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Forbidden Knowledge!
For the most, this "forbidden chemistry" you're talking about is just mundane chemistry employed ont ... |
23-6-2020 at 07:20
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
@Tsjerk Great write-up man. I must admit it's a bit disappointing to hear that even though you seeme ... |
23-6-2020 at 06:25
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
[rquote=638817&tid=155581&author=Boffis]...[/rquote]
As for the solid that formed after add ... |
20-6-2020 at 04:53
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
[rquote=638757&tid=155581&author=Tsjerk]I had such a great idea... only the execution was a ... |
20-6-2020 at 00:26
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
[rquote=638651&tid=155581&author=Tsjerk]With a bit of luck I can try this reaction tomorrow, ... |
18-6-2020 at 07:11
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
Well, the DCM nitration didn't went very well to say the least.
I started by mixing 0.2n of KNO[sub ... |
17-6-2020 at 12:20
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
[rquote=638457&tid=155581&author=Boffis]@B.D.E; I am currently trying to prepare 2-amino-4-c ... |
16-6-2020 at 04:09
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
[rquote=638337&tid=155581&author=njl]I don't remember the yield but I left the solution of d ... |
15-6-2020 at 02:49
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
[rquote=638289&tid=155581&author=Tsjerk]Have you seen the HNO3 in DCM nitration of toluene? ... |
14-6-2020 at 09:58
by: B.D.E |
ortho nitration of p-toluenesulfonic acid(QUESTIONS)
Hey there 
I just made some p-TsOH*H[sub]2[/sub]O, and I'm hoping on nitrating its ortho positi ... |
14-6-2020 at 01:48
by: B.D.E |
My new lab
[rquote=637615&tid=155528&author=Bedlasky]
Elephant toothpaste with NaOCl? This doesn't wor ... |
6-6-2020 at 09:41
by: B.D.E |
My new lab
my first home experiment was to simply make concetrated NaOH solutions and putting stuff into it. fl ... |
4-6-2020 at 10:09
by: B.D.E |
Alternative Solvents and New Solvents - General Discussion
[rquote=114678&tid=9757&author=pantone159]I was told once that hexane is significantly more ... |
12-5-2020 at 02:13
by: B.D.E |
Anthranilic acid preparation(questions)
[rquote=635661&tid=155329&author=S.C. Wack][rquote=635649&tid=155329&author=B.D.E]wh ... |
11-5-2020 at 13:33
by: B.D.E |
Anthranilic acid preparation(questions)
[rquote=635639&tid=155329&author=Tsjerk]As long as the extracts from the ether extraction ar ... |
9-5-2020 at 10:40
by: B.D.E |
Anthranilic acid preparation(questions)
[rquote=635628&tid=155329&author=Tsjerk]Very nice, I already thought hypobromite should work ... |
9-5-2020 at 07:06
by: B.D.E |
Anthranilic acid preparation(questions)
Okay, so I ran the synthesis on a small scale(4.19gr of phthalamide), and it worked great :[color=Bl ... |
9-5-2020 at 04:03
by: B.D.E |
Anthranilic acid preparation(questions)
wow. I'm overwhelmed by the amount of people willing to spare from their time just to help a strange ... |
7-5-2020 at 04:10
by: B.D.E |
Anthranilic acid preparation(questions)
P.S. I already tried the reaction using 3% household bleach(presumably without any additives), and i ... |
6-5-2020 at 03:26
by: B.D.E |
Anthranilic acid preparation(questions)
hey there, I've read some thread about it. I also watched chemplayer video about the syntheses. I st ... |
6-5-2020 at 03:21
by: B.D.E |
Importing Sodium nitroprusside
oh and in case it easn't clear, the question is - should I be worried about ordering it?(i.e is the ... |
26-4-2020 at 13:18
by: B.D.E |
Importing Sodium nitroprusside
Hey there, I'm considering ordering some sodium nitroprusside(Na2[Fe(CN)5NO]), but I'm a bit worried ... |
26-4-2020 at 11:22
by: B.D.E |
Q: Making sodium cyanide from sodium cyanate and sodium metal
[rquote=633271&tid=155046&author=PirateDocBrown]B.D.E, what are you using to heat your cruci ... |
3-4-2020 at 09:08
by: B.D.E |
Q: Making sodium cyanide from sodium cyanate and sodium metal
[NEVERMIND]
[Edited on 28-3-2020 by B.D.E] |
28-3-2020 at 02:34
by: B.D.E |
Q: Making sodium cyanide from sodium cyanate and sodium metal
Some more crystals after cooling the solution:
[file]80070[/file]
Final yield isn't great(55% ba ... |
27-3-2020 at 02:33
by: B.D.E |
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