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Proposed novel 6-step syntheis of 5-MeO-4-AcO-DMT
Needs references
13-6-2021 at 05:25
by: njl
Oxalyl Chloride Challenge
What if we tried chlorinating glyoxal???
9-6-2021 at 08:10
by: njl
Choice of oxidants for tinder

[quote]
KBrO3 - 69 g/l @ 20 C, 167 g/mol, 0,41 mol/l
KClO3 - 81 g/l @ 25 C, 122 g/mol, 0,66 mol/ ...
7-6-2021 at 12:49
by: njl
16 oz of nitroethane. Buy or nah?
[quote]
I always get back just a little bit more product than the amount of aldehyde I put in
[/qu ...
7-6-2021 at 12:45
by: njl
The Short Questions Thread (4)
Carboxylic acids can be activated by formation of mixed anhydrides. Could the acid instead be reacte ...
6-6-2021 at 16:12
by: njl
Preparation of dimethyl carbonate without autoclave or phosgene
As you know ethylene glycol is less volatile than methanol so beyond using a large excess of methano ...
5-6-2021 at 10:17
by: njl
Indole-3-Carbinol Oxidation
I think we all have a few "side projects" like that collecting dust :D
5-6-2021 at 06:29
by: njl
Indole-3-Carbinol Oxidation
To what end, karl? Just out of curiosity.
5-6-2021 at 05:54
by: njl
16 oz of nitroethane. Buy or nah?
[rquote=661306&tid=157565&author=draculic acid69][rquote=661280&tid=157565&author=ch ...
5-6-2021 at 04:43
by: njl
Aldehyde oxidation
I would like to try DCM for the workup instead of ether. Does DCM react with hypochlorite? I can't f ...
4-6-2021 at 10:05
by: njl
Dragendorff reagent preparation
How confident are you in the purity of the bismuth compound? I would check its reaction with other a ...
4-6-2021 at 06:20
by: njl
Dragendorff reagent preparation
That's really odd, I would assume the mixed oxide/nitrate wouldn't be soluble but with added acid I ...
4-6-2021 at 05:47
by: njl
Cicada fungi
Very cool paper Zed, it also happens to mention a different cicada fungi that yields some ergot deri ...
4-6-2021 at 03:51
by: njl
Cicada fungi
Karl, it could definitely be contamination. All I know is a few local news stations have run with it ...
3-6-2021 at 16:27
by: njl
Cicada fungi
I thought I would share some regional science here! Where I live, the famous 17 year brood X cicadas ...
3-6-2021 at 12:30
by: njl
Aldehyde oxidation
Ok no answers there, but I would like to report some success using basic aqueous NaOCl and no additi ...
3-6-2021 at 07:59
by: njl
What to dissolve Stannic acid with?
For me HCl would be best, but it depends on what you want to keep.
1-6-2021 at 12:31
by: njl
Ideas for Engineering In-Demand Lab Equipment
1. MP testing equipment
2. Recirculating water heater/cooler, useful for hot and cold water baths a ...
27-5-2021 at 08:09
by: njl
Methyl ester and o-methylation of sinapic acid
Really refreshing stuff! Would love to hear more about the other acids you tried, and the experiment ...
26-5-2021 at 11:33
by: njl
A foray into phenethylamines of the Shulgin kind
I have seen some CuCl2 write ups, I have not seen any NBS brominations. Sounds like you are familiar ...
24-5-2021 at 11:20
by: njl
A foray into phenethylamines of the Shulgin kind
[rquote=660505&tid=157496&author=karlosĀ³]Great stuff!
Have you used my writeup on 2C-H by ...
24-5-2021 at 07:22
by: njl
Orthosilicate esters from silica gel
I think you would need very high temperatures for that, maybe higher than the boiling point of sulfu ...
24-5-2021 at 07:18
by: njl
Green hydrogen production
What are your thoughts on promising green hydrogen technologies? More specifically, which reactions/ ...
24-5-2021 at 06:42
by: njl
so much bubbles in glass
I'd really avoid putting much stress on that joint, and distillations where the vapor front moves sl ...
21-5-2021 at 06:23
by: njl
Orthosilicate esters from silica gel
Problem is EG is much less volatile than ethanol. So there's nothing driving the equilibrium towards ...
20-5-2021 at 10:05
by: njl
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