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Purifying of denaturated alcohol.
[rquote=415816&tid=63104&author=Bot0nist]You say 3L of [b]pure[/b] ethanol... I assume you m ...
22-8-2015 at 08:49
by: dermolotov
Possible OTC, 'safe' methylating agents
[rquote=415457&tid=11580&author=clearly_not_atara]Not terrifically safe, but -- silver tosyl ...
22-8-2015 at 08:43
by: dermolotov
Buchwald Hartwig Cross Coupling - Any Stories?
[rquote=415838&tid=63305&author=RareEarth]What kind of Pd catalyst are you using?[/rquote]
...
22-8-2015 at 08:29
by: dermolotov
Buchwald Hartwig Cross Coupling - Any Stories?
[rquote=415820&tid=63305&author=AvBaeyer]A good deal of the Buchwald-Hartwig chemistry is fr ...
13-8-2015 at 22:49
by: dermolotov
Buchwald Hartwig Cross Coupling - Any Stories?
Tossing out a wild question here in hopes of answers.
After two failed attempts with a Pd-catalyse ...
13-8-2015 at 15:37
by: dermolotov
Purifying of denaturated alcohol.
[rquote=413568&tid=63104&author=aga]It is far simpler to brew yourself some crude ethanol an ...
13-8-2015 at 13:11
by: dermolotov
Reductive Amination
I believe raney nickel is used only because of its price on the industrial level. I have never even ...
13-8-2015 at 13:06
by: dermolotov
Uses for H2WO4???
[rquote=414088&tid=63158&author=diggafromdover]Make the Tungstic Acid into a salt and ship i ...
13-8-2015 at 13:02
by: dermolotov
Bad Habits In The Lab
I'm probably going to be shamed to hell and back for this but... I smoke a cigar when I do refluxes/ ...
21-4-2015 at 19:47
by: dermolotov
Bromo-methane Disposal - Quick Question
Quick Question, gents.
Just routinely demethylating an anisole to produce a phenol. More specifical ...
21-4-2015 at 19:28
by: dermolotov
Platinum Wire for Electrolysis
[rquote=397127&tid=61786&author=cyanureeves]i can plate stuff but just cant get it to stick ...
15-3-2015 at 18:53
by: dermolotov
Synthesis of Aluminium Phenoxide
[rquote=397125&tid=61808&author=gdflp]I can't answer definitively, but this thread may be of ...
15-3-2015 at 18:31
by: dermolotov
Platinum Wire for Electrolysis
[rquote=397123&tid=61786&author=cyanureeves]dermolotov how similiar?have you electroplated w ...
15-3-2015 at 18:11
by: dermolotov
Synthesis of Aluminium Phenoxide
Ah! Brilliant. This was the exact pdf that I found a few days ago. For some reason, I couldn't find ...
15-3-2015 at 17:55
by: dermolotov
Platinum Wire for Electrolysis
[rquote=397080&tid=61786&author=jock88]
Try to purchase a used Pt crucible (scrap) if you c ...
15-3-2015 at 17:45
by: dermolotov
Synthesis of Aluminium Phenoxide
Addendum: I should mention that gritted aluminium is one of the biggest wastes of money if I can jus ...
15-3-2015 at 17:42
by: dermolotov
Synthesis of Aluminium Phenoxide
I can't find any current methods of this synthesis at the moment. The only one came from an old manu ...
15-3-2015 at 17:34
by: dermolotov
Palladium on Carbon Hydrogenation - Working out the kinks
Late time bump. things have been too cold nowadays to work in my shed. I might have discovered a new ...
15-3-2015 at 17:31
by: dermolotov
5 Ltr rbf, hotplate, other bits too!
200 quid or dollars?

Overhead stirrer is bloody expensive most of the times. 200 would be great i ...
11-1-2015 at 12:22
by: dermolotov
Naoum's improved glass nitrating funnel
Honestly... This just looks way too overcomplicated. I can understand why someone would want if nitr ...
10-1-2015 at 13:27
by: dermolotov
Magic!
I do the same with my hotplate/stirrer (Corning PC 420) for overnight oxidation sometimes. Since it ...
10-1-2015 at 13:09
by: dermolotov
OTC Calcium Chloride - Good for Drying
Yupp. This is what I recommend in lue of impure Magnesium Sulphate and others.

This I have found ...
7-1-2015 at 10:43
by: dermolotov
Any one else feel good after smelling ammonia?
[rquote=383875&tid=58153&author=forgottenpassword]Smelling salts are tried and teated over g ...
3-1-2015 at 15:29
by: dermolotov
Ammonia and tap water
[rquote=384846&tid=59438&author=gardul]Awesomeness - Since my local store only had ammonia i ...
3-1-2015 at 15:28
by: dermolotov
Iodine from iodised salt?
[rquote=383623&tid=58625&author=blogfast25]
You'll form also ICl.[/rquote]
Didn't know the ...
29-12-2014 at 11:52
by: dermolotov
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