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First nickel nitrate synthesis... did I do it right?
How much ethanol did you use, surely some should pass the filter, my mix was super gloopy and even i ... |
13-12-2021 at 15:53
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
Paper towels are my usual choice but they Usually take days to fully dry the NHN, steam bath works v ... |
13-12-2021 at 12:09
by: fredsci93 |
NHN synthesis not working
the freebasing gets very hot, so much to that it can occasionally boil, cooling (if not an ice bath ... |
13-12-2021 at 12:05
by: fredsci93 |
NHN synthesis not working
[rquote=668574&tid=154712&author=MineMan]
You should follow LL. CHP I believe is better t ... |
13-12-2021 at 03:34
by: fredsci93 |
Cesium Reduction/Distillation
this? https://www.youtube.com/watch?v=Ymgu_LaDrN0 |
13-12-2021 at 01:22
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
Yea, I only filtered it after my mix wouldn’t settle out, but it cleaned up the product alot.
T ... |
13-12-2021 at 01:18
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
yea, 20g scale is good and would make ~10g NHN, add 12.2g sodium hydroxide to 20g hydrazine sulphate ... |
12-12-2021 at 19:46
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
Yea, it’s fine so long as the beaker is mostly covered (as shown in the photos) |
12-12-2021 at 19:42
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
Your synth technique sounds fine, probably something weird making it fail.
As for the freebasing yo ... |
12-12-2021 at 18:07
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
[rquote=668546&tid=158176&author=ManyInterests]
Edit: Hydrazine question: I realize the ans ... |
12-12-2021 at 15:19
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
the pH looks alright, you could remove the cloudiness with a filtration which would improve the colo ... |
12-12-2021 at 14:04
by: fredsci93 |
Hydrazine
One test for hydrazine is to heat the hydrazine sulfate with nitric acid to ~70C and pass the produc ... |
12-12-2021 at 11:58
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
it looks a little more turquoise that one would expect, probably has some nickel hydroxide, what's t ... |
12-12-2021 at 11:49
by: fredsci93 |
NHN synthesis not working
[rquote=668495&tid=154712&author=ManyInterests]
Edit: I added calcium hypochlorite and some ... |
12-12-2021 at 01:44
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
[rquote=668500&tid=158150&author=S.C. Wack]
FWIW the original lit says "Im Porzellantiege ... |
12-12-2021 at 01:36
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
First off, One can melt cast ETN by submerging the ETN in a boing water bath, I put 500mg ETN in the ... |
12-12-2021 at 01:28
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
For my det caps I use a centrifuge tube with 500mg melt cast ETN at the Bottom, 200mg ETN in the mid ... |
11-12-2021 at 12:30
by: fredsci93 |
NHN synthesis not working
Yea, just add the nickel nitrate in water to the ethanol solution, the concentrations aren’t cruci ... |
11-12-2021 at 12:20
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
On the sensitivity, it's going to go off if you hit it with a hammer most times (I use a honking 2kg ... |
10-12-2021 at 22:58
by: fredsci93 |
NHN synthesis not working
If the nickel nitrate is fully dried then the pH will not be a problem, I would strongly dissuade hy ... |
10-12-2021 at 22:48
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
You shouldn’t have much in the way of contaminants (given you had pure nickel metal) so you could ... |
10-12-2021 at 22:34
by: fredsci93 |
NHN synthesis not working
[rquote=668422&tid=154712&author=ManyInterests] Is the green liquid nickel nitrate? Can I us ... |
10-12-2021 at 22:25
by: fredsci93 |
WARNING: Explosive reaction between pool chlorine chemicals
That's terrifying, I can't believe I had never heard about that, makes some sense in retrospect thou ... |
6-12-2021 at 15:25
by: fredsci93 |
Noob question about nitration reactions
[rquote=666826&tid=157957&author=wmacturk]Sorry for the late response. That's interesting. ... |
6-12-2021 at 15:20
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
Hydrazine produced from hydrazine sulfate + NaOH seems to be much less suitable for NHN synthesis si ... |
6-12-2021 at 02:45
by: fredsci93 |
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