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Latest chemical order?
300g Oxalic acid
50g sodium bromide
1lb potassium nitrate (not reagent grade...)

And a thermome ...
8-8-2017 at 10:59
by: myristicinaldehyde
"Mn(V) sulfate" Woes
[rquote=485841&tid=74797&author=AJKOER]Per the following redox reaction, I suspect, one may ...
18-6-2017 at 13:36
by: myristicinaldehyde
"Mn(V) sulfate" Woes
[rquote=485816&tid=74797&author=Cryolite.]You probably can purify your manganese paste via a ...
17-6-2017 at 16:21
by: myristicinaldehyde
"Mn(V) sulfate" Woes
Yup, I used battery crap. Which probably explains the results.

I took the failed second run, adde ...
17-6-2017 at 05:55
by: myristicinaldehyde
"Mn(V) sulfate" Woes
Based on this post (which is based on neograviton's method), I decided to attempt the preparation of ...
15-6-2017 at 14:20
by: myristicinaldehyde
Best and worst smelling chemicals?
[rquote=472423&tid=1216&author=myristicinaldehyde]I discovered a new least favorite: 1-bromo ...
26-5-2017 at 14:21
by: myristicinaldehyde
Copper Dichloroisocyanurate Complex Synthesis and Analogs.
I tried iron once- using a solution of iron(iii). The color intensified, to an impressive red but no ...
7-5-2017 at 16:55
by: myristicinaldehyde
Tetramine nickel chlorate
Symboom, your post is blank.
29-3-2017 at 04:11
by: myristicinaldehyde
Sodium Carbonate and Aluminum reaction
[rquote=479209&tid=71493&author=Booze][rquote=470391&tid=71493&author=Fulmen]The mai ...
28-3-2017 at 16:45
by: myristicinaldehyde
Favorite chemical drawing programs?
I use BIOVA Draw 2016, mostly because it's free. That being said, I don't actually know how to prope ...
28-3-2017 at 14:06
by: myristicinaldehyde
help with mechanisms
The simplest answer is that LAH is used strictly in anhydrous conditions, and reacts aggressively wi ...
2-3-2017 at 16:45
by: myristicinaldehyde
help with mechanisms
The 2nd step would tautomerize to the imine- the acidic solution would then hydrolyze it to 2-butano ...
26-2-2017 at 08:32
by: myristicinaldehyde
Unique silver compounds
I would guess the pink precipitate is silver sulfite, which apparently decomposes very readily on ex ...
9-2-2017 at 16:02
by: myristicinaldehyde
Best and worst smelling chemicals?
I discovered a new least favorite: 1-bromo 3,5 dimethoxy benzene.
It has a unique and lingering odo ...
20-1-2017 at 18:26
by: myristicinaldehyde
Selling: 3,4,5-Trimethoxybenzaldehyde >99%
[rquote=471693&tid=62680&author=Melgar][rquote=408621&tid=62680&author=zed]There is ...
12-1-2017 at 12:11
by: myristicinaldehyde
Sodium Carbide synthesis(acetylene)
https://www.google.com/patents/US2802723
1-1-2017 at 05:43
by: myristicinaldehyde
aluminium hydride from aluminium formate
[rquote=470305&tid=71457&author=smartgene1]what about with magnesium aluminide or raney nick ...
29-12-2016 at 13:00
by: myristicinaldehyde
Aluminum bromide, AlBr3
AlBr3 can also cleave ethers- my new research group will be using it for that purpose. Maybe it will ...
17-12-2016 at 09:24
by: myristicinaldehyde
Need ideas!
Well, if you have a large amount of black (or preferably) white pepper, you could extract the piperi ...
12-12-2016 at 16:37
by: myristicinaldehyde
4-piperidone drying?
Sigma Aldrich sells this as the monohydrate (http://www.sigmaaldrich.com/catalog/product/aldrich/151 ...
1-12-2016 at 16:32
by: myristicinaldehyde
acetoxy-methoxy exchange from acetylsalicylic acid? [edit]
The problem with your scheme is that anisole is an ether, not a ester! You can't exchange the entire ...
6-11-2016 at 16:42
by: myristicinaldehyde
Alternative Nitroethane Synthesis
https://erowid.org/archive/rhodium/chemistry/nitroethane.html
3-11-2016 at 11:12
by: myristicinaldehyde
Halide-free Friedel-Crafts acylation, using P2O5 as both Lewis acid and acid dehydrator
Chemplayer has a video on this too-https://www.youtube.com/watch?v=xAUlglOiVos
24-10-2016 at 04:01
by: myristicinaldehyde
What to do with extra nitromethane
1) Henry condensation with vanillin- Chemplayer has a video. You could then reduce it to the carbony ...
11-10-2016 at 14:10
by: myristicinaldehyde
"Indicator" solution of copper(ii) salicylate in dilute acetic acid
Olive green sounds right, and the most acidic solutions I got were a pale turquoise. Thanks for the ...
9-10-2016 at 12:18
by: myristicinaldehyde
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