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Chemistry of Terephthalic acid
It is no problem Boffis, just an idea I had (excellent analogy, by the way). I'm currently looking i ... |
13-9-2015 at 12:32
by: nlegaux |
What to do with tryptamine?
Something else that can be done is a Pictet-Spengler reaction allowing for the creation of interesti ... |
12-9-2015 at 16:27
by: nlegaux |
Chemistry of Terephthalic acid
It is rather ironic that something so seemingly foolish could kill such a brilliant chemist.
Anot ... |
12-9-2015 at 14:27
by: nlegaux |
Chemistry of Terephthalic acid
A reaction I haven't seen listed yet is Letts nitrile synthesis. If you react the terepthalic acid w ... |
11-9-2015 at 10:39
by: nlegaux |
What to do with tryptamine?
You could perform a Hofmann rearrangement using the tryptamine. It would remove the α-carbon shorte ... |
11-9-2015 at 10:34
by: nlegaux |
Preparation of 2-aminophenol from Salicylic Acid
I attempted the acid hydrolysis yesterday. I added 3ml 96% H2SO4 to 0.5g benzoxazolone and refluxed ... |
2-9-2015 at 11:04
by: nlegaux |
Preparation of 2-aminophenol from Salicylic Acid
Nice find on the patent nitro-genes! It offered a lot of insight. I have been isolating the benzoxaz ... |
1-9-2015 at 12:55
by: nlegaux |
Preparation of 2-aminophenol from Salicylic Acid
The Diammonium phosphate idea isn't a bad one... Once I perfect the second stage of this synthesis, ... |
28-8-2015 at 13:23
by: nlegaux |
Preparation of 2-aminophenol from Salicylic Acid
Is this better characterization of the salicylamide intermediate?
"The final product was a white ... |
21-8-2015 at 19:14
by: nlegaux |
Preparation of 2-aminophenol from Salicylic Acid
Thank you for these pointers, I will work on improving/correcting the report. The final product is a ... |
17-8-2015 at 11:02
by: nlegaux |
Preparation of 2-aminophenol from Salicylic Acid
Presented below is a useful procedure for the production of salicylamide, benzoxazolone, and ultimat ... |
16-8-2015 at 17:36
by: nlegaux |
Strongest Acid
Fluoroantimonic acid has a pKa of -25. It is also interesting because it is an ionic liquid.
https: ... |
10-7-2015 at 14:55
by: nlegaux |
Deep Eutectic Solvents (OTC Ionic Liquid)
I have been able to create a Type IV deep eutectic solvent by heating a 1:1 molar ratio of AlCl3 and ... |
9-7-2015 at 19:06
by: nlegaux |
Phenoxyacetic Acid Synthesis
On the MSDS the dimethylamine salt of 2,4-D is listed as an amber colored liquid. Whether this means ... |
21-6-2015 at 18:58
by: nlegaux |
Phenoxyacetic Acid Synthesis
Because of the new information stated previously, I have attempted the separation a third time. I st ... |
20-6-2015 at 16:34
by: nlegaux |
Phenoxyacetic Acid Synthesis
The precipitate formed after allowing the solution to cool at room temperature is still too fine to ... |
20-6-2015 at 13:57
by: nlegaux |
Phenoxyacetic Acid Synthesis
Earlier I checked the MSDS for the product and nothing else was listed, but as you said Pumukli ther ... |
19-6-2015 at 11:37
by: nlegaux |
Phenoxyacetic Acid Synthesis
For now I am only interested in obtaining the product, but in the future I would like to attempt syn ... |
18-6-2015 at 06:34
by: nlegaux |
Phenoxyacetic Acid Synthesis
Thank you for the excellent suggestion Pumukli, tomorrow I plan on going to the local hardware store ... |
17-6-2015 at 17:23
by: nlegaux |
Phenoxyacetic Acid Synthesis
Hello all. Recently I have been looking into synthesizing 2,4-Dichlorophenoxyacetic acid to be used ... |
17-6-2015 at 08:12
by: nlegaux |
Difficulty with AlCl3/Urea DES
I have found that a 1:1 molar ratio of AlCl3/Urea heated under mineral oil forms a eutectic that see ... |
9-5-2015 at 15:42
by: nlegaux |
Difficulty with AlCl3/Urea DES
I am trying to create an Aluminum Chloride/Urea deep eutectic solvent. This and the other type IV DE ... |
21-4-2015 at 14:13
by: nlegaux |
Copper Salicylate
Thanks for the link! Not sure how I missed that in the search. Is there a practical way to test if i ... |
21-1-2015 at 16:49
by: nlegaux |
Copper Compound Collection
Thanks for the tip! I will definitely have to check my local hardware store for some. |
20-1-2015 at 19:09
by: nlegaux |
Copper Salicylate
I recently prepared some copper salicylate. Since there is nothing on the forum about it (the only s ... |
19-1-2015 at 13:41
by: nlegaux |
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