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Failed distillation of HNO3 from KNO3 ??
Should I start a new thread? Since this went from a failed distillation to figuring out a mystery ox ...
23-3-2023 at 12:32
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
So I made some flash powder 5:3:2 - Ox:Al:S and hit a little pinch of it with a hammer and now my ea ...
23-3-2023 at 11:52
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
No reaction with hot NaOH or NaOCl, not sure what other chemicals I have that I can test it with. I ...
23-3-2023 at 11:41
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
I should note that the white fumes did not evolve until after strong heating. At room temp there's n ...
23-3-2023 at 08:51
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
Definitely not KClO3, that immediately reacts to form HClO3 which is unstable and yields bright yell ...
23-3-2023 at 07:59
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
I did a bunch of small scale tests which ended up leaving me even more confused...

These were don ...
23-3-2023 at 07:28
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
So the "KNO3" is barely soluable in water both before and after the reaction. I noticed the slurry g ...
22-3-2023 at 20:59
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
I will have to check it when I get home from work in a couple hours.
22-3-2023 at 17:29
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
It's a popular source among amatures. I've used it for other experiments and it works great.

I t ...
22-3-2023 at 17:03
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
I was just trying to find a target that gave a KNO3 value similar to what I used to see how much H2S ...
22-3-2023 at 16:46
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
Head temp. Meant to put that in the original post..

[Edited on 3-23-2023 by Gammatron]
22-3-2023 at 16:42
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
If I put a target of 250ml of 90% HNO3 into the calculator it gives me very close values to what I u ...
22-3-2023 at 16:34
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
I know... I say this with shame "Honestly I didn't even check the ratio." Cause now I probably just ...
22-3-2023 at 15:20
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
Honestly I didn't even check the ratio. I just had that in my notes that I copied from an old nile r ...
22-3-2023 at 14:43
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
I believe this particular batch came from a fireworks supply store but I also have a bunch that I bo ...
22-3-2023 at 13:16
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
KCl has an immediate reaction with H2SO4 at room temp producing a lot of bubbles. There was no perce ...
22-3-2023 at 11:04
by: Gammatron
Failed distillation of HNO3 from KNO3 ??
So this morning I attempted a distillation of HNO3 using 550g of KNO3 and 300ml of rooto H2SO4 in a ...
22-3-2023 at 08:24
by: Gammatron
Homemade and Repurposed Lab Gear
Thanks! There is a thermostat which I have set to the lowest temperature but I found that If I bypas ...
4-12-2022 at 16:30
by: Gammatron
An effective method for stipping uranyl nitrate from TBP
Also I have written about my extraction process on my WordPress site if anyone is interested but it' ...
30-11-2022 at 19:01
by: Gammatron
An effective method for stipping uranyl nitrate from TBP
I got the TBP from a buddy who is a professional chemist but I'm not sure where he got it from, the ...
30-11-2022 at 18:59
by: Gammatron
Catboy Chemical Society
How about gigachad chemical society
30-11-2022 at 07:03
by: Gammatron
Homemade and Repurposed Lab Gear
I'll be interested to see how that turns out, I have a bunch of those and old HHD's are cheap too.
24-11-2022 at 05:59
by: Gammatron
Protecting vacuum from H2SO4 vapors?
You can buy PTFE tubing really cheap on eBay, I've used it for distilling HF at over 200C with 0 iss ...
16-11-2022 at 06:20
by: Gammatron
Question on hammer mill construction
I am about to start working on a small hammer mill for crushing ore; there are two designs I see a l ...
25-10-2022 at 12:49
by: Gammatron
An effective method for stipping uranyl nitrate from TBP
When using tributyl phosphate to extract uranium it takes several washings to recover the uranyl nit ...
20-10-2022 at 20:37
by: Gammatron
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