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Author: Subject: organic chemistry thioester preparation
ramarao
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[*] posted on 23-9-2006 at 18:53
organic chemistry thioester preparation


I would like to prepare thioester of (2-aminothiozolyl )-2-methoxycarbonyl-methoxyimino-3-oxobutanoic acid with Dibenzothiozole disyulphide,using Triethylphosphite as catalyst/oxygen scavenger.Could any one please help me with operating parameters to get highest yield without any residue of TEP oxide in the product.
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