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Cubic acetone peroxide crystals
Dear all,

I just was unpacking some boxes in my basement and I found a shoebox which contained a ...
27-12-2009 at 06:21
by: DNA
lithiation of 8-bromoquinoline
Does anyone know what possibly could happen here.
Concerning the mechanism.

[img]http://www.foto ...
5-8-2009 at 00:55
by: DNA
new phenethylamine?
Does anyone know if from a nitrone one could form a salt?
Like when you would form the nitrone with ...
6-4-2009 at 01:18
by: DNA
new phenethylamine?
Not if you look at the ceised drug labs then most of them 90% uses phenylacetone, but anyway I don't ...
2-4-2009 at 06:11
by: DNA
new phenethylamine?
Or you could insted of making the oxime by hydroxylamine use o-methoxyhydroxylamine immediately.
Sa ...
1-4-2009 at 23:55
by: DNA
new phenethylamine?
Does anyone know of the existance of the following compound has it ever been tested or made?

Inst ...
1-4-2009 at 04:44
by: DNA
Nitromethane HE purity required
Concerning the plx it is actually not that insensitive...
I've done quite a lot of experiments conc ...
26-3-2009 at 01:13
by: DNA
Zinc reduction for 2C-H from nitrostyrene
No it is not enough vacuum to distill 2C-H.
I don't know the boiling point by heart but you can loo ...
5-3-2009 at 00:19
by: DNA
strange (?) results from nitrating toluene
Why would you want to seperate the isomers at all when making trinitrotoluene.
Just nitrate it so y ...
17-2-2009 at 05:44
by: DNA
Zinc reduction for 2C-H from nitrostyrene
I think it would be nice actually to steam distill the freebase directly out of the reaction mixture ...
17-2-2009 at 05:34
by: DNA
Unconventional Shaped Charges
You also need to look into what you want to achieve, in a very hard material it is hard to drill a h ...
17-2-2009 at 04:55
by: DNA
Unconventional Shaped Charges
I know of the experiment of AXT, but I mean is there any info about the glass thickness from AXT him ...
16-2-2009 at 02:21
by: DNA
Unconventional Shaped Charges
I've read the entire thread, and also done quite some reading about glass liners.
I was just wonder ...
10-2-2009 at 08:56
by: DNA
Unconventional Shaped Charges
Isn't there any more information available about the glass liners?
I am about the have some conical ...
10-2-2009 at 04:55
by: DNA
Leuckart reaction
Vogelzang, haven't you got any recent literature....the newest article you posted is from 1951, not ...
28-1-2009 at 00:24
by: DNA
Unconventional Shaped Charges
Is there any more info available about the glass liners for conically shaped charges.
AXT I also se ...
12-1-2009 at 07:23
by: DNA
6-Bromo-1-hexanol synthesis
NBS in DMF works also really well to selectively bromate compounds in my experience.
30-10-2008 at 00:31
by: DNA
liquid liquid seperation
Column Chromatography would do a great job, although would be quite expensive and time-consuming (st ...
30-10-2008 at 00:29
by: DNA
Buchi Rotavapor R for sale (from Europe) with pump, vac controller, stand etc.!
This is from the buchi website, does anyone know why to add borax to distilled water?

[quote]Heat ...
22-10-2008 at 04:35
by: DNA
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
Concerning the 2,5-dimethoxynitropropene apparantly the reduction of it with BF3.Et2O and NaBH4 (à ...
21-10-2008 at 02:12
by: DNA
100% yield
Just found this topic and wanted to report that *I* got an excellent 100% yield on the 2,5-dimethoxy ...
17-10-2008 at 01:18
by: DNA
hotplate/stirrer
Yes and No,
I did order to products from the same brand, but the magnetic stirrer I have is quite o ...
13-10-2008 at 00:09
by: DNA
hotplate/stirrer
No no the top picture I showed is the DIN plug I wanted to show so it is clear that I mean the plug ...
10-10-2008 at 03:57
by: DNA
hotplate/stirrer
Dear all,

I've got a problem with a IKA hotplate/stirrer combination.

This thing has a DIN out ...
9-10-2008 at 06:49
by: DNA
300 deg/C oil bath
I was just about the ask the same question (no not about the sigarettes), I've tried to do a ultra-m ...
9-10-2008 at 00:33
by: DNA
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