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Fluoroform for -CF3 incorporation I have a 10lb cylinder of fluoroform. Anyone have any interesting ideas of what to do with it?
I ... |
22-4-2020 at 16:15 by: numos |
Help with lecture bottles? I thought it was a temperature thing as well, but heating it to 40C had no effect. It should have a ... |
19-4-2020 at 22:16 by: numos |
Help with lecture bottles? I've worked with lecture bottles before, and I have this beautiful bottle of NO2 that by tare, is co ... |
19-4-2020 at 16:39 by: numos |
Setting up a home Schlenk system Thank you all for the kind words!
[rquote=634337&tid=155190&author=Heptylene]Wow incredib ... |
19-4-2020 at 15:37 by: numos |
The mingling of Palladium and Arsenic Probably not anytime soon. I wanted to make the Pd complex because I've used the PPh3 analog for cou ... |
17-4-2020 at 18:49 by: numos |
Setting up a home Schlenk system There was some interest in doing Schlenk chemistry, and I hope this post can do it justice. Doing ai ... |
17-4-2020 at 18:46 by: numos |
Hand sanitizer ratio Just multiply everything by final amount
If you want 1kg
1 kg x .7 = 700 g
1 kg x .05 = 50 g
... |
10-4-2020 at 15:21 by: numos |
The mingling of Palladium and Arsenic [rquote=633805&tid=155152&author=woelen]AsI3 is something, which I could try.[/rquote]
Gl ... |
10-4-2020 at 11:41 by: numos |
The mingling of Palladium and Arsenic Also, I know a few of you have asked to see my schlenk setup. I'm working on putting that together i ... |
8-4-2020 at 18:47 by: numos |
The mingling of Palladium and Arsenic Dichlorobis(triphenylphosphine)palladium is a very common precatalyst in cross coupling reactions. B ... |
8-4-2020 at 18:43 by: numos |
Synthesis of substituted azulenes Indeed it's getting excellent use now. I guess I'm thankful I have something to do at home. Some of ... |
4-4-2020 at 15:22 by: numos |
A convenient home synthesis of brightly colored pyrylium compounds Mayko took care of the papers (thanks!), but if it's the preps you are interested in, they can be fo ... |
4-4-2020 at 12:43 by: numos |
Synthesis of substituted azulenes Azulenes are beautifully colored compounds which are, for the most part, inaccessible to the home ch ... |
3-4-2020 at 17:59 by: numos |
A convenient home synthesis of brightly colored pyrylium compounds I'm glad this post was so well recieved!
[rquote=633512&tid=155119&author=Boffis]
Do you ... |
3-4-2020 at 11:50 by: numos |
A convenient home synthesis of brightly colored pyrylium compounds Labs are shut down, so I find myself having a bit more free time.....
I recently got interested i ... |
2-4-2020 at 14:26 by: numos |
Custom milled heating blocks Something that's always annoyed me about the aluminum heating blocks by IKA and various other suppli ... |
16-3-2020 at 16:59 by: numos |
Original Jack Roberts compounds [rquote=632426&tid=155003&author=Heptylene][rquote=632421&tid=155003&author=phlogist ... |
11-3-2020 at 18:59 by: numos |
Preparation of Arsenic trichloride [rquote=632396&tid=155002&author=Bedlasky]Interesting synthesis.
What complexes of Pd wit ... |
10-3-2020 at 14:40 by: numos |
Original Jack Roberts compounds [rquote=632411&tid=155003&author=Heptylene]Incredibly cool find! Do you know how old they ar ... |
10-3-2020 at 14:29 by: numos |
Preparation of Arsenic trichloride [rquote=632341&tid=155002&author=njl]what are those metal pellets you're using for temp cont ... |
9-3-2020 at 23:07 by: numos |
Original Jack Roberts compounds Came across a set of compounds which were made in the lab of Jack Roberts. I've taken pictures of so ... |
8-3-2020 at 21:40 by: numos |
Preparation of Arsenic trichloride Took a break from organic chemistry this weekend and decided to make some triphenylarsine to make so ... |
8-3-2020 at 18:55 by: numos |
An assortment of fluorescent pyridine copper iodides [rquote=631335&tid=154902&author=Heptylene]Wow really nice work! Some look really gorgeous l ... |
19-2-2020 at 21:42 by: numos |
An assortment of fluorescent pyridine copper iodides Based on the well known paper in chemical education (J. Chem. Educ. 2012, 89, 7, 946-949), I reckon ... |
18-2-2020 at 20:34 by: numos |
Synthesis of Boron subphthalocyanine chloride (with pictures!) [rquote=626108&tid=154316&author=wg48temp9]
Did you make the nitrile, if so how?
PS: Ac ... |
13-11-2019 at 22:25 by: numos |
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