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Storage of Fuming Nitric acid
Wait till the 2nd of August (my birthday- im getting a digi cam)!!!
Which experiment did you perf ...
20-6-2009 at 13:55
by: Saber
Storage of Fuming Nitric acid
Someones a fan of FEP bottles i see ;)
I will try get one of those bottles and try em out. I admit ...
18-6-2009 at 06:35
by: Saber
Storage of Fuming Nitric acid
I was thinking of making around 250ml of FNA at a time to store.
Does RFNA have different nitrating ...
15-6-2009 at 09:41
by: Saber
Storage of Fuming Nitric acid
Thanks for all your replys,
@ Picric-A - If you hadnt picked up fag ends and read the rest the res ...
14-6-2009 at 11:40
by: Saber
Storage of Fuming Nitric acid
Every time I required Fuming nitric acid in the past, I would make it in situ by distill a mix of Na ...
12-6-2009 at 13:31
by: Saber
Anhydrous Diethyl Ether via NaOH?
Small ultrasonic baths can be bought off ebay for around £10.
They can be modified to make larger ...
12-6-2009 at 02:14
by: Saber
Anhydrous Diethyl Ether via NaOH?
Firstly Sodium is not a compound.
Secondly anhydrous Sodium hydroxide does suffice for drying ether ...
5-6-2009 at 07:31
by: Saber
Hydrogen peroxide synthesis - 2-ethyl-9,10-dihydroxyanthracene
Sweet, thanks Formatic and unionised! great patents!
@unionised- google translate worked perfectly ...
1-6-2009 at 10:31
by: Saber
Hydrogen peroxide synthesis - 2-ethyl-9,10-dihydroxyanthracene
@-TheMadMen- Sorry I must of put my question out badly in the beginning, I am not at all interested ...
31-5-2009 at 10:40
by: Saber
Lab prep of Dimethyl Urea
Has anybody found a lab prep of Dimethyl urea?
I presume reating urea with Dimethyl Sulphate wont d ...
15-5-2009 at 12:56
by: Saber
H2O2 by ozone -- The slow method.
At current i will not be able to upload any pictures as i do not own a camera, I will though asap.
...
9-5-2009 at 08:26
by: Saber
H2O2 by ozone -- The slow method.
Preparing Oleum on tap is extremely useful however there is only so much oleum you can use, so I nev ...
8-5-2009 at 23:19
by: Saber
H2O2 by ozone -- The slow method.
For ozone generation, yields are greatly increased by using a negative corona discharge.
Keep temps ...
8-5-2009 at 11:45
by: Saber
Black Phosphorus
Black P is rather expencive to buy.
One can make it however, simply use a the apparatus used to pro ...
8-5-2009 at 02:16
by: Saber
Hydrogen peroxide synthesis - 2-ethyl-9,10-dihydroxyanthracene
I am a fan of taking industrial procedures and downsizing them to lab size for producing extremely u ...
5-5-2009 at 12:03
by: Saber
Mentos + Coca Cola Light
Mentos react with Coke (generally) becuase it has a highly porous surface and that surace catalyses ...
29-4-2009 at 12:21
by: Saber
Methylation agents
Here is a source which states diethyl oxalate is a good alkylating agent, I will have a look at my p ...
29-4-2009 at 11:59
by: Saber
Chemistry-related photography
Could anybody in England reccomend a decent easy to use camera?
I plan on taking photos and posting ...
29-4-2009 at 11:30
by: Saber
Methylation agents
I am going to try some methylations in the near future.
the bonus with dimethyl oxalate is it is ea ...
29-4-2009 at 11:26
by: Saber
Methylation agents
There have been posts of using dimethyl oxalate as a safe methylating agent.
I am unsure as to how ...
29-4-2009 at 10:51
by: Saber
Methylation agents
WHY THE CAPITALS?!
Both will work, the only reason methyl iodide is preferred is its a liquid at rt ...
29-4-2009 at 10:40
by: Saber
KN03 ---- or not???
how fine was the sugar you mixed it with?
Normally you either mix it with icing sugar or melt granu ...
8-9-2008 at 05:23
by: Saber
Acetonitrile form Ammonium acetate
I want to do this just for fun. I can buy Acetamide and acetonitrile quite cheap however i love maki ...
8-9-2008 at 01:07
by: Saber
Acetonitrile form Ammonium acetate
I built it out of glass. It uses a Vanadium pentoxide, K2SO4 catalyst mounted on silica.
I unfortun ...
7-9-2008 at 13:17
by: Saber
Acetonitrile form Ammonium acetate
What about using a cheaper dehydrating material, eg Oleum?
I have my own mini contact process machi ...
7-9-2008 at 12:12
by: Saber
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