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Author: Subject: Potassium Perchlorate from Potassium Chlorate
symboom
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[*] posted on 8-1-2017 at 18:15
Potassium Perchlorate from Potassium Chlorate


So ive performed the reaction of porassium peroxymonosulfate
(Oxone) non chlorine bleach and formed this percipitate along with a chlorine smell to the reaction

What else could be used to oxidize potassium chlorate to perchlorate

Ive read that silver oxide supposedly works also

Supposedly hydrogen peroxide also works havnt found anyone trying to chemically oxidize chlorate



[Edited on 9-1-2017 by symboom]
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[*] posted on 9-1-2017 at 09:15



Quote:
What else could be used to oxidize potassium chlorate to perchlorate



http://people.ku.edu/~matt915/projects/chloratedecomp.html

Thermal decomposition of chlorate to perchlorate.




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[*] posted on 10-1-2017 at 00:28


Thank you very much also shows it being made from potassium chlorate
https://m.youtube.com/watch?v=EC4OPnvPkLU
I dont know how I miss this video when I was searching


[Edited on 10-1-2017 by symboom]
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[*] posted on 10-1-2017 at 01:15


I would prefer the anodic oxidation of conc. kClO3 solution This is easy. Hold the conc solution temp. betw. 30-40 C deg. during the process and use suitable anode. After the process cooling the solution in fridge, the perchlorate cristall will be falling like snowflake alow of dish. You get pure KClO4 by filtration.
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[*] posted on 10-1-2017 at 03:03


Xenon trioxide



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