited on 18-3-2013 by Steve_hi]
[Edited on 18-3-2013 by Steve_hi]
|
|
|
Mailinmypocket
International Hazard
Posts: 1351
Registered: 12-5-2011
Member Is Offline
Mood: No Mood
|
|
Oddly enough I have already contacted them and they told me that the hazardous materials I ordered (phenol being one of them) cannot be shipped to
Canada even for an extra fee. This was by email though and I never spoke to them on the phone, maybe I should try again...
|
|
|
![[*]](images/xpblue/default_icon.gif){kind=icon}
