thesmug
Hazard to Others
Posts: 370
Registered: 17-1-2014
Location: Chicago, Il (USA)
Member Is Offline
Mood: No Mood
|
|
Chromatography jars
I was looking online for easier methods of doing chromatography since right now I use tall beakers with a pencil and a piece of string and I was
always considering actual chromatography jars but they cost over $1000! Why are they so expensive and is there any place to get them where they aren't
so expensive?
|
|
|
Hockeydemon
Hazard to Others
Posts: 218
Registered: 25-2-2013
Member Is Offline
Mood: No Mood
|
|
If you're referring to the chromatography jar that's listed on amazon it has to be a mistake. There is really no reason for you to even bother buying
a chromatography jar anyways. Any jar will work just fine. If you need something more precise invest in a different technique. You're not going to
gain any noticeable precision by buying a jar designed for chromatography.
I am curious what you mean when you say you're using a pencil and a piece of string though.
BTW Dr.Bob sells chromatography chambers for $20 on here.
[Edited on 11-3-2014 by Hockeydemon]
|
|
|
J2xP
Harmless
Posts: 21
Registered: 14-1-2014
Member Is Offline
Mood: No Mood
|
|
Hockeydemon is right...there is no magic to regular jars vs. chromatography jars. The price is due to manufacturers capitalizing on the fact that is a
"speciality item" so they mark it up insanely. I have chromatography jars (square and cylindrical) for sale cheap but as previously stated any jar
will yield the same results.
|
|
|
Dr.Bob
International Hazard
Posts: 2660
Registered: 26-1-2011
Location: USA - NC
Member Is Offline
Mood: No Mood
|
|
I agree with everyone here. The only special thing about chromatography jars is a flat bottom is best and an easy way to close it, preferable without
threads, as often plates sometimes move around when you try to take off the lid. I often use a simple tall crystallizing disk type jar (straight
sides and flat bottom) and then put an upside down lid on the top, just to keep the solvent from evaporating. But simple TLC jars are $10 or so,
depending on the TLC slide size. I do find a piece of filter paper on the bottom helps to keep the slide from moving around.
|
|
|
thesmug
Hazard to Others
Posts: 370
Registered: 17-1-2014
Location: Chicago, Il (USA)
Member Is Offline
Mood: No Mood
|
|
Quote: Originally posted by Hockeydemon  |
I am curious what you mean when you say you're using a pencil and a piece of string though.
[Edited on 11-3-2014 by Hockeydemon] |
I lay a pencil across the top of the beaker, thread a string through the chromatography paper and tie the string around the pencil. The reason I
wanted an actual chromatography jar is that I've seen them that have a glass bar across the inside that you can suspend the chromatography paper from.
|
|
|
Dr.Bob
International Hazard
Posts: 2660
Registered: 26-1-2011
Location: USA - NC
Member Is Offline
Mood: No Mood
|
|
So you are doing paper chromatography, I guess. You could form the piece of paper into a curl, then stand it on end as well. The key is to cover
the container to keep the solvent from evaporating off of the plate or paper, as the normally improves the chromatography.
|
|
|
thesmug
Hazard to Others
Posts: 370
Registered: 17-1-2014
Location: Chicago, Il (USA)
Member Is Offline
Mood: No Mood
|
|
| Quote: Originally posted by Dr.Bob | | So you are doing paper chromatography, I guess. You could form the piece of paper into a curl, then stand it on end as well. The key is to cover
the container to keep the solvent from evaporating off of the plate or paper, as the normally improves the chromatography. |
I've thought of that but my chromatography paper comes in rolls of strips, each 2cm wide. Sitting them on their side would make for a very quick
chromatography session!
|
|
|
![[*]](images/xpblue/default_icon.gif){kind=icon}
