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Author: Subject: Ethylenediamine diacetic acid
Waffles SS
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[*] posted on 18-9-2013 at 21:09



Quote:

Another suitable method for the preparation of 2-imidazolidone,affording excellent yield on a laboratory scale,is based on the interaction of ethylenediamine with urea in the presence of water as a moderator.also, the interaction of ethylene glycol with urea leads to the formation of 20imidazolidone.
The reaction is best carried out in two steps.First, a mixture of ethylene glycol and an excess of urea is heated gradually from 150 to 240 during a period of several hours. Ammonia and carbon dioxide are evolved and a brittle resinous solid is obtained.Hydrolysis with water at 250c converts this material into 2-imidazolidone.

The Chemistry of Heterocyclic Compounds, Imidazole and Its Derivatives By Klaus Hofmann,p.227

Is there any easier way for preparing Imidazolidone?What is method for converting Imidazolidone to ethylenediamine or Ethylenediamine diacetic acid?
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