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Benzylamine via the delepine reaction
[rquote=468452&tid=70913&author=gluon47]
[i] 60g of benzyl chloride, 60 of urea and 40cc of ... |
21-1-2017 at 20:19
by: gluon47 |
Williamson ether synthesis
I'm planning to make some tert-butyl ethyl ether via Williamson ether synthesis. Although I understa ... |
1-1-2017 at 00:19
by: gluon47 |
Benzylamine via the delepine reaction
OK, you've convinced me CuReUS. If I can make some magnesium nitride, I will probably give it a go.
... |
20-12-2016 at 10:31
by: gluon47 |
Benzylamine via the delepine reaction
Wow, that sounds interesting, magnesium nitride far out!
However if the magnesium nitride forms a ... |
19-12-2016 at 22:32
by: gluon47 |
Benzylamine via the delepine reaction
To answer your question, there's not really any specific use I have for benzylamine, I just find t ... |
13-12-2016 at 20:03
by: gluon47 |
Benzylamine via the delepine reaction
That would yield p-methylaniline (p-toluidine) not benzylamine. To make benzylamine this way, you wo ... |
12-12-2016 at 20:52
by: gluon47 |
Benzylamine via the delepine reaction
@Metacelsus thanks for the explanation! the whole thing makes a lot more sense to me now.
@A ... |
8-12-2016 at 10:39
by: gluon47 |
Benzylamine via the delepine reaction
I've had to change my plans a bit. Although Avbaeyer's write up looked very appealing, I'm currently ... |
7-12-2016 at 22:02
by: gluon47 |
The Short Questions Thread (4)
Ok, I went ahead and dried the isopropylamine over NaOH. The amine looks like it has taken on a slig ... |
4-12-2016 at 21:29
by: gluon47 |
The Short Questions Thread (4)
Thanks, I suspected It might react. I might try drying over sodium hydroxide, But doesn't the commer ... |
3-12-2016 at 21:21
by: gluon47 |
drying isopropylamine
Just finished distilling a Bach of isopropylamine extracted from a glyphosate herbicide. I want to d ... |
3-12-2016 at 17:10
by: gluon47 |
Benzylamine via the delepine reaction
Thanks for sharing avbaeyer!
I'll definitely try making some chloroform more efficiently then tr ... |
27-11-2016 at 21:35
by: gluon47 |
Benzylamine via the delepine reaction
yes, I suspected so. Ammonia from the ammonium chloride. Methylamine from the ammonium chloride reac ... |
27-11-2016 at 10:27
by: gluon47 |
Benzylamine via the delepine reaction
I've attached the write up so I could include images.
I didn't manage to isolate the freebase, b ... |
26-11-2016 at 22:29
by: gluon47 |
Benzylamine via the delepine reaction
I've been taking plenty of photos along the way. I'll be sure to include them. Thanks! |
26-11-2016 at 11:46
by: gluon47 |
Benzylamine via the delepine reaction
I'm performing the reaction. Everything looks good so far. If anyone is interested and if I get any ... |
26-11-2016 at 11:31
by: gluon47 |
Benzylamine via the delepine reaction
Thanks all of you for your advice so far.
I think I'll use ethanol as the solvent for the reacti ... |
20-11-2016 at 10:36
by: gluon47 |
Benzylamine via the delepine reaction
Thanks for the response!
I've tried making chloroform several times using the same reaction as ni ... |
19-11-2016 at 22:59
by: gluon47 |
Benzylamine via the delepine reaction
I receintly made some benzyl chloride via the free-radical halogenation of toluene. I beleive my pro ... |
19-11-2016 at 21:59
by: gluon47 |
Excess toluene for benzyl chloride synth
I'm planning to make a small amount of benzyl chloride sometime soon. The chlorination of toluene in ... |
16-10-2016 at 23:30
by: gluon47 |
Ethyl nitrate
I'm planning to make some ethyl nitrate soon using the method described here
http://www.prepchem.co ... |
27-7-2016 at 23:16
by: gluon47 |
Methyldichloramine
Your right, Sorry I'm no master of organic chemistry.
I swear I'm not any of the above. I just li ... |
6-6-2016 at 11:51
by: gluon47 |
Methyldichloramine
[rquote=450879&tid=66290&author=aga]methyl dichloramine or isopropyl dichloramine ?
Are ' ... |
5-6-2016 at 13:59
by: gluon47 |
Methyldichloramine
[rquote=450839&tid=66290&author=CuReUS]there are other ways to make the target compound
1. ... |
5-6-2016 at 13:02
by: gluon47 |
Methyldichloramine
Of course! I forgot HCl and NaOCl produce chlorine.
I do have access to glacial acetic acid and I ... |
4-6-2016 at 13:13
by: gluon47 |
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