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Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Oh I have that thread bookmarked, still have to try that synthesis out. I didn't read through the wh ... |
11-6-2021 at 21:28
by: mr_bovinejony |
Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Do you have the link for that thread? |
11-6-2021 at 09:41
by: mr_bovinejony |
16 oz of nitroethane. Buy or nah?
Ohh I recognize that brand. I'm curious to know how much of a yield you get if you distill it |
7-6-2021 at 09:05
by: mr_bovinejony |
Indole-3-Carbinol Oxidation
Sure haven't! I'm going to run a tlc on these indoles I have now for practice |
5-6-2021 at 07:47
by: mr_bovinejony |
Indole-3-Carbinol Oxidation
I had some succes recrystallizing indole 3 aldehyde with dmf and water, maybe it'll work for indole ... |
5-6-2021 at 06:43
by: mr_bovinejony |
Indole-3-Carbinol Oxidation
Yeah I still have them, but the color is stupid and two recrystalizations later helped none. It's a ... |
5-6-2021 at 06:23
by: mr_bovinejony |
Indole-3-Carbinol Oxidation
I have already tried this with PCC twice with no success, but I haven't seen any other trials so don ... |
5-6-2021 at 03:58
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
Not sure why I can't edit the posts, but I have the images saved for if they do disappear. I don't t ... |
28-5-2021 at 17:41
by: mr_bovinejony |
LabDIRECT is now an Official US TCI Distributer!
Is there any kind of markup for these products? I imagine a very good percentage of my chemicals wil ... |
27-5-2021 at 14:56
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
The end of the vilsmeier saga: part one
5 grams of pcl5 is added to 5 ml of dmf. This heats up a ... |
26-5-2021 at 16:12
by: mr_bovinejony |
Elemental Scientific Liquidating Chemicals, glassware, and used equipment
Is this something you have to pick up in person? Or can they be shipped? |
25-5-2021 at 19:28
by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind
Very!! Bromo saccharin is incredibly easy to make. And it's much less irritating than nbs, although ... |
24-5-2021 at 20:23
by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind
Yes it did work, in fact it was as easy as replacing nbs with it in this bromination of 2ch. But fo ... |
24-5-2021 at 17:28
by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind
Dissolve 2ch in a minimum amount of gaa and add an equal weight of nbs! The product will precipitate ... |
24-5-2021 at 15:11
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
Of course not, I'm looking for some indole identification right now
The stuff decomposed once it ... |
24-5-2021 at 08:38
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
One last update until I get some real results, this first picture here is what I'm thinking is the f ... |
24-5-2021 at 07:52
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
Some interesting thing happens now, 5 grams of pcl5 are added to 5 ml of ice cold dmf. After this is ... |
24-5-2021 at 00:22
by: mr_bovinejony |
A foray into phenethylamines of the Shulgin kind
You added all the nabh4 at once to a solution of the nitrostyrene and refluxed? Or they were partial ... |
21-5-2021 at 17:27
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
All experiments with the formation of the vh reagent in dmf and pcl5 have failed, I guess there is s ... |
21-5-2021 at 10:20
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
I'm not sure where you buy your reagents but the place I get mine from pocl3 is readily available, a ... |
19-5-2021 at 03:10
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
I have the opposite problem, I have pcl5 easily but not p2o5. I have seen that procedure though, and ... |
17-5-2021 at 10:44
by: mr_bovinejony |
Vilsmeier reagent/POCl3 formation
I have plans to try out the Vilsmeier Haack reaction, but only have PCl5 for it. I found a paper her ... |
15-5-2021 at 21:31
by: mr_bovinejony |
Thermometers,Clamps and stuff
Is this real life? It's nice to see this account posting again |
13-5-2021 at 21:15
by: mr_bovinejony |
Dichromate overoxidation
Oooo don't give me any more ideas! There's already too much on the list  |
24-4-2021 at 16:10
by: mr_bovinejony |
Dichromate overoxidation
@carl I do have that paper downloaded like 3 times on my phone, ill have to dig for it. The only rea ... |
24-4-2021 at 10:58
by: mr_bovinejony |
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