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Acetanilide synthesis from aniline and acetic acid
[rquote=703301&tid=161282&author=MaeBorowski]Vogel calls for heating aniline with a roughly ...
19-9-2025 at 11:24
by: Keras
Laboratoriumdiscounter.nl ratings
Well, I have send them another mail about the carbon disulphide, zero answer after one week.
They h ...
17-9-2025 at 23:58
by: Keras
Increase Sintered Glass ("Frit") Pore Size
[rquote=703231&tid=161293&author=Sulaiman]
PS If you really have 99% vacuum (7.6mm Hg or 1k ...
15-9-2025 at 04:24
by: Keras
benzyl alcohol + sulphuric acid = ?
It would be interesting to do this experiment with a non-oxidising acid, such as phosphoric or metha ...
13-9-2025 at 00:05
by: Keras
storage of PCl5 and AlCl3
[rquote=703190&tid=161290&author=davidfetter]Sadly, quite a few halogenated compounds includ ...
12-9-2025 at 12:09
by: Keras
storage of PCl5 and AlCl3
[rquote=703182&tid=161290&author=woelen]The worst is PCl5, which is really really hard to ke ...
12-9-2025 at 02:37
by: Keras
My dessicator lid is shifting
[rquote=703139&tid=161287&author=teodor]I put as much as to remove air bubbles, but yes, I c ...
11-9-2025 at 07:42
by: Keras
storage of PCl5 and AlCl3
I have PCl₅ I ordered several years ago when I was beginning to set up my lab, it’s in an iron c ...
11-9-2025 at 07:39
by: Keras
My dessicator lid is shifting
I’m surprised. Mine is so tightly held I need really to push very hard to open it.
Are you sure y ...
10-9-2025 at 08:32
by: Keras
In-demand reagents
[rquote=703103&tid=161274&author=clearly_not_atara]
E.g. 1,1'-oxalyldiimidazole, the rxn pr ...
9-9-2025 at 07:04
by: Keras
Acetanilide synthesis from aniline and acetic acid
[rquote=703089&tid=161282&author=Diachrynic]A friend of mine has done and posted this proced ...
9-9-2025 at 01:35
by: Keras
Acetanilide synthesis from aniline and acetic acid
[rquote=703071&tid=161282&author=bnull]
[…]
[quote][b]Synthesis of compounds (I-IV) by g ...
9-9-2025 at 00:39
by: Keras
Laboratoriumdiscounter.nl ratings
[rquote=703065&tid=157773&author=Fery]I have also thiourea something like 10 kg.
Some old C ...
9-9-2025 at 00:07
by: Keras
Laboratoriumdiscounter.nl ratings
[rquote=703041&tid=157773&author=Fery]They used Stad Alkmaar Logistic and then Raben (very l ...
8-9-2025 at 00:22
by: Keras
Acetanilide synthesis from aniline and acetic acid
Folks,

there is a recipe on the book ‘Experimental Organic Chemistry, Laboratory Manual' descri ...
7-9-2025 at 23:42
by: Keras
Laboratoriumdiscounter.nl ratings
I agree they’re becoming sloppy. I have basic items like a 0…360°C thermometer in backorder fro ...
5-9-2025 at 00:41
by: Keras
In-demand reagents
[rquote=702945&tid=161274&author=BenJ]
I’m in the UK. Do you know of anything specific to ...
4-9-2025 at 06:23
by: Keras
Laboratoriumdiscounter.nl ratings
I have had some issues with them recently. They couldn't find a proper transporter to send me the bo ...
4-9-2025 at 00:56
by: Keras
Looking for Re-usable crucible for molten sodium hydroxide / silicate
I’m not sure why your stainless steel crucible eroded. I have done several fusion reactions in min ...
24-8-2025 at 21:48
by: Keras
successful method for purifying anthranilic acid(quick report)
[rquote=702677&tid=155744&author=Lionel Spanner]
The solubility of anthranilic acid in wate ...
22-8-2025 at 23:51
by: Keras
Spontaneous (non-shock) cracking of a borosilicate beaker
Having good quality beakers helps. For w/e raison I remember having recently put something in a stan ...
18-8-2025 at 21:51
by: Keras
Embarrassing question about Grignard reaction
I would expect the reaction to take place on the carbonyl carbon which is the most electropositive. ...
17-8-2025 at 23:42
by: Keras
Iodine stain damage and iodine storage
Keep your iodine under concentrated sulphuric acid? It is said to suppress the tendency of iodine to ...
17-8-2025 at 23:32
by: Keras
successful method for purifying anthranilic acid(quick report)
So, here is what I finally found on preparing pure (white) anthranilic acid:

• Use recrystallis ...
17-8-2025 at 00:38
by: Keras
wanted: Bulletin de la Société chimique de France
[url=https://gallica.bnf.fr]Gallica?[/url]
16-8-2025 at 12:58
by: Keras
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