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Boron Tribromide from Boron and Bromine in grey iron pipe?
Would this work? Or the pipe would explode from bromine pressure?
16-10-2014 at 11:35
by: bmays
Will glacial acetic acid esterify testosterone?
"Heptanoic acid is used to esterify steroids in the preparation of drugs such as testosterone enanth ...
3-10-2014 at 21:35
by: bmays
Help with bromine from bromate
I apologize for that, it is sodium bromide i have from the pool supply. I was looking at a jar of so ...
7-4-2014 at 18:35
by: bmays
Help with bromine from bromate
I would like a small bit of bromine for a bromination. I will use the sodium bromate, potassium perm ...
6-4-2014 at 16:40
by: bmays
Makeshift polarimeter construstion issue.
I am trying to crudely observe optical rotation by using light from an lcd monitor and some salvaged ...
17-3-2014 at 23:53
by: bmays
Chloroethane synth from methanol
CH3OH + PCl5 = HCl + CH3Cl + POCl3

I think chlorine gas and a catalytic amount of red phosphorous ...
1-12-2013 at 12:01
by: bmays
"Nascent Iodine" "Atomidine"
[quote]Nascent iodine is formed when the iodine molecule is broken down to produce charged iodine at ...
20-10-2013 at 20:10
by: bmays
Tetraethyl lead synthysis with lithium lead alloy?
4NaPb + 4CH3CH2Cl → (CH3CH2)4Pb + 4NaCl + 3Pb

I see no reason the reaction will not pro ...
9-8-2013 at 16:07
by: bmays
Interchanging salt forms of a compound.
Say you have quinidine (random choice) acetate, if you add a stronger acid like hbr will it become q ...
9-6-2013 at 21:43
by: bmays
Preperation of HBr in acetic acid.
NaBr does not seam to react with an oxalic acid and sodium bisulfite. Does it require heating for HB ...
6-6-2013 at 17:48
by: bmays
Preperation of HBr in acetic acid.
Oh, i see. Then i will make an 50% aqueous HBr solution first using my NaBr, the diluted H2SO4 will ...
12-5-2013 at 13:27
by: bmays
Preperation of HBr in acetic acid.
I need to prepare a 15% solution. I think i will use NaBr and H2SO4, this should make HBr and Br2 wh ...
11-5-2013 at 23:30
by: bmays
Calcium sodium phosphosilicate synthesis?
Yes, thanks.
14-2-2013 at 03:26
by: bmays
Calcium sodium phosphosilicate synthesis?
Anyone have any idea how this would be synthesized?

[Edited on 12-2-2013 by bmays]
12-2-2013 at 03:53
by: bmays
F- From Tap Water?
According to my research and observation ingesting fluorine in any way is bad. No matter if it is a ...
12-2-2013 at 03:51
by: bmays
Good materials for a small vial based ball mill?
I am milling down a water insoluble hormone to create a suspension of particles in water with tween ...
3-2-2013 at 15:55
by: bmays
Good materials for a small vial based ball mill?
Is incredibly clumpy in a mortar and pestle, impossible without water even in ball mill. Would take ...
29-1-2013 at 13:51
by: bmays
Good materials for a small vial based ball mill?
I am having trouble making a ball mill that won't itself be worn down and contaminate what is being ...
27-1-2013 at 09:53
by: bmays
Isolating tert-Butyl from a solution of petroleum distilate.
Wynns hot shot injector cleaner with octane booster.
10-1-2013 at 19:42
by: bmays
Isolating tert-Butyl from a solution of petroleum distilate.
Injector cleaner contains 10% tert-butyl and 50% petroleum distillates...doesn't say what the other ...
10-1-2013 at 02:44
by: bmays
Anything besides heat that reliably destroys organic compounds?
Breaking them to their base elements, or just breaking all carbon bonds.
1-1-2013 at 22:00
by: bmays
Pyridine a substitute for pyrdine hcl in demethylation reaction?
Heating the amine with pyridine hcl to 230c in a dry inert atmosphere is specified. I think refluxin ...
26-12-2012 at 13:30
by: bmays
Rhodiums loss of GABA to GHB
Just distill it, atmospheric is fine but all glass is necessary. Discard the first bit, shut it off ...
7-12-2012 at 22:08
by: bmays
Mysterious White Powder
On a hotplate with some sand you can get a general idea of the melting point, boiling point, decompo ...
1-10-2012 at 22:30
by: bmays

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